CN204134638U - A kind of rubidium caesium extractant synthesis dedicated kettle - Google Patents
A kind of rubidium caesium extractant synthesis dedicated kettle Download PDFInfo
- Publication number
- CN204134638U CN204134638U CN201420597206.2U CN201420597206U CN204134638U CN 204134638 U CN204134638 U CN 204134638U CN 201420597206 U CN201420597206 U CN 201420597206U CN 204134638 U CN204134638 U CN 204134638U
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- kettle
- extractant
- water bath
- fixed
- turning cylinder
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Abstract
The utility model discloses a kind of rubidium caesium extractant synthesis dedicated kettle, comprise kettle and kettle cover, the inside of kettle is provided with steam heating structure, and the outside of kettle is provided with water-bath system, the middle part of kettle cover is provided with turning cylinder bearing, turning cylinder bearing is provided with the agitator extending into kettle inside.The utility model can Fast back-projection algorithm extractant, while enhancing productivity, decreases the side reaction of synthesis material in kettle, improves the degree of purity of extractant, and practical, is worthy to be popularized.
Description
Technical field
The utility model relates to a kind of rubidium caesium extractant synthesis dedicated kettle.
Background technology
At present, rubidium caesium is separated the general extracting process that adopts to carry out, and the extractant adopted is often containing gas chromatography, purity is low, if but extractant is purified will greatly reduce extractant synthesis yield through repeatedly fractionation, increase cost, and reductions effect of extracting and reduction service life of extractant are increased cost by the low extractant of purity.Therefore develop and a kind ofly can improve the synthesis reactor that combined coefficient can reduce again the rubidium caesium extractant of side reaction and become the task of top priority.
And the heating arrangement of the synthesis reactor that conventional art adopts adopts chuck heat transfer oil electric heating structure, what adopt in kettle is that yi word pattern stirs, but conventional art has following deficiency in long-term facts have proved: first, chuck heat transfer oil electric heating structure operationally, cannot accomplish that rapid heat cycle controls to the synthesis material in kettle, temperature control flexibility ratio and efficiency low, will make like this synthesis material synthesize time produce more side reaction, need repeatedly fractionation to purify after synthesis, yield is low; The second, the synthesis material that uses of rubidium caesium extractant is comparatively dense thick when synthesizing, and rapid stirring is even to adopt the stirring structure of yi word pattern to accomplish, mixing time is long, just easily causes synthesizing the overlong time that material is in side reaction, produces impurity; 3rd, traditional synthesis reactor is all disposable charging, and the excessive mixing time that also makes of charging is long, can increase the time of side reaction too, affect the purity of extractant.
Utility model content
The utility model, in order to solve the above-mentioned deficiency of prior art, proposes a kind of rubidium caesium extractant synthesis dedicated kettle.
In order to solve the problems of the technologies described above, the utility model is by the following technical solutions: a kind of rubidium caesium extractant synthesis dedicated kettle, comprise kettle and kettle cover, the side of described kettle cover is provided with charging adapter, opposite side is provided with passage, the middle part of kettle cover is provided with turning cylinder bearing, turning cylinder bearing is provided with the agitator extending into kettle inside, the upper end that correspond to this turning cylinder bearing of agitator is provided with drive motors, the mixing part of described agitator is fusiform, and the inner side of the fusellal fabric of mixing part is fixed with large-meshed net; Charging adapter is provided with constant displacement pump and valve; The bottom of kettle is provided with discharging adapter.
In one embodiment, comprise water-bath system further, water-bath system comprises water bath, circulating line, water tank and circulating pump, kettle is supported and fixed in described water bath by the support portion that external upper is arranged, discharging adapter passes described water bath, and the outside of discharging adapter is provided with brace table and is supported and fixed in water bath.
The inwall of described kettle is installed with steam pipe coil, and described steam pipe coil is fixed on inwall by U-bolt spiral, and the air inlet tube of steam pipe coil and outgoing gas connection tube all pass and be fixed on the sidewall of water bath.
Compared with prior art, the utility model has the following advantages:
1, the utility model adopts constant displacement pump to carry out charging, and the synthesis material equivalent making to join in kettle is even, and the synthesis of the small component of segmented, shortens the generated time of extractant, eliminates side reaction, improves the purity of extractant.
2, the utility model have employed fusoid agitator of band large-meshed net, when stirring, having the speed that stirs faster, shortening the reaction time, while enhancing productivity, also reduce side reaction further for thick synthesis material.
3, the utility model have employed steam-heated steam pipe coil structure, can accomplish Fast Heating to the synthesis material of kettle inside, and the water-bath system adopted can be applied in a flexible way, when needs heat, hot water is poured in water bath, but when needing to begin to cool down, while steam off heating, and inject cold water in water bath, reduce kettle internal temperature fast, accomplish rapid heat cycle, enhanced productivity, prevent the generation of side reaction.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Detailed description of the invention
Below in conjunction with drawings and Examples, utility model is described in detail.
As shown in Figure 1, the rubidium caesium extractant synthesis dedicated kettle that the utility model proposes, comprise kettle 1 and kettle cover 2, the bottom of kettle 1 is provided with discharging adapter 9, the side of kettle cover 2 is provided with charging adapter 21, opposite side is provided with passage 22, the middle part of kettle cover is provided with turning cylinder bearing 3, turning cylinder bearing 3 is provided with the agitator 4 extending into kettle inside, the upper end that correspond to this turning cylinder bearing 3 of agitator is provided with drive motors 5, drive motors 5 drives agitator to rotate, the mixing part of agitator is fusiform, and the inside of the fusellal fabric of mixing part be one hollow, hollow parts is fixed with large-meshed net 6, the aperture of large-meshed net 6 can be decided according to the actual requirements.Charging adapter 21 is provided with constant displacement pump 7 and valve 8, constant displacement pump 7 can send into the material of equivalent, and the equivalent of material is thrown in, and makes synthetic work segmented, also just indirectly improves combined coefficient.
In order to ensure the stability of temperature in kettle, a water-bath system is added in the outside of kettle, water-bath system comprises water bath 10, circulating line 11, water tank 12 and circulating pump 13, kettle 1 is supported and fixed in described water bath 10 by the support portion 14 that external upper is arranged, discharging adapter 9 passes described water bath 10, and the outside of discharging adapter 9 is provided with brace table 15 is supported and fixed in water bath 10, when connecting, circulating line 11 is arranged on the low level of water inlet in side of water bath 10, and delivery port is in a high position for water bath side.
In order to improve the operating efficiency of synthesis, in order to kettle internal temperature can be improved fast, the utility model is also in conjunction with a steam-heated system, the inwall of wherein kettle 1 is installed with steam pipe coil 16, steam pipe coil 16 is fixed on inwall by U-bolt 17 spiral, U-bolt 17 is all provided with hermetically-sealed construction at the position through kettle sidewall, prevent material from leaking outside, and the air inlet tube 18 of steam pipe coil 16 and outgoing gas connection tube 19 all pass be fixed on water bath 10 sidewall on, air inlet tube 18 and outgoing gas connection tube 19 are arranged in cyclic steam pipe-line system.
Above-described embodiment only have expressed several embodiment of the present utility model, and it describes comparatively concrete and detailed, but therefore can not be interpreted as the restriction to the utility model the scope of the claims.It should be pointed out that for the person of ordinary skill of the art, without departing from the concept of the premise utility, can also make some distortion and improvement, these all belong to protection domain of the present utility model.Therefore, the utility model patent and protection domain should be as the criterion with appended claims.
Claims (3)
1. a rubidium caesium extractant synthesis dedicated kettle, comprise kettle (1) and kettle cover (2), the side of described kettle cover (2) is provided with charging adapter (21), opposite side is provided with passage (22), the middle part of kettle cover is provided with turning cylinder bearing (3), described turning cylinder bearing (3) is provided with the agitator (4) extending into kettle inside, the upper end that correspond to this turning cylinder bearing (3) of agitator is provided with drive motors (5), it is characterized in that: the mixing part of described agitator is fusiform, and the inner side of the fusellal fabric of mixing part is fixed with large-meshed net (6); Described charging adapter (21) is provided with constant displacement pump (7) and valve (8); The bottom of described kettle (1) is provided with discharging adapter (9).
2. rubidium caesium extractant synthesis dedicated kettle as claimed in claim 1, it is characterized in that: comprise water-bath system further, described water-bath system comprises water bath (10), circulating line (11), water tank (12) and circulating pump (13), the support portion (14) that described kettle (1) is arranged by external upper is supported and fixed in described water bath (10), described discharging adapter (9) passes described water bath (10), and the outside of discharging adapter (9) is provided with brace table (15) is supported and fixed in water bath (10).
3. rubidium caesium extractant synthesis dedicated kettle as claimed in claim 2, it is characterized in that: the inwall of described kettle (1) is installed with steam pipe coil (16), described steam pipe coil (16) is fixed on inwall by U-bolt (17) spiral, and the air inlet tube (18) of steam pipe coil (16) and outgoing gas connection tube (19) all pass be fixed on water bath (10) sidewall on.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420597206.2U CN204134638U (en) | 2014-10-16 | 2014-10-16 | A kind of rubidium caesium extractant synthesis dedicated kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420597206.2U CN204134638U (en) | 2014-10-16 | 2014-10-16 | A kind of rubidium caesium extractant synthesis dedicated kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204134638U true CN204134638U (en) | 2015-02-04 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420597206.2U Expired - Fee Related CN204134638U (en) | 2014-10-16 | 2014-10-16 | A kind of rubidium caesium extractant synthesis dedicated kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204134638U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105771753A (en) * | 2016-04-23 | 2016-07-20 | 长葛市怡盛蜂业有限公司 | Honey stirring device |
| CN111650978A (en) * | 2020-06-19 | 2020-09-11 | 临沂晟泰高分子材料有限公司 | Temperature monitoring and adjusting device of synthesis reaction kettle |
-
2014
- 2014-10-16 CN CN201420597206.2U patent/CN204134638U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105771753A (en) * | 2016-04-23 | 2016-07-20 | 长葛市怡盛蜂业有限公司 | Honey stirring device |
| CN111650978A (en) * | 2020-06-19 | 2020-09-11 | 临沂晟泰高分子材料有限公司 | Temperature monitoring and adjusting device of synthesis reaction kettle |
| CN111650978B (en) * | 2020-06-19 | 2021-11-09 | 临沂晟泰高分子材料有限公司 | Temperature monitoring and adjusting device of synthesis reaction kettle |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150204 Termination date: 20151016 |
|
| EXPY | Termination of patent right or utility model |