CN204125460U - A kind of extraction chondroitin sulfate temperature-controlling reaction apparatus - Google Patents
A kind of extraction chondroitin sulfate temperature-controlling reaction apparatus Download PDFInfo
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- CN204125460U CN204125460U CN201420424235.9U CN201420424235U CN204125460U CN 204125460 U CN204125460 U CN 204125460U CN 201420424235 U CN201420424235 U CN 201420424235U CN 204125460 U CN204125460 U CN 204125460U
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Abstract
The utility model discloses a kind of extraction chondroitin sulfate temperature-controlling reaction apparatus, comprise isothermal reaction tank, described isothermal reaction tank is provided with vision slit, feed port, discharge hole and whipping appts, the tank skin of described isothermal reaction tank is provided with heating and heat-insulating device, described heating and heat-insulating device comprises thermal insulation layer and constant temperature jacket layer, described constant temperature jacket layer is connected with isothermal reaction top tank structure, described thermal insulation layer is coated on the outer wall of isothermal reaction tank, described constant temperature jacket layer internal circulation has circulating-heating medium, described heating medium is communicated with electronic thermostatic heating unit, described electronic thermostatic heating unit is connected with electronic thermostatic control device, described isothermal reaction tank inside is provided with temperature sensor, described temperature sensor is connected with electronic thermostatic control device signal.This temperature-controlling reaction apparatus, can ensure the homo(io)thermism of reacting slurry, makes temperature of reaction more accurate, effectively improves the extraction yield of chondroitin sulfate and extract quality.
Description
Technical field
The utility model relates to reaction unit technical field, especially relates to a kind of extraction chondroitin sulfate temperature-controlling reaction apparatus.
Background technology
At present, extracting topmost step in the production technique of chondroitin sulfate is exactly, pure white clean cartilage block is put into reactor, and add suitable quantity of water, add the trypsinase of 0.1 ~ 1.5% of cartilage block weight, regulate pH between 8.0 ~ 9.0, control temperature, between 45 ~ 55 DEG C, stirs 3 ~ 10 hours; In this process, the temperature of reaction unit inside will control at 45 ~ 55 DEG C.The control ratio of this temperature is more crucial, but reactor of the prior art, directly interior stirring device is driven to stir by agitator motor, temperature is non-constant, uneven, meanwhile, because reactor adopts metallic substance to make, exist and extraneous phenomenon of carrying out heat exchange, cause reactor temperature can not keep constant.
Chinese patent literature (day for announcing: on June 22nd, 2011 notification number: 102103139A) discloses a kind of constant temperature vibration reaction unit, includes thermostat and vibrating device.Thermostat comprises thermostat container shell, thermostat container upper cover, Stage microscope, stage carrier, air circulation device, temperature sensor, radiator element one and heating piece.Vibrating device comprises eccentric wheel, motor fixing plate, motor, vibration rack and firm banking.Thermostat is fixed on vibrating device by thermostat container support, drives eccentric wheel to drive whole temperature-controlling reaction apparatus to vibrate by motor.
What technique scheme solved is that the problem of the uneven instability of reaction unit internal temperature is applicable to simply small and exquisite biochip and enzyme linked immunological etc.
Utility model content
The purpose of this utility model is that the internal heat in order to solve the existence of existing extraction chondroitin sulfate reactor is uneven, heat exchange is had to affect reactor internal temperature with outside atmosphere, the problem that the extraction efficiency of chondroitin sulfate is low, and provide one can keep reaction unit internal temperature constant, effectively improve the extraction chondroitin sulfate temperature-controlling reaction apparatus of extraction yield.
The utility model realizes the technical scheme that its technical purpose adopts: a kind ofly extract chondroitin sulfate temperature-controlling reaction apparatus, comprise isothermal reaction tank, described isothermal reaction tank is provided with vision slit, feed port, discharge hole and whipping appts, the tank skin of described isothermal reaction tank is provided with heating and heat-insulating device, described heating and heat-insulating device comprises thermal insulation layer and constant temperature jacket layer, described constant temperature jacket layer is connected with isothermal reaction top tank structure, described thermal insulation layer is coated on the outer wall of isothermal reaction tank, described constant temperature jacket layer internal circulation has circulating-heating medium, described heating medium is communicated with electronic thermostatic heating unit, described electronic thermostatic heating unit is connected with electronic thermostatic control device, described isothermal reaction tank inside is provided with temperature sensor, described temperature sensor is connected with electronic thermostatic control device signal.This temperature-controlling reaction apparatus, by arranging constant temperature jacket layer and thermal insulation layer on the tank skin of isothermal reaction tank, thermostatically heating layer inside passes into the medium through heating of flowing, this heating medium is heated by electronic thermostatic heating unit, electronic thermostatic heating unit is controlled by electronic thermostatic control device, simultaneously, isothermal reaction tank inside is provided with temperature sensor, temperature sensor is connected with electronic thermostatic control device signal, when temperature sensor detects that change appears in the temperature of isothermal reaction tank inside, can by timely for signal transfer line electronic thermostatic control device, electronic thermostatic control device can adjust the Heating temperature of electronic thermostatic heating unit, realize the constant heating to the temperature of heating medium, and then ensure the homo(io)thermism of the inner slurries of isothermal reaction tank, slurry agitation is made to react more abundant, thermal insulation layer realizes the insulation to isothermal reaction tank internal temperature, heat and the external world is avoided to carry out heat exchange.This temperature-controlling reaction apparatus, can realize carrying out detection control constantly to the slurry temperature of isothermal reaction tank inside, temperature of reaction is remained between 45 ~ 55 DEG C, and temperature controlling range can be less, more accurate, effectively improve the extraction yield of chondroitin sulfate and extract quality.
As preferably, described constant temperature jacket layer is provided with medium inlet and media outlet, and described medium inlet is arranged on the top of constant temperature jacket layer, and described media outlet is arranged on the bottom of constant temperature jacket layer.Constant temperature jacket layer is arranged medium inlet and media outlet, the convenient heating medium passing into steady temperature in constant temperature jacket layer inside, and realize the circulation of medium in constant temperature jacket layer inside.
As preferably, described electronic thermostatic heating unit comprises dielectric heating container, constent temperature heater, heating medium Send out pump, heating medium output tube and heating medium input tube, and described constent temperature heater is arranged on dielectric heating internal tank with heating medium Send out pump and is connected with electronic thermostatic control device.Electronic thermostatic heating unit comprises dielectric heating container, dielectric heating internal tank is provided with constent temperature heater, constent temperature heater is by the control of electronic thermostatic control device, medium is heated, medium after heating is transported to isothermal reaction chuck layer inside by heating medium Send out pump and heats isothermal reaction tank, make the temperature of isothermal reaction tank inside control at optimum temperature range, ensure stirring reaction effect.
As preferably, described heating medium output tube and heating medium input tube outer setting have muff, and described heating medium output tube is connected with heating medium Send out pump, and described heating medium input tube is arranged on the bottom of dielectric heating container.Heating medium output tube and heating medium input tube outer setting muff are to ensure the constant of heating medium temperature, can not carry out heat exchange in working cycle with outside.
As preferably, the top of described isothermal reaction tank is also provided with safety valve and thermometer.Arranging safety valve is the reaction safety energy ensureing isothermal reaction tank, and set temperature meter is can conveniently from the temperature conditions of outside observing response tank inside.
The beneficial effects of the utility model are: this extraction chondroitin sulfate temperature-controlling reaction apparatus, the homo(io)thermism of the inner slurries of isothermal reaction tank can be ensured, slurry agitation is made to react more abundant, simultaneously, can realize carrying out detection control constantly to the slurry temperature of isothermal reaction tank inside, temperature of reaction is remained between 45 ~ 55 DEG C, and temperature controlling range can be less, more accurate, effectively improve the extraction yield of chondroitin sulfate and extract quality.
Accompanying drawing explanation
Fig. 1 is a kind of structural representation that the utility model extracts chondroitin sulfate temperature-controlling reaction apparatus;
In figure: 1, isothermal reaction tank, 2, vision slit, 3, feed port, 4, discharge hole, 5, whipping appts, 6, thermal insulation layer, 7, constant temperature jacket layer, 8, heating medium, 9, electronic thermostatic heating unit, 10, electronic thermostatic control device, 11, temperature sensor, 12, medium inlet, 13, media outlet, 14, dielectric heating container, 15, constent temperature heater, 16, heating medium Send out pump, 17, heating medium output tube, 18, heating medium input tube, 19, muff, 20, safety valve, 21, thermometer.
Embodiment
Also by reference to the accompanying drawings the technical solution of the utility model is described in further detail below by specific embodiment.
Embodiment 1:
In the embodiment shown in fig. 1, a kind of extraction chondroitin sulfate temperature-controlling reaction apparatus, comprise isothermal reaction tank 1, isothermal reaction tank 1 is provided with vision slit 2, feed port 3, discharge hole 4 and whipping appts 5, the top of isothermal reaction tank 1 is also provided with safety valve 20 and thermometer 21.
The tank skin of isothermal reaction tank 1 is provided with heating and heat-insulating device, heating and heat-insulating device comprises thermal insulation layer 6 and constant temperature jacket layer 7, constant temperature jacket layer 7 is connected with isothermal reaction tank 1 inwall, thermal insulation layer 6 is coated on the outer wall of isothermal reaction tank 1, constant temperature jacket layer 7 internal circulation has circulating-heating medium 8, heating medium 8 is communicated with electronic thermostatic heating unit 9, electronic thermostatic heating unit 9 is connected with electronic thermostatic control device 10, isothermal reaction tank 1 inside is provided with temperature sensor 11, and temperature sensor 11 is connected with electronic thermostatic control device 10 signal.
Electronic thermostatic heating unit 9 comprises dielectric heating container 14, constent temperature heater 15, heating medium Send out pump 16, heating medium output tube 17 and heating medium input tube 18, and constent temperature heater 15 and heating medium Send out pump 16 are arranged on dielectric heating container 14 inside and are connected with electronic thermostatic control device 10.
Constant temperature jacket layer 7 is provided with medium inlet 12 and media outlet 13, medium inlet 12 is arranged on the top of constant temperature jacket layer 7, and media outlet 13 is arranged on the bottom of constant temperature jacket layer 7.Heating medium output tube 17 and heating medium input tube 18 outer setting have muff 19, and heating medium output tube 17 is connected with heating medium Send out pump 16, and heating medium input tube 18 is arranged on the bottom of dielectric heating container 14.Heating medium output tube 17 is connected with medium inlet 12, and heating medium input tube 18 is connected with media outlet 13.
This extraction chondroitin sulfate temperature-controlling reaction apparatus, during use, according to the temperature of reaction requirement of the inner slurries of isothermal reaction tank, the startup control temperature value of setting electronic thermostatic control device 10, started by electronic thermostatic control device 10 and control the medium of electronic thermostatic heating unit 9 to inside and heat, and make heating medium be heated to the temperature of setting, now heating medium Send out pump 16 starts work, heating medium is input to constant temperature jacket layer 7 inside by heating medium output tube 17 and provides default temperature of reaction to temperature-controlling reaction apparatus, because the heating medium of constant temperature jacket layer inside constantly circulates, and outside has thermal insulation layer to prevent from carrying out heat exchange with the external world, therefore, this temperature-controlling reaction apparatus effectively ensure that the stirring reaction temperature of inner slurries, make reaction more abundant, extraction effect is more remarkable.Simultaneously, this temperature-controlling reaction apparatus can realize carrying out detection control constantly to the slurry temperature of isothermal reaction tank inside, temperature of reaction is remained between 45 ~ 55 DEG C, and temperature controlling range can be less, more accurate, effectively improve the extraction yield of chondroitin sulfate and extract quality.
Claims (5)
1. one kind is extracted chondroitin sulfate temperature-controlling reaction apparatus, comprise isothermal reaction tank (1), described isothermal reaction tank (1) is provided with vision slit (2), feed port (3), discharge hole (4) and whipping appts (5), it is characterized in that: the tank skin of described isothermal reaction tank (1) is provided with heating and heat-insulating device, described heating and heat-insulating device comprises thermal insulation layer (6) and constant temperature jacket layer (7), described constant temperature jacket layer (7) is connected with isothermal reaction tank (1) inwall, described thermal insulation layer (6) is coated on the outer wall of isothermal reaction tank (1), described constant temperature jacket layer (7) internal circulation has circulating-heating medium (8), described heating medium (8) is communicated with electronic thermostatic heating unit (9), described electronic thermostatic heating unit (9) is connected with electronic thermostatic control device (10), described isothermal reaction tank (1) inside is provided with temperature sensor (11), described temperature sensor (11) is connected with electronic thermostatic control device (10) signal.
2. one according to claim 1 extracts chondroitin sulfate temperature-controlling reaction apparatus, it is characterized in that: described constant temperature jacket layer (7) is provided with medium inlet (12) and media outlet (13), described medium inlet (12) is arranged on the top of constant temperature jacket layer (7), and described media outlet (13) is arranged on the bottom of constant temperature jacket layer (7).
3. one according to claim 1 extracts chondroitin sulfate temperature-controlling reaction apparatus, it is characterized in that: described electronic thermostatic heating unit (9) comprises dielectric heating container (14), constent temperature heater (15), heating medium Send out pump (16), heating medium output tube (17) and heating medium input tube (18), described constent temperature heater (15) and heating medium Send out pump (16) are arranged on dielectric heating container (14) inside and are connected with electronic thermostatic control device (10).
4. one according to claim 3 extracts chondroitin sulfate temperature-controlling reaction apparatus, it is characterized in that: described heating medium output tube (17) and heating medium input tube (18) outer setting have muff (19), described heating medium output tube (17) is connected with heating medium Send out pump (16), and described heating medium input tube (18) is arranged on the bottom of dielectric heating container (14).
5. the one according to claim 1 or 2 or 3 or 4 extracts chondroitin sulfate temperature-controlling reaction apparatus, it is characterized in that: the top of described isothermal reaction tank (1) is also provided with safety valve (20) and thermometer (21).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420424235.9U CN204125460U (en) | 2014-07-30 | 2014-07-30 | A kind of extraction chondroitin sulfate temperature-controlling reaction apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420424235.9U CN204125460U (en) | 2014-07-30 | 2014-07-30 | A kind of extraction chondroitin sulfate temperature-controlling reaction apparatus |
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| Publication Number | Publication Date |
|---|---|
| CN204125460U true CN204125460U (en) | 2015-01-28 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420424235.9U Expired - Fee Related CN204125460U (en) | 2014-07-30 | 2014-07-30 | A kind of extraction chondroitin sulfate temperature-controlling reaction apparatus |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109293793A (en) * | 2018-09-29 | 2019-02-01 | 平顶山金晶生物科技股份有限公司 | A kind of auxiliary device extracting soybean polyoses extracting solution using the acid-hatching of young eggs |
-
2014
- 2014-07-30 CN CN201420424235.9U patent/CN204125460U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109293793A (en) * | 2018-09-29 | 2019-02-01 | 平顶山金晶生物科技股份有限公司 | A kind of auxiliary device extracting soybean polyoses extracting solution using the acid-hatching of young eggs |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150128 Termination date: 20170730 |