CN204093081U - A kind of powdered soy bean phosphatide purification by liquid extraction device - Google Patents
A kind of powdered soy bean phosphatide purification by liquid extraction device Download PDFInfo
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- CN204093081U CN204093081U CN201420561312.5U CN201420561312U CN204093081U CN 204093081 U CN204093081 U CN 204093081U CN 201420561312 U CN201420561312 U CN 201420561312U CN 204093081 U CN204093081 U CN 204093081U
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Abstract
The utility model discloses a kind of powdered soy bean phosphatide purification by liquid extraction device, comprise basal plane, operating desk, weigh-bridge, high shear extraction kettle, measuring tank, solvent pump, centrifuge, extraction liquid pump, sedimentation frame, settling vat, expansion chamber, fancy cutting head, electric cabinet; Described extraction section is vertically arranged with basal plane, operating desk, weigh-bridge; Described basal plane is provided with solvent pump, centrifuge, extraction liquid pump; Described operating desk is provided with high shear extraction kettle and weigh-bridge, described weigh-bridge is set side by side with two measuring tanks; Described weigh-bridge support column is fixedly installed electric cabinet, is provided with the sedimentation frame that multiple lamination is placed in described expansion chamber, described basal plane, operating desk is provided with antistatic backing, described operating desk and weigh-bridge are provided with guardrail and staircase; This novel extraction purifying plant adopts high shear still, and configures sedimentation frame and settling vat, improves content of phospholipid and yield, promotes low temperature settling efficiency, increases sedimentation solid-liquid separation effect.
Description
Technical field
The utility model relates to a kind of soybean lecithin production technology apparatus field, particularly a kind of powdered soy bean phosphatide purification by liquid extraction device.
Background technology
Along with the raising of people's living standard, the quickening of rhythm of life and living-pattern preservation, diet structure not science brings serious threat to health of people, causes the growth year by year of the diseases such as cardiovascular disease, diabetes, tumour, cerebrovascular disease, senile anemia.Therefore, in order to improve the general level of the health of people, food scientific research worker constantly develops the demand that types of functionality health food meets health of people.In recent years along with the development of food science and technology, some discarded objects that the past produces in conventional edible vegetable oil and fat processing or byproduct are developed many novelty teabag gradually.Be be rich in soybean lecithin in the residue after soybean oil produced by raw material with soybean.Soybean lecithin is the essence substance extracted from soybean, also be one of lipid component of human body needs, there is much important biological function and various health care functions: delay senility, the blood fat that effective reduction is too high and cholesterol, brain tonic and intelligence development, strengthens liver cell metabolism, promotes fat acid decomposition, protection liver, the generation of the illnesss such as prevention fatty liver; Become the new lover in health food gradually, be subject to the favor of consumer in world wide, output and consumption figure present sustainable growth, define the industry that of being different from edible vegetable oil and fat is relatively independent and huge.
Phosphatide is the general name of the phosphorous lipoid of a class, lecithin (phosphatid ylcholine, be called for short PC) be that wherein there is most bioactive a kind of phosphatide, lecithin can extract from soybean fat and yolk and yolk powder, is called soybean lecithin and egg yolk lecithin; Phosphatide is the Surface Active Substance of both sexes, and have the effects such as emulsification, dispersion, wetting, the demoulding, separation, refining natural phospholipid can be used as the auxiliary material preparing various pharmaceutical preparation, and its phosphatidylcholine content is generally more than 45%.Powdered soy bean phosphatide after degreasing, its phosphatidylcholine content is about 20%, need to carry out purifying further, general employing solvent extraction is purified, and this method has that production capacity is large, the cycle is short, be convenient to attended operation, solvent price is relatively cheap, nontoxic, be convenient to the advantages such as recycled solvent.
The shortcoming and defect part of prior art is: agitator tank stirs extraction powdered soy bean phosphatide, when purification by liquid extraction, and powdered soy bean phosphatide meeting conglomeration, cannot disperse in a solvent completely, therefore its extraction yield is low, and major product high-purity soybean phosphatide yield is low, improves phosphatid ylcholine yield also low; The slow inferior separating effect of sedimentation separation process medium velocity.
Utility model content
For solving the problems of the technologies described above, the utility model provides a kind of powdered soy bean phosphatide purification by liquid extraction device, for deficiency of the prior art, adopt high shear extraction kettle and fancy cutting head, and configure low temperature expansion chamber, sedimentation frame and settling vat, improve phosphatidylcholine content in phospholipid prod, improve powdered soy bean phosphatide dispersity in a solvent when solvent extraction is purified, improve the yield of phosphatid ylcholine and high-purity soybean phosphatide; Promote low temperature settling efficiency, shorten the sedimentation time, increase sedimentation solid-liquid separation effect.
For achieving the above object, the technical solution of the utility model is as follows: a kind of powdered soy bean phosphatide purification by liquid extraction device, comprise basal plane, operating desk, weigh-bridge, high shear extraction kettle, measuring tank, solvent pump, centrifuge, extraction liquid pump, valve, sedimentation frame, settling vat, expansion chamber, refrigeration machine, hermatic door, driving, staircase, process pipe, cooling water pipe, steam pipe, tail gas recycle pipe, fancy cutting head, electric cabinet, it is characterized in that:
Described powdered soy bean phosphatide purification by liquid extraction device lateral main shaft is furnished with and extracts section and expansion chamber, be provided with guide rail between described extraction section and expansion chamber, described guide rail be provided with sedimentation frame, described sedimentation frame is equipped with multiple settling vat; Described extraction section is longitudinally furnished with three layers, is basal plane, operating desk, weigh-bridge respectively; Described basal plane is provided with solvent pump, centrifuge, extraction liquid pump; Described operating desk is the metal framework Welding Structure of two-layer platform, it is fixedly installed high shear extraction kettle, described operating desk is welded and fixed and is provided with weigh-bridge, described weigh-bridge is spirally connected and is fixedly installed two measuring tanks, described two measuring tanks are set up in parallel; Described weigh-bridge support column is fixedly installed electric cabinet, be provided with multiple sedimentation frame in described expansion chamber, described sedimentation frame lamination is placed, and described top of settling chamber is provided with driving, be provided with heat-insulation layer in described expansion chamber body of wall, described expansion chamber is provided with hermatic door; Described expansion chamber arranged outside has refrigeration machine, and described refrigeration machine is communicated with described expansion chamber by refrigeration window; Described electric cabinet is explosion-proof electric apparatus control box, and described electric cabinet is connected with solvent pump, measuring tank, fire-proof motor, valve, centrifuge, extraction liquid pump, thermometer, Pressure gauge electric signal; Described basal plane, operating desk are provided with antistatic backing, described operating desk and weigh-bridge are provided with guardrail and staircase.
Between described solvent pump and measuring tank, between described measuring tank and high shear extraction kettle, between described high shear extraction kettle and extraction liquid pump, be interconnected by process pipe and valve between described high shear extraction kettle and centrifuge.
Described high shear extraction kettle is provided with fire-proof motor, described high shear extraction kettle inside is provided with multiple fancy cutting head, described high shear extraction kettle is provided with sandwich, described interlayer is provided with cooling water pipe and steam pipe, described cooling water pipe and steam pipe and cooling water system vapour system of unifying is communicated with, in order to regulate the temperature extracting mixture in still; Described high shear extraction kettle is provided with thermometer and Pressure gauge, in order to monitor the pressure and temperature in high shear extraction kettle.
Described high shear extraction kettle and measuring tank are provided with tail gas recycle pipe, and described tail gas recycle pipe is communicated with tail gas recycling and treating device, reduces tail gas in tank and assembles generation pressure, avoid tail gas to discharge on the spot and produce environmental pollution and potential safety hazard.
Described fancy cutting head is provided with multiple shearing sheet, and described shearing sheet distributes along described cutting head uniform plane.
Described fancy cutting head is provided with 2-6 layers, and described fancy cutting head is coaxially fixedly connected with, and shears sheet and be crisscross arranged between described fancy cutting head.
Described settling vat is the cylinder of plastic material, and be taper bottom it, described bottom is provided with the drainage conduit of inclination, described drainage conduit is provided with blow-off valve, and described drainage conduit is assembled towards described settling vat side surface direction; Described sedimentation frame is provided with multiple settling vat.
Described high shear extraction kettle is provided with extraction solution discharging opening, in order to the extract containing phosphatide on upper strata after extraction extraction, sedimentation.
Described high shear extraction kettle chuck is provided with Pressure gauge, extracts the pressure in still tank body chuck in order to monitoring.
Described solvent pump and extraction liquid pump are food-grade sanitary pump, before being arranged at described measuring tank and after high shear extraction kettle, described measuring tank is stainless steel measuring tank, be arranged on described weigh-bridge, solvent, higher than high shear extraction kettle, is quantitatively joined in described high shear extraction kettle by technological requirement by measuring tank by horizontal level.
Utilize the principle of the different solubility in a solvent of each phosphatide component in powdered soy bean phosphatide, by the effect of high shear extraction kettle dispersion and emulsion, under rapid refinement, the effect of high speed dispersion power, make powdered soy bean phosphatide be cut into fine particle is evenly dispersed in solvent, and then the easy melt into part soy phosphatidylcholine in powdered soy bean phosphatide is farthest extracted in solvent, obtain the extraction solution of higher phosphorous phosphatidylcholine content, extraction solution obtains the phospholipid prod of higher degree after treatment, or as being further purified the stoste of technique; Insoluble composition then by sedimentation and centrifugation out, and then reaches the object of separating-purifying soy phosphatidylcholine.
The utility model has that production capacity is large, the cycle is short, be convenient to attended operation, solvent price is relatively cheap, nontoxic, be convenient to the advantages such as recycled solvent.
Pass through technique scheme, the beneficial effect of technical solutions of the utility model is: adopt high shear extraction kettle and fancy cutting head, and configure sedimentation frame and settling vat, peptizaiton is sheared by the high-shear emulsifying extracting still, improve powdered soy bean phosphatide dispersity in a solvent, ease of solubility composition in powdered soy bean phosphatide is farthest dissolved in solvent, improves content and the yield of ease of solubility composition phosphatid ylcholine, also improve the yield of high purity phosphorus fat prod; By the method for natural subsidence, quickly and easily most phospholipid solution is separated with insoluble matter, reduces equipment cost, substantially increase operating efficiency; Promote low temperature settling efficiency, shorten the sedimentation time, increase sedimentation solid-liquid separation effect.
Accompanying drawing explanation
In order to be illustrated more clearly in the utility model embodiment or technical scheme of the prior art, be briefly described to the accompanying drawing used required in embodiment or description of the prior art below, apparently, accompanying drawing in the following describes is only embodiments more of the present utility model, for those of ordinary skill in the art, under the prerequisite not paying creative work, other accompanying drawing can also be obtained according to these accompanying drawings.
Fig. 1 is a kind of powdered soy bean phosphatide purification by liquid extraction device schematic diagram disclosed in the utility model embodiment.
Numeral and the corresponding component title represented by letter in figure:
1. basal plane 2. operating desk 3. weigh-bridge 4. high shear extraction kettle
5. measuring tank 6. solvent pump 7. centrifuge 8. extracts liquid pump
9. valve 10. sedimentation frame 11. settling vat 12. expansion chamber
13. refrigeration machine 14. hermatic doors 15. are driven a vehicle 16. staircases
17. process pipe 18. cooling water pipe 19. steam pipe 20. tail gas recycle pipes
21. fancy cutting head 22. electric cabinets
Detailed description of the invention
Below in conjunction with the accompanying drawing in the utility model embodiment, be clearly and completely described the technical scheme in the utility model embodiment, obviously, described embodiment is only the utility model part embodiment, instead of whole embodiments.Based on the embodiment in the utility model, those of ordinary skill in the art are not making the every other embodiment obtained under creative work prerequisite, all belong to the scope of the utility model protection.
According to Fig. 1, the utility model provides a kind of powdered soy bean phosphatide purification by liquid extraction device, comprises basal plane 1, operating desk 2, weigh-bridge 3, high shear extraction kettle 4, measuring tank 5, solvent pump 6, centrifuge 7, extraction liquid pump 8, valve 9, sedimentation frame 10, settling vat 11, expansion chamber 12, refrigeration machine 13, hermatic door 14, driving 15, staircase 16, process pipe 17, cooling water pipe 18, steam pipe 19, tail gas recycle pipe 20, fancy cutting head 21, electric cabinet 22.
Described powdered soy bean phosphatide purification by liquid extraction device lateral main shaft is furnished with and extracts section and expansion chamber 12, be provided with guide rail between described extraction section and expansion chamber 12, described guide rail be provided with sedimentation frame 10, described sedimentation frame 10 is equipped with four settling vats 11; Described extraction section is longitudinally furnished with three layers, is basal plane 1, operating desk 2, weigh-bridge 3 respectively; Described basal plane 1 is provided with solvent pump 6, centrifuge 7, extraction liquid pump 8; Described operating desk 2 is the metal framework Welding Structure of two-layer platform, it is fixedly installed high shear extraction kettle 4, described operating desk 2 is welded and fixed and is provided with weigh-bridge 3, described weigh-bridge 3 is spirally connected is fixedly installed two measuring tanks 5, and described two measuring tanks 5 are set up in parallel; Described weigh-bridge 3 support column is fixedly installed electric cabinet 22, multiple sedimentation frame 10 is provided with in described expansion chamber 12, described sedimentation frame 10 lamination is placed, described expansion chamber 12 top is provided with driving 15, be provided with heat-insulation layer in described expansion chamber 12 body of wall, described expansion chamber 12 is provided with hermatic door 14; Described expansion chamber 12 arranged outside has refrigeration machine 13, and described refrigeration machine 13 is communicated with described expansion chamber 12 by refrigeration window; Described electric cabinet 22 is explosion-proof electric apparatus control box, described electric cabinet 22 and solvent pump 6, measuring tank 5, fire-proof motor, valve 9, centrifuge 7, extract liquid pump 8, thermometer, Pressure gauge electric signal be connected; Described basal plane 1, operating desk 2 are provided with antistatic backing, described operating desk 2 and weigh-bridge 3 are provided with guardrail and staircase.
Between described solvent pump 6 and measuring tank 5, between described measuring tank 5 and high shear extraction kettle 4, between described high shear extraction kettle 4 and extraction liquid pump 8, be interconnected by process pipe 17 and valve 9 between described high shear extraction kettle 4 and centrifuge 7.
Described high shear extraction kettle 4 is provided with fire-proof motor, described high shear extraction kettle 4 inside is provided with multiple fancy cutting head, described high shear extraction kettle 4 is provided with sandwich, described interlayer is provided with cooling water pipe 18 and steam pipe 19, described cooling water pipe 18 and steam pipe 19 and cooling water system vapour system of unifying is communicated with, in order to regulate the temperature of mixture in high shear extraction kettle 4; Described high shear extraction kettle 4 is provided with thermometer and Pressure gauge, in order to monitor the pressure and temperature in high shear extraction kettle 4.
Described high shear extraction kettle 4 and measuring tank 5 are provided with tail gas recycle pipe 20, and described tail gas recycle pipe 20 is communicated with tail gas recycling and treating device, reduces tail gas in tank and assembles generation pressure, avoid tail gas to discharge on the spot and produce environmental pollution and potential safety hazard.
Described fancy cutting head is provided with multiple shearing sheet, and described shearing sheet distributes along described cutting head uniform plane.
Described fancy cutting head is provided with 4 layers, and described fancy cutting head is coaxially fixedly connected with, and shears sheet and be crisscross arranged between described fancy cutting head.
Described settling vat 11 is the cylinder of plastic material, and be taper bottom it, described bottom is provided with the drainage conduit of inclination, described drainage conduit is provided with blow-off valve, and described drainage conduit is assembled towards described settling vat side surface direction; Described sedimentation frame 10 is provided with 4 settling vats.
Described high shear extraction kettle 4 is provided with extraction solution discharging opening, in order to the extract containing phosphatide on upper strata after extraction extraction, sedimentation.
Described high shear extraction kettle 4 chuck is provided with Pressure gauge, extracts the pressure in still tank body chuck in order to monitoring.
Described solvent pump 6 and extraction liquid pump 8 are food-grade sanitary pump, before being arranged at described measuring tank 5 and after high shear extraction kettle 4, described measuring tank 5 is stainless steel measuring tank, be arranged on described weigh-bridge 3, solvent, higher than high shear extraction kettle 4, is quantitatively joined in described high shear extraction kettle 4 by technological requirement by measuring tank 5 by horizontal level.
Concrete operation step of the present utility model is: with solvent pump 6 by solvent suction measuring tank 5, adding a certain amount of solvent by technological requirement enters in high shear extraction kettle 4, open fire-proof motor, drive is coaxially arranged with fancy cutting head, unlatching steam valve or cooling water make temperature in high shear extraction kettle 4 remain on room temperature, then drop into the powdered soy bean phosphatide of predetermined weight in high shear extraction kettle 4, shear extraction 60 minutes; After shearing extraction terminates, close fire-proof motor, stop high-shear emulsifying, natural sedimentation 30-60 minute; After the phospholipid solution clarification on the upper strata in high shear extraction kettle 4, supernatant solution is evacuated in the settling vat 11 in sedimentation frame 10 by extraction liquid pump 8, and by guide rail, described sedimentation frame 10 is transported in described expansion chamber 12, by described driving 15, described sedimentation frame 10 lamination is placed, low temperature sedimentation in described expansion chamber 12, after sedimentation terminates, by the drainage conduit of described settling vat 11, precipitum and supernatant are separated; Precipitation in described high shear extraction kettle 4 enters described centrifuge 7 by bottom discharge mouth and carries out centrifugal filtration, the supernatant merging treatment of centrifugal clear liquid out and extraction; Phosphatide accessory substance is obtained after the further drying of centrifugal filtration gained solids; This accessory substance can be used for food service industry or further after process for pharmaceuticals industry.
By above-mentioned specific embodiment, the beneficial effects of the utility model are: adopt high shear extraction kettle and fancy cutting head, and configure sedimentation frame and settling vat, peptizaiton is sheared by the high-shear emulsifying extracting still, improve powdered soy bean phosphatide dispersity in a solvent, ease of solubility composition in powdered soy bean phosphatide is farthest dissolved in solvent, improves content and the yield of ease of solubility composition phosphatid ylcholine, also improve the yield of high purity phosphorus fat prod; By the method for natural subsidence, quickly and easily most phospholipid solution is separated with insoluble matter, reduces equipment cost, substantially increase operating efficiency; Promote low temperature settling efficiency, shorten the sedimentation time, increase sedimentation solid-liquid separation effect.
To the above-mentioned explanation of the disclosed embodiments, professional and technical personnel in the field are realized or uses the utility model.To be apparent for those skilled in the art to the multiple amendment of these embodiments, General Principle as defined herein when not departing from spirit or scope of the present utility model, can realize in other embodiments.Therefore, the utility model can not be restricted to these embodiments shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.
Claims (6)
1. a powdered soy bean phosphatide purification by liquid extraction device, it is characterized in that, comprise basal plane, operating desk, weigh-bridge, high shear extraction kettle, measuring tank, solvent pump, centrifuge, extraction liquid pump, valve, sedimentation frame, settling vat, expansion chamber, refrigeration machine, hermatic door, driving, staircase, process pipe, cooling water pipe, steam pipe, tail gas recycle pipe, fancy cutting head, electric cabinet; Described powdered soy bean phosphatide purification by liquid extraction device lateral main shaft is furnished with and extracts section and expansion chamber, be provided with guide rail between described extraction section and expansion chamber, described guide rail be provided with sedimentation frame, described sedimentation frame is equipped with multiple settling vat; Described extraction section is longitudinally furnished with three layers, is basal plane, operating desk, weigh-bridge respectively; Described basal plane is provided with solvent pump, centrifuge, extraction liquid pump; Described operating desk is the metal framework Welding Structure of two-layer platform, it is fixedly installed high shear extraction kettle, described operating desk is welded and fixed and is provided with weigh-bridge, described weigh-bridge is spirally connected and is fixedly installed two measuring tanks, described two measuring tanks are set up in parallel; Described weigh-bridge support column is fixedly installed electric cabinet, be provided with multiple sedimentation frame in described expansion chamber, described sedimentation frame lamination is placed, and described top of settling chamber is provided with driving, be provided with heat-insulation layer in described expansion chamber body of wall, described expansion chamber is provided with hermatic door; Described expansion chamber arranged outside has refrigeration machine, and described refrigeration machine is communicated with described expansion chamber by refrigeration window; Described electric cabinet is explosion-proof electric apparatus control box, and described electric cabinet is connected with solvent pump, measuring tank, fire-proof motor, valve, centrifuge, extraction liquid pump, thermometer, Pressure gauge electric signal; Described basal plane, operating desk are provided with antistatic backing, described operating desk and weigh-bridge are provided with guardrail and staircase.
2. a kind of powdered soy bean phosphatide purification by liquid extraction device according to claim 1, it is characterized in that, between described solvent pump and measuring tank, between described measuring tank and high shear extraction kettle, between described high shear extraction kettle and extraction liquid pump, be interconnected by process pipe and valve between described high shear extraction kettle and centrifuge.
3. a kind of powdered soy bean phosphatide purification by liquid extraction device according to claim 1, it is characterized in that, described high shear extraction kettle is provided with fire-proof motor, described high shear extraction kettle inside is provided with multiple fancy cutting head, described high shear extraction kettle is provided with sandwich, described interlayer is provided with cooling water pipe and steam pipe, described cooling water pipe and steam pipe and cooling water system vapour system of unifying is communicated with, and described high shear extraction kettle is provided with thermometer and Pressure gauge.
4. a kind of powdered soy bean phosphatide purification by liquid extraction device according to claim 1, is characterized in that, described high shear extraction kettle and measuring tank are provided with tail gas recycle pipe, and described tail gas recycle pipe is communicated with tail gas recycling and treating device.
5. a kind of powdered soy bean phosphatide purification by liquid extraction device according to claim 3, is characterized in that, described fancy cutting head is provided with multiple shearing sheet, and described shearing sheet distributes along described cutting head uniform plane; Described fancy cutting head is provided with 2-6 layers, and described fancy cutting head is coaxially fixedly connected with, and shears sheet and be crisscross arranged between described fancy cutting head.
6. a kind of powdered soy bean phosphatide purification by liquid extraction device according to claim 1, it is characterized in that, described settling vat is the cylinder of plastic material, it is taper bottom it, described bottom is provided with the drainage conduit of inclination, described drainage conduit is provided with blow-off valve, and described drainage conduit is assembled towards described settling vat side surface direction, and described sedimentation frame is provided with multiple settling vat.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420561312.5U CN204093081U (en) | 2014-09-26 | 2014-09-26 | A kind of powdered soy bean phosphatide purification by liquid extraction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420561312.5U CN204093081U (en) | 2014-09-26 | 2014-09-26 | A kind of powdered soy bean phosphatide purification by liquid extraction device |
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| Publication Number | Publication Date |
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| CN204093081U true CN204093081U (en) | 2015-01-14 |
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ID=52261552
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|---|---|---|---|
| CN201420561312.5U Expired - Fee Related CN204093081U (en) | 2014-09-26 | 2014-09-26 | A kind of powdered soy bean phosphatide purification by liquid extraction device |
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|---|---|
| CN (1) | CN204093081U (en) |
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2014
- 2014-09-26 CN CN201420561312.5U patent/CN204093081U/en not_active Expired - Fee Related
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| C56 | Change in the name or address of the patentee |
Owner name: JIANGSU MANSHI BIO-TECHNOLOGY CO., LTD. Free format text: FORMER NAME: JIANGSU MANSHI BIO-TECHNOLOGY LTD. |
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| CP03 | Change of name, title or address |
Address after: Kunshan City Qiandeng Town Suzhou city Jiangsu province 215341 Zhiwei branch No. 28 Jiangsu man's biological Polytron Technologies Inc Patentee after: JIANGSU MANSHI BIOLOGICAL TECHNOLOGIES CO.,LTD. Address before: Kunshan City Qiandeng Town Suzhou city Jiangsu province 215341 Zhiwei branch No. 28 Jiangsu man's Biological Technology Co. Ltd. Patentee before: JIANGSU MANSHI BIOTECHNOLOGY Co.,Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150114 Termination date: 20210926 |
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| CF01 | Termination of patent right due to non-payment of annual fee |