CN204193896U - A kind ofly fast reaction can be realized and the reactor of discharging - Google Patents
A kind ofly fast reaction can be realized and the reactor of discharging Download PDFInfo
- Publication number
- CN204193896U CN204193896U CN201420636838.5U CN201420636838U CN204193896U CN 204193896 U CN204193896 U CN 204193896U CN 201420636838 U CN201420636838 U CN 201420636838U CN 204193896 U CN204193896 U CN 204193896U
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- catalytic liquid
- kettle
- storage tank
- cooling water
- liquid storage
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Abstract
The utility model discloses and a kind ofly can realize fast reaction and the reactor of discharging, comprise catalytic liquid storage tank, reactor body and cooling water circulation cooling system, zone of heating and catalytic liquid muff is disposed with outside described catalytic liquid storage tank, be provided with temperature indicator and controller in catalytic liquid storage tank side, controller is electrically connected with zone of heating.The utility model passes through at catalytic liquid storage tank arranged outside temperature indicator, catalytic liquid muff and zone of heating, allow to the catalytic liquid temperature conditions understood in time in catalytic liquid storage tank, and can make and adjusting timely, make catalytic liquid temperature remain at optimum state required for reaction; The catalytic liquid charging aperture on catalytic liquid storage tank and kettle is connected by communicating pipe, and measuring pump and flow control valve are set on communicating pipe, can be good at joining the dosage of reaction kettle body to catalytic liquid and speed controls, ensure the quality of reacting synthesis medicament and the medicine generated.
Description
Technical field
The utility model relates to pharmaceutical technology apparatus field, specifically a kind ofly can realize fast reaction and the reactor of discharging.
Background technology
In the process of carrying out pharmacy; various medicament, medicine often need catalyst to carry out catalysis to it when synthesizing; and; the speed that catalyst drips, dosage and temperature usually can cause larger impact to the quality of synthetic drug agent, medicine; existing medicament, drug synthetic reaction still Chang Wufa accomplish these; in addition; after the reaction was completed; often need to carry out cooling discharge to reactor; need to pass into a large amount of cooling circulating waters in the process and just can reach demand; a large amount of wastes will be caused to water like this, cannot using water wisely be accomplished.
Utility model content
The purpose of this utility model is that providing a kind of can realize fast reaction and the reactor of discharging, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the utility model provides following technical scheme:
A kind ofly fast reaction can be realized and the reactor of discharging, comprise catalytic liquid storage tank, reactor body and cooling water circulation cooling system, zone of heating and catalytic liquid muff is disposed with outside described catalytic liquid storage tank, be provided with temperature indicator and controller in catalytic liquid storage tank side, controller is electrically connected with zone of heating, described reactor body comprises kettle, water circulation layer is provided with outside kettle, kettle muff is provided with outside water circulation layer, kettle top is provided with stirring motor, catalytic liquid charging aperture is provided with on the left of stirring motor, catalytic liquid charging aperture is communicated with by communicating pipe with catalytic liquid storage tank, described communicating pipe is provided with measuring pump and flow control valve, material inlet and top cooling water delivery outlet is provided with on the right side of stirring motor, described autoclave body bottom is provided with discharging opening and bottom coohng water output, temperature indicator and cooling water jet is provided with on the right side of kettle, cooling water jet, top cooling water delivery outlet is all communicated with water circulation layer with bottom coohng water output, described cooling water circulation cooling system top and bottom are equipped with input, cooling water circulation cooling system side is provided with output, the input at cooling water circulation cooling system top and the input of bottom pass through cross current with the top cooling water delivery outlet on kettle and bottom coohng water output respectively, output is connected by water pipe with the cooling water jet on kettle, is respectively equipped with valve at described water pipe near the position of kettle and cooling water circulation cooling system, described catalytic liquid storage tank and kettle inside are provided with temperature sensor, and temperature sensor is electrically connected with temperature indicator.
As further program of the utility model: described measuring pump and flow control valve are all electrically connected with controller.
As further program of the utility model: described inner wall of kettle is provided with Polypropylene Anticorrosion Coating.
Compared with prior art, the utility model passes through at catalytic liquid storage tank arranged outside temperature indicator, catalytic liquid muff and zone of heating, allow to the catalytic liquid temperature conditions understood in time in catalytic liquid storage tank, and can make and adjusting timely, make catalytic liquid temperature remain at optimum state required for reaction, the catalytic liquid charging aperture on catalytic liquid storage tank and kettle is connected by communicating pipe, and measuring pump and flow control valve are set on communicating pipe, can be good at joining the dosage of reaction kettle body to catalytic liquid and speed controls, ensure the quality of reacting synthesis medicament and the medicine generated, after reaction terminates, need to carry out cooling discharge to reactor, now, open cooling water jet and top cooling water delivery outlet and bottom coohng water output, cooling water enters reactor water circulation layer after spraying, reactor is lowered the temperature, now can generating portion steam, steam is by top cooling water delivery outlet, take away amount of heat, when top, cooling water delivery outlet temperature drops to less than 100 degree, close bottom coohng water output, these export the higher water of rear temperature after the process of cooling water circulation cooling system, again enter into water circulation layer from cooling water jet, continue to lower the temperature to kettle, until reach technological requirement, this process has can prevent water hammer relative to existing device, also save cooling water amount.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: 1-catalytic liquid storage tank, 2-reactor body, 3-measuring pump, 4-flow control valve, 5-temperature indicator, 6-catalytic liquid muff, 7-catalytic liquid charging aperture, 8-material inlet, 9-discharging opening, 10-stirring motor, 11-kettle muff, 12-kettle, 13-zone of heating, 14-controller, 15-water circulation layer, 16-top cooling water delivery outlet, 17-bottom coohng water output, 18-cooling water jet, 19-cooling water circulation cooling system, 20-output, 21-input, 22-water pipe, 23-valve.
Detailed description of the invention
Below in conjunction with the accompanying drawing in the utility model embodiment, be clearly and completely described the technical scheme in the utility model embodiment, obviously, described embodiment is only the utility model part embodiment, instead of whole embodiments.Based on the embodiment in the utility model, those of ordinary skill in the art are not making the every other embodiment obtained under creative work prerequisite, all belong to the scope of the utility model protection.
Refer to Fig. 1, in the utility model embodiment, a kind ofly fast reaction can be realized and the reactor of discharging, comprise catalytic liquid storage tank 1, reactor body 2 and cooling water circulation cooling system 19, zone of heating 13 and catalytic liquid muff 6 is disposed with outside described catalytic liquid storage tank 1, temperature in catalytic liquid storage tank 1 can be regulated by zone of heating 13, the insulation to catalytic liquid storage tank 1 is realized by catalytic liquid muff 6, prevent the variations in temperature of catalytic liquid very fast, temperature indicator 5 and controller 14 is provided with in catalytic liquid storage tank 1 side, controller 14 is electrically connected with zone of heating 13, can be understood the temperature of catalytic liquid storage tank 1 inside timely by temperature indicator 5 in good time, made adjustment timely by controller 14 and zone of heating 13, described reactor body 2 comprises kettle 12, water circulation layer 15 is provided with outside kettle 12, lowered the temperature to completing reacted kettle 12 by water circulation layer 15, allow to fast cooling, rapid discharging, kettle muff 11 is provided with outside water circulation layer 15, kettle muff 11 can ensure the impact of material when reacting not by ambient temperature in kettle 12, remain good state of temperature, kettle 12 top is provided with stirring motor 10, stirring motor 10 can make fully to contact between various material, add the speed of fast response, catalytic liquid charging aperture 7 is provided with on the left of stirring motor 10, catalytic liquid charging aperture 7 is communicated with by communicating pipe with catalytic liquid storage tank 1, described communicating pipe is provided with measuring pump 3 and flow control valve 4, communicating pipe arranges measuring pump 3 and flow control valve 4, realize the control of speed and the dosage that catalyst is added, material inlet 8 and top cooling water delivery outlet 16 is provided with on the right side of stirring motor 10, discharging opening 9 and bottom coohng water output 17 is provided with bottom described kettle 12, temperature indicator 5 and cooling water jet 18 is provided with on the right side of kettle 12, cooling water jet 18, top cooling water delivery outlet 16 is all communicated with water circulation layer 15 with bottom coohng water output 17, described cooling water circulation cooling system 18 top and bottom are equipped with input 21, cooling water circulation cooling system 19 side is provided with output 20, the input 21 at cooling water circulation cooling system 19 top and the input 21 of bottom are communicated with by water pipe 22 with bottom coohng water output 17 with the top cooling water delivery outlet 16 on kettle 12 respectively, output 20 is connected by water pipe 22 with the cooling water jet 18 on kettle 12, valve 23 is respectively equipped with near the position of kettle 12 and cooling water circulation cooling system 19 at described water pipe 22, after reaction terminates, need to carry out cooling discharge to reactor, now, open cooling water jet 18 and top cooling water exports 16 mouthfuls and bottom coohng water output 17, cooling water enters reactor water circulation layer 15 after spraying, reactor is lowered the temperature, now can generating portion steam, steam is by top cooling water delivery outlet 16, take away amount of heat, when top, cooling water delivery outlet 16 temperature drops to less than 100 degree, close bottom coohng water output 17, these export the higher water of rear temperature after cooling water circulation cooling system 19 processes, again enter into water circulation layer 15 from cooling water jet 18, continue to lower the temperature to kettle 12, until reach technological requirement, this process has can prevent water hammer relative to existing device, also save cooling water amount, described catalytic liquid storage tank 1 and kettle 12 inside are provided with temperature sensor, temperature sensor is electrically connected with temperature indicator 5, by temperature sensor by the temperature survey of catalytic liquid storage tank 1 and kettle 12 inside out, in good time shows on temperature indicator 5, understands the temperature conditions of catalytic liquid storage tank 1 and kettle 12 inside in time.Described measuring pump 3 and flow control valve 4 are all electrically connected with controller 14.Described kettle 12 inwall is provided with Polypropylene Anticorrosion Coating, and Polypropylene Anticorrosion Coating can prevent the corrosion of kettle 12 inwall, extends the service life of reactor, reduces production cost.By at catalytic liquid storage tank 1 arranged outside temperature indicator 5, catalytic liquid muff 6 and zone of heating 13, allow to the catalytic liquid temperature conditions understood in time in catalytic liquid storage tank 1, and can make and adjusting timely, make catalytic liquid temperature remain at optimum state required for reaction; The catalytic liquid charging aperture 7 on catalytic liquid storage tank 1 and kettle 12 is connected by communicating pipe, and measuring pump 3 and flow control valve 4 are set on communicating pipe, can be good at joining the dosage of reaction kettle body to catalytic liquid and speed controls, ensure the quality of reacting synthesis medicament and the medicine generated;
To those skilled in the art, obvious the utility model is not limited to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present utility model or essential characteristic, can realize the utility model in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present utility model is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the utility model.Any Reference numeral in claim should be considered as the claim involved by limiting.
In addition, be to be understood that, although this description is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of description is only for clarity sake, those skilled in the art should by description integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (3)
1. one kind can realize fast reaction and the reactor of discharging, comprise catalytic liquid storage tank (1), reactor body (2) and cooling water circulation cooling system (19), it is characterized in that, described catalytic liquid storage tank (1) outside is disposed with zone of heating (13) and catalytic liquid muff (6), be provided with temperature indicator (5) and controller (14) in catalytic liquid storage tank (1) side, controller (14) is electrically connected with zone of heating (13), described reactor body (2) comprises kettle (12), kettle (12) outside is provided with water circulation layer (15), water circulation layer (15) outside is provided with kettle muff (11), kettle (12) top is provided with stirring motor (10), stirring motor (10) left side is provided with catalytic liquid charging aperture (7), catalytic liquid charging aperture (7) is communicated with by communicating pipe with catalytic liquid storage tank (1), described communicating pipe is provided with measuring pump (3) and flow control valve (4), stirring motor (10) right side is provided with material inlet (8) and top cooling water delivery outlet (16), described kettle (12) bottom is provided with discharging opening (9) and bottom coohng water output (17), kettle (12) right side is provided with temperature indicator (5) and cooling water jet (18), cooling water jet (18), top cooling water delivery outlet (16) is all communicated with water circulation layer (15) with bottom coohng water output (17), described cooling water circulation cooling system (19) top and bottom are equipped with input (21), cooling water circulation cooling system (19) side is provided with output (20), the input (21) at cooling water circulation cooling system (19) top is communicated with by water pipe (22) with bottom coohng water output (17) with top cooling water delivery outlet (16) on kettle (12) respectively with the input (21) of bottom, output (20) is connected by water pipe (22) with the cooling water jet (18) on kettle (12), valve (23) is respectively equipped with near the position of kettle (12) and cooling water circulation cooling system (19) at described water pipe (22), described catalytic liquid storage tank (1) and kettle (12) inside are provided with temperature sensor, and temperature sensor is electrically connected with temperature indicator (5).
2. according to claim 1ly a kind ofly can realize fast reaction and the reactor of discharging, it is characterized in that, described measuring pump (3) and flow control valve (4) are all electrically connected with controller (14).
3. according to claim 1ly a kind ofly can realize fast reaction and the reactor of discharging, it is characterized in that, described kettle (12) inwall is provided with Polypropylene Anticorrosion Coating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420636838.5U CN204193896U (en) | 2014-10-30 | 2014-10-30 | A kind ofly fast reaction can be realized and the reactor of discharging |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420636838.5U CN204193896U (en) | 2014-10-30 | 2014-10-30 | A kind ofly fast reaction can be realized and the reactor of discharging |
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| Publication Number | Publication Date |
|---|---|
| CN204193896U true CN204193896U (en) | 2015-03-11 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420636838.5U Expired - Fee Related CN204193896U (en) | 2014-10-30 | 2014-10-30 | A kind ofly fast reaction can be realized and the reactor of discharging |
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| Country | Link |
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| CN (1) | CN204193896U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111111575A (en) * | 2019-12-27 | 2020-05-08 | 北京英惠尔生物技术有限公司 | Method for improving efficiency of Vc ester reaction kettle and simple cold water supply system thereof |
-
2014
- 2014-10-30 CN CN201420636838.5U patent/CN204193896U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111111575A (en) * | 2019-12-27 | 2020-05-08 | 北京英惠尔生物技术有限公司 | Method for improving efficiency of Vc ester reaction kettle and simple cold water supply system thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150311 Termination date: 20151030 |
|
| EXPY | Termination of patent right or utility model |