CN204122760U - A kind of device of preparation in macroscopic quantity nano metal material - Google Patents
A kind of device of preparation in macroscopic quantity nano metal material Download PDFInfo
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- CN204122760U CN204122760U CN201420491686.4U CN201420491686U CN204122760U CN 204122760 U CN204122760 U CN 204122760U CN 201420491686 U CN201420491686 U CN 201420491686U CN 204122760 U CN204122760 U CN 204122760U
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- intermediate liquid
- stoste
- treatment system
- metal material
- nano metal
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Abstract
The utility model discloses a kind of device of preparation in macroscopic quantity nano metal material, comprise stoste treatment system, intermediate liquid treatment system and control system; Wherein stoste treatment system comprises magnetic stirring apparatus, it is arranged intermediate liquid reaction reservoir vessel, funnel and stoste store adds container, first stoste input pipe connects funnel and intermediate liquid reacts reservoir vessel, and the second stoste input pipe connects stoste storage interpolation container and intermediate liquid reacts reservoir vessel; Intermediate liquid treatment system comprises reaction vessel that intermediate liquid carrier pipe connects and stoste stores and adds container, and reaction vessel is arranged in constant water bath box; Control system comprises the first flow sensor be arranged on the first stoste input pipe, be arranged at the second quantity sensor on intermediate liquid carrier pipe, be arranged at the temperature sensor in constant water bath box, be arranged at the magnetic valve on intermediate liquid carrier pipe, guidance panel for controlling nano metal material preparation process and setting parameter, the integrated whole control circuit of controller.
Description
Technical field
The utility model belongs to field of nano material preparation, particularly a kind of device using immersion method preparation in macroscopic quantity nano metal material.
Background technology
Nano metal material integrates metallurgy, chemical industry, electronic technology, biologic medical purposes, is a kind of high-tech nano-functional material, for the preparation of electronic devices and components and antimicrobial medical apparatus, is also widely used in the field such as new forms of energy, catalysis material simultaneously.
Nano metal material is a kind of emerging functional material, has very high specific area and surface-active, and as Nano Silver, its conductance is at least higher than common silver bullion block 20 times.Therefore, nano metal material is widely used as catalyst material, antistatic material, low temperature superconducting material, thin film switch, piezo-resistance, thermistor, integrated circuit, solar cell, electromagnetic shielding, vehicle glass defrost and biology sensor material etc.Again such as, nano silver particles can enter in microbial body, interrupts the copying of RNA, and stops microbial reproduction, also can be adsorbed on microorganism wall simultaneously, affect the transmission that Institute of Micro-biology needs base substance, and final bacterial cell can break and dead.Can apply and medicine and cosmetic industry.In chemical fibre, add some performance that proper amount of nano metal can change chemical fabrics, what have will have very strong sterilizing ability.
At present, Chinese Enterprises can produce the Nano metal powder of various traditional performance substantially, but no matter from technology, kind, quality and the market share, all lags far behind advanced country in the world.Such as Nano Silver, in high-end product, the development of domestic industries has to rely on external a large amount of import to the kind of nano-silver powder, the demand of quality and quantity within quite long period.Although the market capacity of Nano metal powder is very huge, it is urgently to be resolved hurrily also to there is a lot of technique bottleneck in the research and development of preparation of industrialization particularly relevant apparatus equipment, and such as output is not high, and the particle size obtained is uneven first-class.
Utility model content
The utility model, for above-mentioned deficiency, overcomes existing yielding poorly, and the uneven first-class technological deficiency of particle size, provides a kind of device of preparation in macroscopic quantity nano metal material, namely utilize the device of water-bath oxidation-reduction method preparation in macroscopic quantity nano metal material.
For achieving the above object, the utility model is realized by following technological means:
A device for preparation in macroscopic quantity nano metal material, comprises stoste treatment system, intermediate liquid treatment system and control system; Wherein stoste treatment system comprises magnetic stirring apparatus, intermediate liquid reaction reservoir vessel, the first stoste input pipe, the second stoste input pipe, and funnel and stoste store adds container; Intermediate liquid reaction reservoir vessel is arranged on magnetic stirring apparatus, and the first stoste input pipe connects funnel and intermediate liquid reacts reservoir vessel, and the second stoste input pipe connects stoste storage interpolation container and intermediate liquid reacts reservoir vessel; Intermediate liquid treatment system comprises intermediate liquid carrier pipe, reaction vessel, constant water bath box, and intermediate liquid carrier pipe coupled reaction container and stoste store adds container, and reaction vessel is arranged in constant water bath box; Control system comprises first flow sensor, second quantity sensor, temperature sensor, magnetic valve, guidance panel and controller, first flow sensor setting is on the first stoste input pipe, and second quantity sensor is arranged on intermediate liquid carrier pipe, temperature sensor is arranged in constant water bath box, and magnetic valve is arranged on intermediate liquid carrier pipe; First flow sensor, second quantity sensor, temperature sensor and magnetic valve are connected by circuit and are integrated in controller, the integrated whole control circuit of controller; Guidance panel connection control device also controls nano metal material preparation process and setting parameter.
The device of described preparation in macroscopic quantity nano metal material, intermediate liquid treatment system can also comprise gripper shoe and swivel plate, reaction vessel quantity can arrange more than one, intermediate liquid carrier pipe can connect stoste storage interpolation container in one end, the other end connects swivel plate, gripper shoe one end is arranged on constant water bath box by rotating shaft, and the other end connects swivel plate, and gripper shoe is combined the position that intermediate liquid carrier pipe can be made to arrive more than one reaction vessel with swivel plate.
The device of above-described preparation in macroscopic quantity nano metal material, can be provided with the mechanical stirring device stirred the intermediate liquid in reaction vessel bottom constant water bath box.
The device of above-described preparation in macroscopic quantity nano metal material, controller is detachable.
The utility model provides a kind of device of preparation in macroscopic quantity nano metal material, and the stoste input system be wherein made up of stoste input pipe, flow sensor, funnel effectively can control the course of conveying of stoste, ensure that the quality of product; The intermediate liquid input system be made up of intermediate liquid carrier pipe, magnetic valve can ensure that intermediate liquid is identical at the flow of diverse location, for product quality provides guarantee, also for preparation in macroscopic quantity provides technical support; Gripper shoe is combined with swivel plate and intermediate liquid carrier pipe can be made to arrive diverse location, facilitates operation, makes device hommization more; The whole production procedures such as guidance panel can add raw material, mechanical agitation, water-bath water temperature and relevant parameter set, and can greatly enhance productivity, and reduce production cost, also can ensure product quality; Controller, can dismantle, convenient for maintaining and inspection.
The device of a kind of preparation in macroscopic quantity nano metal material that the utility model provides, rational in infrastructure, the preparation adding intermediate liquid from initial raw material to exports, arrive the preparation of end product again, Digital Control and ease of Use can be realized, thus reach production procedure automation, and it is homogeneous to produce quality, the nano metal material that output is higher.Successfully prepare uniform particle diameter with this device, the Nano Silver that output is higher at present.
Accompanying drawing explanation
Fig. 1 is the structural representation of the device of preparation in macroscopic quantity nano metal material of the present utility model;
Wherein 1 is magnetic stirring apparatus; 2 is intermediate liquid reaction reservoir vessel; 3-1 is the first stoste input pipe; 3-2 is the second stoste input pipe; 4-1 is first flow sensor; 4-2 is second quantity sensor; 5 is funnel; 6 add container for stoste stores; 7 is intermediate liquid carrier pipe; 8 is temperature sensor; 9 is magnetic valve; 10 is gripper shoe; 11 is swivel plate; 12 is reaction vessel; 13 is constant water bath box; 14 is guidance panel; 15 is controller.
detailed description of the invention:
Below in conjunction with accompanying drawing, the utility model is described in further detail.
Embodiment 1
Fig. 1 is the apparatus structure schematic diagram of a kind of preparation in macroscopic quantity nano metal material of the utility model; Comprising stoste treatment system, intermediate liquid treatment system and control system; Stoste treatment system comprises magnetic stirring apparatus 1, can be uniformly mixed formation intermediate liquid to stoste; Intermediate liquid reaction reservoir vessel 2, first stoste input pipe 3-1, the second stoste input pipe 3-2, funnel 5 and stoste store adds container 6; Intermediate liquid reaction reservoir vessel 2 is arranged on magnetic stirring apparatus 1, and the first stoste input pipe 3-1 connects funnel 5 and reacts reservoir vessel 2 with intermediate liquid, and the second stoste input pipe 3-2 connection stoste storage is added container 6 and reacted reservoir vessel 2 with intermediate liquid; Intermediate liquid treatment system comprises intermediate liquid carrier pipe 7, reaction vessel 12, constant water bath box 13, and intermediate liquid carrier pipe 7 coupled reaction container 12 and stoste store adds container 6, and reaction vessel 12 is arranged in constant water bath box 13; Control system comprises first flow sensor 4-1, second quantity sensor 4-2, temperature sensor 8, magnetic valve 9, guidance panel 14 and controller 15, and first flow sensor 4-1 is arranged on the first stoste input pipe 3-1, can control the constrained input of stoste; Second quantity sensor 4-2 is arranged on intermediate liquid carrier pipe 7, can control the constrained input of intermediate liquid; Temperature sensor 8 is arranged in constant water bath box 13, for measuring the water temperature in constant water bath box; Magnetic valve 9 is arranged on intermediate liquid carrier pipe 7, can raffinate in interrupt pipe, improves precision; First flow sensor 4-1, second quantity sensor 4-2, temperature sensor 8 and magnetic valve 9 are connected by circuit and are integrated in controller 15, the integrated whole control circuit of controller 15 and detachable, convenient for maintaining; Guidance panel 14 connection control device 15 the whole production procedure such as mechanical agitation, fluid flow, water-bath water temperature controlled in nano metal material preparation process and relevant parameter setting.
Be provided with the mechanical stirring device that can stir the intermediate liquid in reaction vessel 12 in the present embodiment bottom constant water bath box 13, stir process can be carried out to the intermediate liquid in reaction vessel; Intermediate liquid treatment system is also provided with gripper shoe 10 and swivel plate 11, and reaction vessel 12 quantity is arranged six (also can be arranged to other quantity according to specific requirement), can carry out the reaction of intermediate liquid more easily; Intermediate liquid carrier pipe 7 one end connects stoste and stores interpolation container 6, and the other end connects swivel plate 11, and stoste stores to add in container 6 and is provided with water pump; Gripper shoe 10 one end is arranged on constant water bath box 13 by rotating shaft, and the other end connects swivel plate 11, and gripper shoe 10 is combined the position that intermediate liquid carrier pipe 7 can be made to arrive differential responses container 12 with swivel plate 11.
The present embodiment Central Plains liquid treating system, intermediate liquid treatment system and control system are respectively provided with two covers, can be convenient carry out the reaction that two kinds of reactant reactions obtain a kind of product.
What the present embodiment middle controller 15 adopted is that PLC controls.Wherein, first flow sensor 4-1, being the sensor of record inlet amount, is not controlled sensor, display charging total amount.Second quantity sensor 4-2 is controlled, is to measure intermediate liquid flow, and the control of its flow stores by adjustment stoste the pump working voltage added in container 6 to realize.Guidance panel is the display of not controlled PLC part, the flow of display charging, the display of intermediate liquid speed of agitator and adjustment; And reactant liquor stirs speed display and adjustment; Separately there is water temperature display in water bath.
The device of above preparation in macroscopic quantity nano metal material is utilized to prepare the method for nano metal material as follows:
First, the stoste one in stoste storage interpolation container enters intermediate liquid with stoste two respectively by pipeline and reacts reservoir vessel, flow sensor record inlet amount.Then, mechanical agitation forming reactions liquid one and reactant liquor two are carried out to stoste, they are entered in reaction vessel by different pipelines and mix, flow sensor is wherein had to control flow, magnetic valve improves precision, ensure that intermediate liquid is identical at the flow of diverse location, gripper shoe and swivel plate make them enter the reaction vessel of diverse location.Finally, two kinds of reactant liquors are mixed by mechanical agitation, and under certain water bath condition, reaction forms end product.Guidance panel is the display of not controlled PLC part, the flow of display charging, the display of intermediate liquid speed of agitator and adjustment; And reactant liquor stirs speed display and adjustment; Separately there is water temperature display in water bath.
Utilize the nano-silver powder that the device of above-described preparation in macroscopic quantity nano metal material prepares, Nano Silver particle diameter can regulate and control in 10-50nm scope, and output reaches a kilogram rank.
To the above-mentioned explanation of the disclosed embodiments, professional and technical personnel in the field are realized or uses the utility model.To be apparent for those skilled in the art to the multiple amendment of these embodiments, General Principle as defined herein when not departing from spirit or scope of the present utility model, can realize in other embodiments.Therefore, the utility model can not be restricted to embodiment illustrated herein, but will meet the widest scope consistent with principle disclosed herein and features of novelty.
Claims (5)
1. a device for preparation in macroscopic quantity nano metal material, is characterized in that, comprises stoste treatment system, intermediate liquid treatment system and control system; Wherein stoste treatment system comprises magnetic stirring apparatus (1), intermediate liquid reaction reservoir vessel (2), the first stoste input pipe (3-1), the second stoste input pipe (3-2), and funnel (5) and stoste store adds container (6); Intermediate liquid reaction reservoir vessel (2) is arranged on magnetic stirring apparatus (1), first stoste input pipe (3-1) connects funnel (5) and reacts reservoir vessel (2) with intermediate liquid, and the second stoste input pipe (3-2) connects stoste storage interpolation container (6) and reacts reservoir vessel (2) with intermediate liquid; Intermediate liquid treatment system comprises intermediate liquid carrier pipe (7), reaction vessel (12), constant water bath box (13), intermediate liquid carrier pipe (7) coupled reaction container (12) and stoste store adds container (6), and reaction vessel (12) is arranged in constant water bath box (13); Control system comprises first flow sensor (4-1), second quantity sensor (4-2), temperature sensor (8), magnetic valve (9), guidance panel (14) and controller (15), first flow sensor (4-1) is arranged on the first stoste input pipe (3-1), and second quantity sensor (4-2) is arranged on intermediate liquid carrier pipe (7), temperature sensor (8) is arranged in constant water bath box (13), and magnetic valve (9) is arranged on intermediate liquid carrier pipe (7); First flow sensor (4-1), second quantity sensor (4-2), temperature sensor (8) and magnetic valve (9) are connected by circuit and are integrated in controller (15), the integrated whole control circuit of controller (15); Guidance panel (14) connection control device (15) also controls nano metal material preparation process and setting parameter.
2. the device of preparation in macroscopic quantity nano metal material according to claim 1, is characterized in that, stoste treatment system, intermediate liquid treatment system and set-up of control system a set of more than.
3. the device of preparation in macroscopic quantity nano metal material according to claim 1, it is characterized in that, intermediate liquid treatment system also comprises gripper shoe (10) and swivel plate (11), reaction vessel (12) quantity arranges more than one, intermediate liquid carrier pipe (7) one end connects stoste and stores interpolation container (6), the other end connects swivel plate (11), gripper shoe (10) one end is arranged on constant water bath box (13) by rotating shaft, the other end connects swivel plate (11), gripper shoe (10) and swivel plate (11) combine the position that intermediate liquid carrier pipe (7) can be made to arrive more than one reaction vessel (12).
4. the device of the preparation in macroscopic quantity nano metal material according to claim 1 or 2 or 3, is characterized in that, constant water bath box (13) bottom is provided with mechanical stirring device.
5. the device of the preparation in macroscopic quantity nano metal material according to claim 1 or 2 or 3, is characterized in that, controller (15) is detachable.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420491686.4U CN204122760U (en) | 2014-08-29 | 2014-08-29 | A kind of device of preparation in macroscopic quantity nano metal material |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420491686.4U CN204122760U (en) | 2014-08-29 | 2014-08-29 | A kind of device of preparation in macroscopic quantity nano metal material |
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| CN204122760U true CN204122760U (en) | 2015-01-28 |
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| CN201420491686.4U Expired - Fee Related CN204122760U (en) | 2014-08-29 | 2014-08-29 | A kind of device of preparation in macroscopic quantity nano metal material |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104227011A (en) * | 2014-08-29 | 2014-12-24 | 南京邮电大学 | Device for preparing nano-metallic material in macroscopic amount and preparation method for nano-metallic material |
-
2014
- 2014-08-29 CN CN201420491686.4U patent/CN204122760U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104227011A (en) * | 2014-08-29 | 2014-12-24 | 南京邮电大学 | Device for preparing nano-metallic material in macroscopic amount and preparation method for nano-metallic material |
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Legal Events
| Date | Code | Title | Description |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Jiangsu Nanyou IOT Technology Park Ltd. Assignor: Nanjing Post & Telecommunication Univ. Contract record no.: 2016320000209 Denomination of utility model: Device for preparing nano-metallic material in macroscopic amount and preparation method for nano-metallic material Granted publication date: 20150128 License type: Common License Record date: 20161111 |
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| LICC | Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model | ||
| EC01 | Cancellation of recordation of patent licensing contract |
Assignee: Jiangsu Nanyou IOT Technology Park Ltd. Assignor: Nanjing Post & Telecommunication Univ. Contract record no.: 2016320000209 Date of cancellation: 20180116 |
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| EC01 | Cancellation of recordation of patent licensing contract | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150128 Termination date: 20170829 |
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| CF01 | Termination of patent right due to non-payment of annual fee |