CN204017434U - A kind of Supercritical Fluid Extraction Enhanced by Ultrasonic device - Google Patents

A kind of Supercritical Fluid Extraction Enhanced by Ultrasonic device Download PDF

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Publication number
CN204017434U
CN204017434U CN201420442434.2U CN201420442434U CN204017434U CN 204017434 U CN204017434 U CN 204017434U CN 201420442434 U CN201420442434 U CN 201420442434U CN 204017434 U CN204017434 U CN 204017434U
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CN
China
Prior art keywords
extractor
supercritical fluid
supercritical
ultrasonic transducer
lid
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Expired - Fee Related
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CN201420442434.2U
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Chinese (zh)
Inventor
吴浩
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Changzhou Institute for Advanced Materials Beijing University of Chemical Technology
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Changzhou Institute for Advanced Materials Beijing University of Chemical Technology
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Priority to CN201420442434.2U priority Critical patent/CN204017434U/en
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Publication of CN204017434U publication Critical patent/CN204017434U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model relates to a kind of ultrasound-enhanced supercritical extractor, comprise supercritical fluid outlet, extractor lid, ultrasonic transducer, supercritical fluid entrance, supersonic generator and extractor cylindrical shell, extractor lid is positioned at extractor top, extractor lid and extractor cylindrical shell match and seal, supercritical fluid outlet is positioned at extractor and covers, supercritical fluid entrance is positioned at bottom extractor, ultrasonic transducer is positioned at the middle part of extractor cylindrical shell, ultrasonic transducer is connected with supersonic generator electronics, and supersonic generator promotes ultrasonic transducer work.Ultrasound-enhanced supercritical extractor veneer power output is large, and power adjustable is safe and reliable, and conveniently easily control, the extraction yield of target product is high.

Description

A kind of Supercritical Fluid Extraction Enhanced by Ultrasonic device
Technical field
The invention belongs to separation equipment, especially a kind of supercritical extract device.
Background technology
Supercritical liquid extraction technique is the novel extraction isolation technics just grown up nearly decades.Supercritical fluid refers to its temperature and pressure all higher than the fluid of critical-temperature and critical pressure, and it has excellent solvability.Supercritical liquid extraction technique, as a kind of new extraction and separation technology, has its superior part in the removing etc. of the recovery of high added value, thermal sensitivity, difficult separate substance and trace impurity.But extracting pressure is high, extraction time is long because supercritical liquid extraction technique also exists, and particularly to the extraction of some solid materials, extraction efficiency is lower, need circulation more repeatedly, thus limit the application of its large-scale industrialization.
For the problems referred to above of supercritical liquid extraction technique, the present invention devises ultrasonic and overcritical GC-MS, uses intensified by ultrasonic wave Supercritical Extraction Process, and veneer power output is large, and power adjustable is safe and reliable, and conveniently easily control, the extraction yield of target product is high.
Summary of the invention
The invention provides a kind of ultrasound-enhanced supercritical extractor, comprise supercritical fluid outlet, extractor lid, ultrasonic transducer, supercritical fluid entrance, supersonic generator, extractor cylindrical shell, extractor lid is positioned at extractor top, extractor lid and extractor cylindrical shell match and seal, supercritical fluid outlet is positioned at extractor and covers, supercritical fluid entrance is positioned at bottom extractor, ultrasonic transducer is positioned at the middle part of extractor cylindrical shell, ultrasonic transducer is connected with supersonic generator electronics, and supersonic generator promotes ultrasonic transducer work.
Extractor lid adopts with extractor cylindrical shell and is threaded, and seals with O-ring seals.
Supercritical fluid entrance and supercritical fluid outlet adopt resin seal structure to seal.
Accompanying drawing explanation
Fig. 1 is ultrasound-enhanced supercritical extractor schematic diagram of the present invention.
Detailed description of the invention
Below in conjunction with accompanying drawing, the present invention is further illustrated.
See Fig. 1, a kind of ultrasound-enhanced supercritical extractor 1, comprise supercritical fluid outlet 2, extractor lid 3, ultrasonic transducer 4, supercritical fluid entrance 5, supersonic generator 6, extractor cylindrical shell 7, extractor lid 3 is positioned at extractor 1 top, extractor lid 3 and extractor cylindrical shell 7 match and seal, supercritical fluid outlet 2 is positioned on extractor lid 3, supercritical fluid entrance 5 is positioned at bottom extractor 1, ultrasonic transducer 4 is positioned at the middle part of extractor cylindrical shell 7, ultrasonic transducer 4 is connected with supersonic generator 6 electronics, supersonic generator 6 promotes ultrasonic transducer 4 and works.
Extractor lid 3 adopts with extractor cylindrical shell 7 and is threaded, and seals with O-ring seals.
Supercritical fluid entrance 5 and supercritical fluid outlet 2 adopt resin seal structure to seal.
Ultrasound-enhanced supercritical extractor of the present invention is applicable to the extraction of multiple natural material, as extracted volatile oil, essential oil from Chinese herbal medicine, to alkaloidal extraction, the separation of aliphatic acid, flavone compound, quinone and derivative thereof, sugar and glycoside thereof etc. can also be applied to.Ultrasound-enhanced supercritical extractor veneer power output of the present invention is large, and power adjustable is safe and reliable, and conveniently easily control, the extraction yield of target product is high, has stronger effect.

Claims (3)

1. a ultrasound-enhanced supercritical extractor, it is characterized in that, extractor (1) comprises supercritical fluid outlet (2), extractor lid (3), ultrasonic transducer (4), supercritical fluid entrance (5), supersonic generator (6), extractor cylindrical shell (7), extractor lid (3) is positioned at extractor (1) top, extractor lid (3) and extractor cylindrical shell (7) match and seal, supercritical fluid outlet (2) is positioned on extractor lid (3), supercritical fluid entrance (5) is positioned at extractor (1) bottom, ultrasonic transducer (4) is positioned at the middle part of extractor cylindrical shell (7), ultrasonic transducer (4) is connected with supersonic generator (6) electronics, supersonic generator (6) promotes ultrasonic transducer (4) work.
2. ultrasound-enhanced supercritical extractor according to claim 1, is characterized in that, described extractor lid (3) adopts with described extractor cylindrical shell (7) and is threaded, and seals with O-ring seals.
3. ultrasound-enhanced supercritical extractor according to claim 1, is characterized in that, described supercritical fluid entrance (5) and described supercritical fluid outlet (2) adopt resin seal structure to seal.
CN201420442434.2U 2014-08-06 2014-08-06 A kind of Supercritical Fluid Extraction Enhanced by Ultrasonic device Expired - Fee Related CN204017434U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420442434.2U CN204017434U (en) 2014-08-06 2014-08-06 A kind of Supercritical Fluid Extraction Enhanced by Ultrasonic device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420442434.2U CN204017434U (en) 2014-08-06 2014-08-06 A kind of Supercritical Fluid Extraction Enhanced by Ultrasonic device

Publications (1)

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CN204017434U true CN204017434U (en) 2014-12-17

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CN201420442434.2U Expired - Fee Related CN204017434U (en) 2014-08-06 2014-08-06 A kind of Supercritical Fluid Extraction Enhanced by Ultrasonic device

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CN (1) CN204017434U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110292787A (en) * 2019-04-27 2019-10-01 孙志良 A kind of supercritical carbon dioxide extraction kettle and extracting process
CN111068358A (en) * 2018-10-19 2020-04-28 联盛科技有限公司 High-efficiency ultrasonic extraction equipment and method for improving supercritical extraction efficiency

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111068358A (en) * 2018-10-19 2020-04-28 联盛科技有限公司 High-efficiency ultrasonic extraction equipment and method for improving supercritical extraction efficiency
CN110292787A (en) * 2019-04-27 2019-10-01 孙志良 A kind of supercritical carbon dioxide extraction kettle and extracting process

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20141217

Termination date: 20200806

CF01 Termination of patent right due to non-payment of annual fee