CN203971473U - Alcohol-settling tank - Google Patents

Alcohol-settling tank Download PDF

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Publication number
CN203971473U
CN203971473U CN201420336122.3U CN201420336122U CN203971473U CN 203971473 U CN203971473 U CN 203971473U CN 201420336122 U CN201420336122 U CN 201420336122U CN 203971473 U CN203971473 U CN 203971473U
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CN
China
Prior art keywords
liquid
tank
alcohol
tank body
stirring motor
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201420336122.3U
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Chinese (zh)
Inventor
姬星宇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HENAN ZHONGSHENG ANIMAL PHARMACEUTICAL Co Ltd
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HENAN ZHONGSHENG ANIMAL PHARMACEUTICAL Co Ltd
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Priority to CN201420336122.3U priority Critical patent/CN203971473U/en
Application granted granted Critical
Publication of CN203971473U publication Critical patent/CN203971473U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model belongs to a kind of Alcohol-settling tank for Chinese medicine water drug-decocting concentrating liquid, comprise tank body, chuck, heat-insulation layer, ellipsoidal head, stirring motor, charging aperture, access hole, observation window, Pneumatic butterfly valve, it is characterized in that: in tank body, be provided with spray nozzle type liquid distribution trough, the shaft being connected with stirring motor, shaft bottom is provided with taper bit, Pneumatic butterfly valve bottom is provided with funnel, funnel bottom is connected with tremie pipe, tremie pipe bottom is provided with centrifugal mechanism, leaving standstill tank outlet is connected with vavuum pump, vacuum pump outlet is provided with liquid back pipe, liquid back pipe is connected with charging aperture, on charging aperture and liquid back pipe, be provided with flowmeter counter, the utility model can be to the By Chinese Medicines precipitation that repeatedly circulates, reduce the impurity in liquid, it is wider that spray nozzle type liquid distribution trough distributes ethanol in tank, reduce mixing speed, not only save ethanol consumption, and avoid concentrate to occur the phenomenon of parcel, liquid has shortened the time of solution left standstill after centrifugation.

Description

Alcohol-settling tank
Technical field
The utility model belongs to a kind of solid-liquid separating equipment of alcohol precipitation process, particularly a kind of Alcohol-settling tank for Chinese medicine water drug-decocting concentrating liquid.
Background technology
In Chinese Traditional Medicine, ethanol precipitation is the process for purification refine that Chinese medicine aqueous extract is conventional, the party's ratio juris is: medicinal material first extracts through decocting, wherein the aqueous soluble active constituent such as alkaloid, acylate, amino acids is extracted, also lixiviate goes out a lot of water-solubility impurities simultaneously, alcohol deposition method is exactly to utilize active ingredient can be dissolved in ethanol and impurity is insoluble to the characteristic of ethanol, is adding after ethanol, and active ingredient turns that to be dissolved in ethanol impurity out precipitated.The object of alcohol precipitation is to retain effective ingredient in order to remove impurity, thereby the applicability of alcohol precipitation unit operations technique and equipment thereof substantial connection security, stability and the validity of tcm product, with formulation and the quality of product be indivisible organic whole.In alcohol precipitation process, need to use Alcohol-settling tank to carry out Separation of Solid and Liquid, existing Alcohol-settling tank often can only carry out once pure heavy, separate rear impurity precipitation not exclusively through primary sedimentation, easily there is the phenomenon of parcel concentrate, ethanol is difficult to fully contact with liquid, cause loss of effective components, meanwhile, the solution after pure sinking often needs to leave standstill 24-48h could extract supernatant; Although can make ethanol disperse by the stirring of agitator, reduce the alcohol amount that contains of regional area, too fast stirring easily makes excess Temperature, has accelerated the volatilization of ethanol, has not only increased ethanol consumption, and has increased the consumption of the energy; In addition, after alcohol precipitation, at the bottom of tank, can assemble a large amount of sediments, cause settling tank deslagging difficulty, sediment often needs again to add hot water that sediment thawing could be discharged, and some sediment is that sticky pastel must could be discharged after extrusion process, making like this to process sediment process wastes time and energy.
Utility model content
The utility model object is to overcome the deficiencies in the prior art and a kind of Alcohol-settling tank for Chinese medicine water drug-decocting concentrating liquid is provided.
The purpose of this utility model is achieved in that a kind of Alcohol-settling tank, comprise tank body, be arranged on the chuck on tank wall, be arranged on the heat-insulation layer in chuck outside, be arranged on the ellipsoidal head at tank body top, be arranged on the stirring motor at ellipsoidal head top, be arranged on the charging aperture in stirring motor left side, be arranged on the access hole on stirring motor right side, be arranged on the observation window on access hole, be arranged on the Pneumatic butterfly valve of tank base, wherein, tank body upper portion side wall is vertically installed with liquid-feeding tube, tank body lower part sidewall is vertically installed with drain pipe, heat-insulation layer bottom is provided with cooling water inlet, heat-insulation layer top is provided with coolant outlet, it is characterized in that: in described tank body, be provided with spray nozzle type liquid distribution trough, spray nozzle type liquid distribution trough is connected with liquid-feeding tube, on liquid-feeding tube, be provided with flow controller, in tank body, be provided with the shaft being connected with stirring motor, shaft bottom is provided with taper bit, taper bit is along with shaft rotates together, Pneumatic butterfly valve bottom is provided with funnel, Pneumatic butterfly valve and funnel are flexibly connected, funnel bottom is connected with tremie pipe by sealing ring, on tremie pipe, be provided with ceramic ball valve, tremie pipe bottom is provided with centrifugal mechanism, centrifugal mechanism outlet with leave standstill tank and be connected, leaving standstill tank outlet is connected with vavuum pump, vacuum pump outlet is provided with liquid back pipe, liquid back pipe is connected with charging aperture, on charging aperture and liquid back pipe, be provided with flowmeter counter.
Described centrifugal mechanism comprises casing, be arranged on the motor on casing, be arranged on the rotary drum being connected with motor in casing, be arranged on the screw feeder in rotary drum, screw feeder two ends are provided with bearing block, screw feeder bottom is provided with differential mechanism, rotary drum top is provided with slag notch, casing bottom is provided with liquid outlet, bottom of the drum is provided with liquid level adjustment sheet, because the rotating speed of screw feeder and rotary drum is different, there is speed discrepancy in the two, the slag notch that utilizes the speed discrepancy of screw feeder and rotary drum to shift the dregs of a decoction onto rotary drum upper end is discharged, liquid is shifted onto to the liquid outlet of rotary drum lower end simultaneously, realize the Separation of Solid and Liquid of liquid, liquid after centrifugation has shortened the time of repose of liquid greatly.
Described standing tank top is provided with sand rod filter course, and standing pot bottom is provided with finished product discharging opening.
On the ellipsoidal head of described observation window bottom, be provided with the explosion-proof lamp of looking.
On described ellipsoidal head, be also provided with temperature sensor and pressure sensor, the thermometer and the Pressure gauge that are connected respectively with temperature sensor and pressure sensor.
On described stirring motor, be provided with speed regulator, rotational speed governor is connected with shaft.
The utlity model has following good effect:
1, by Alcohol-settling tank of the present utility model, can be to the By Chinese Medicines precipitation that repeatedly circulates, reduce the impurity in solution, use spray nozzle type liquid distribution trough to avoid concentrate parcel phenomenon, ethanol is distributed in Alcohol-settling tank wider, ethanol is more abundant with contacting of liquid, retain more active ingredient in herb liquid, solution after pure sinking, through centrifugal, filtration, has greatly reduced the time of solution left standstill, has improved the efficiency of alcohol precipitation;
2, it is more even that spray nozzle type liquid distribution trough makes the sprinkling of ethanol, reduces the alcohol amount that contains of regional area, reduced the mixing speed of agitator, thereby reduce the temperature of solution, reduced the volatilization of ethanol, not only saved ethanol consumption, and reduced the consumption of the energy, save the energy;
3, the sediment of Alcohol-settling tank bottom is by drill bit fragmentation, do not need in tank body, to add hot water or steam to make sediment melt discharge again, or by discharging after extrusion process, while using drill bit broken, can regulate the speed regulator on rotary electric machine, thereby control the rotating speed of shaft, facilitate the deslagging of Alcohol-settling tank bottom, saved the deslagging time.
Brief description of the drawings
Fig. 1 is the structural representation of utility model.
Fig. 2 is the structural representation of centrifugal mechanism.
In figure: 1. tank body 2. chuck 3. heat-insulation layer 4. ellipsoidal head 5. stirring motor 6. charging aperture 7. access hole 8. observation window 9. Pneumatic butterfly valve 10. liquid-feeding tube 11. drain pipe 12. cooling water inlet 13. coolant outlet 14. base 15. spray nozzle type liquid distribution trough 16. flow controller 17. shaft 18. taper bit 19. funnel 20. sealing ring 21. tremie pipe 22. ceramic ball valve 23. centrifugal mechanisms 24. leave standstill explosion-proof lamp 40. temperature sensor 41. pressure sensor 42. speed regulators of looking of tank 25. vavuum pump 26. liquid back pipe 27. flowmeter counter 28. casing 29. motor 30. rotary drum 31. screw feeder 32. bearing block 33. differential mechanism 34. slag notch 35. liquid outlet 36. liquid level adjustment sheet 37. sand rod filter course 38. finished product discharging openings 39..
Detailed description of the invention
Embodiment 1, as Fig. 1, shown in Fig. 2, a kind of Alcohol-settling tank, comprise tank body 1, be arranged on the chuck 2 on tank body 1 outer wall, be arranged on the heat-insulation layer 3 in chuck 2 outsides, be arranged on the ellipsoidal head 4 at tank body 1 top, be arranged on the stirring motor 5 at ellipsoidal head 4 tops, be arranged on the charging aperture 6 in stirring motor 5 left sides, be arranged on the access hole 7 on stirring motor 5 right sides, be arranged on the observation window 8 on access hole 7, be arranged on the Pneumatic butterfly valve 9 of tank body 1 bottom, wherein, tank body 1 upper portion side wall is vertically installed with liquid-feeding tube 10, tank body 1 lower sides is vertically installed with drain pipe 11, heat-insulation layer 3 bottoms are provided with cooling water inlet 12, heat-insulation layer 3 tops are provided with coolant outlet 13, described tank body 1 inwall is provided with base 14, on base 14, be provided with spray nozzle type liquid distribution trough 15, spray nozzle type liquid distribution trough 15 is connected with liquid-feeding tube 10, on liquid-feeding tube 10, be provided with flow controller 16, in tank body 1, be provided with the shaft 17 being connected with stirring motor 5, shaft 17 bottoms are provided with taper bit 18, Pneumatic butterfly valve 10 bottoms are provided with funnel 19, Pneumatic butterfly valve 10 and funnel 19 are flexibly connected, funnel 19 bottoms are connected with tremie pipe 21 by sealing ring 20, on tremie pipe 21, be provided with ceramic ball valve 22, tremie pipe 21 bottoms are provided with centrifugal mechanism 23, centrifugal mechanism 23 outlets are connected with standing tank 24, leaving standstill tank 24 outlets is connected with vavuum pump 25, vavuum pump 25 outlets are provided with liquid back pipe 26, liquid back pipe 26 is connected with charging aperture 6, on charging aperture 7 and liquid back pipe 26, be provided with flowmeter counter 27, centrifugal mechanism 23 comprises casing 28, be arranged on the motor 29 on casing 28, be arranged on the rotary drum 30 being connected with motor in casing 28, be arranged on the screw feeder 31 in rotary drum 30, screw feeder 31 two ends are provided with bearing block 32, screw feeder 31 bottoms are provided with differential mechanism 33, on rotary drum, 30 are provided with slag notch 34, casing 28 bottoms are provided with liquid outlet 35, rotary drum 30 bottoms are provided with liquid level adjustment sheet 36, leave standstill tank 24 tops and be provided with sand rod filter course 37, leave standstill tank 24 bottoms and be provided with finished product discharging opening 38, on the ellipsoidal head 4 of observation window 8 bottoms, be provided with the explosion-proof lamp 39 of looking, on ellipsoidal head 4, be also provided with temperature sensor 40 and pressure sensor 41, the thermometer and the Pressure gauge that are connected respectively with temperature sensor 40 and pressure sensor 41, on stirring motor 5, be provided with speed regulator 42, rotational speed governor 42 is connected with shaft 17.
When the utility model uses, from charging aperture, add liquid, then from liquid-feeding tube, in tank body, add ethanol by spray nozzle type liquid distribution trough, increase the distribution area of ethanol in Alcohol-settling tank, make ethanol more abundant with contacting of liquid, liquid after an alcohol precipitation enters in centrifugal mechanism through funnel, liquid after alcohol precipitation enters and leaves standstill in tank through centrifugal treating, after filtering, form comparatively pure liquid at the liquid leaving standstill in tank, if still contain impurity in liquid, liquid after leaving standstill can be entered and in tank body, carried out secondary alcohol precipitation by liquid back pipe, so not only improve alcohol precipitation efficiency, and the active ingredient in liquid is retained.
The foregoing is only preferred embodiment of the present utility model; not in order to limit the utility model; for a person skilled in the art; the utility model can have various modifications and variations; all within spirit of the present utility model and principle; any amendment of doing, be equal to replacement, improvement etc., within all should being included in protection domain of the present utility model.

Claims (6)

1. an Alcohol-settling tank, comprise tank body, be arranged on the chuck on tank wall, be arranged on the heat-insulation layer in chuck outside, be arranged on the ellipsoidal head at tank body top, be arranged on the stirring motor at ellipsoidal head top, be arranged on the charging aperture in stirring motor left side, be arranged on the access hole on stirring motor right side, be arranged on the observation window on access hole, be arranged on the Pneumatic butterfly valve of tank base, wherein, tank body upper portion side wall is vertically installed with liquid-feeding tube, tank body lower part sidewall is vertically installed with drain pipe, heat-insulation layer bottom is provided with cooling water inlet, heat-insulation layer top is provided with coolant outlet, it is characterized in that: in described tank body, be provided with spray nozzle type liquid distribution trough, spray nozzle type liquid distribution trough is connected with liquid-feeding tube, on liquid-feeding tube, be provided with flow controller, in tank body, be provided with the shaft being connected with stirring motor, shaft bottom is provided with taper bit, Pneumatic butterfly valve bottom is provided with funnel, Pneumatic butterfly valve and funnel are flexibly connected, funnel bottom is connected with tremie pipe by sealing ring, on tremie pipe, be provided with ceramic ball valve, tremie pipe bottom is provided with centrifugal mechanism, centrifugal mechanism outlet with leave standstill tank and be connected, leaving standstill tank outlet is connected with vavuum pump, vacuum pump outlet is provided with liquid back pipe, liquid back pipe is connected with charging aperture, on charging aperture and liquid back pipe, be provided with flowmeter counter.
2. Alcohol-settling tank according to claim 1, it is characterized in that: described centrifugal mechanism comprises casing, be arranged on motor on casing, be arranged on the rotary drum that is connected with motor in casing, be arranged on the screw feeder in rotary drum, screw feeder two ends are provided with bearing block, screw feeder bottom is provided with differential mechanism, rotary drum top is provided with slag notch, casing bottom is provided with liquid outlet, and bottom of the drum is provided with liquid level adjustment sheet.
3. Alcohol-settling tank according to claim 1, is characterized in that: described standing tank top is provided with sand rod filter course, and standing pot bottom is provided with finished product discharging opening.
4. Alcohol-settling tank according to claim 1, is characterized in that: on the ellipsoidal head of described observation window bottom, be provided with the explosion-proof lamp of looking.
5. Alcohol-settling tank according to claim 1, is characterized in that: on described ellipsoidal head, be also provided with temperature sensor and pressure sensor, the thermometer and the Pressure gauge that are connected respectively with temperature sensor and pressure sensor.
6. Alcohol-settling tank according to claim 1, is characterized in that: on described stirring motor, be provided with speed regulator, rotational speed governor is connected with shaft.
CN201420336122.3U 2014-06-23 2014-06-23 Alcohol-settling tank Expired - Fee Related CN203971473U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420336122.3U CN203971473U (en) 2014-06-23 2014-06-23 Alcohol-settling tank

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420336122.3U CN203971473U (en) 2014-06-23 2014-06-23 Alcohol-settling tank

Publications (1)

Publication Number Publication Date
CN203971473U true CN203971473U (en) 2014-12-03

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201420336122.3U Expired - Fee Related CN203971473U (en) 2014-06-23 2014-06-23 Alcohol-settling tank

Country Status (1)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105353800A (en) * 2015-12-11 2016-02-24 苏州泽达兴邦医药科技有限公司 Control method of cold precipitation temperature in traditional Chinese medicine alcohol precipitation process
CN105582707A (en) * 2016-01-08 2016-05-18 安徽华润金蟾药业股份有限公司 Cinobufagin ethanol precipitation device and method for controlling ethanol adding amount in ethanol precipitation process of cinobufagin
CN105694040A (en) * 2016-03-14 2016-06-22 四川天科技股份有限公司 Process for heat dispersion purification under pressure during preparation of polyethersulfone resin
CN108996048A (en) * 2018-07-09 2018-12-14 湘潭大学 A kind of high-temp liquid dump tank buffer structure
CN111481954A (en) * 2020-04-24 2020-08-04 天津市中环系统工程有限责任公司 Alcohol precipitation method capable of automatically sucking supernatant

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105353800A (en) * 2015-12-11 2016-02-24 苏州泽达兴邦医药科技有限公司 Control method of cold precipitation temperature in traditional Chinese medicine alcohol precipitation process
CN105353800B (en) * 2015-12-11 2017-09-15 苏州泽达兴邦医药科技有限公司 A kind of control method of the cold heavy temperature of Chinese medicine alcohol precipitation process
CN105582707A (en) * 2016-01-08 2016-05-18 安徽华润金蟾药业股份有限公司 Cinobufagin ethanol precipitation device and method for controlling ethanol adding amount in ethanol precipitation process of cinobufagin
CN105694040A (en) * 2016-03-14 2016-06-22 四川天科技股份有限公司 Process for heat dispersion purification under pressure during preparation of polyethersulfone resin
CN108996048A (en) * 2018-07-09 2018-12-14 湘潭大学 A kind of high-temp liquid dump tank buffer structure
CN111481954A (en) * 2020-04-24 2020-08-04 天津市中环系统工程有限责任公司 Alcohol precipitation method capable of automatically sucking supernatant

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
EE01 Entry into force of recordation of patent licensing contract

Assignee: Shangqiu Meilan Biological Engineering Co., Ltd.

Assignor: Henan Zhongsheng Animal Pharmaceutical Co., Ltd.

Contract record no.: 2016410000015

Denomination of utility model: Alcohol precipitation tank

Granted publication date: 20141203

License type: Exclusive License

Record date: 20160906

LICC Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: Alcohol precipitation tank

Effective date of registration: 20161216

Granted publication date: 20141203

Pledgee: Bank of China Limited by Share Ltd Zhecheng branch

Pledgor: Henan Zhongsheng Animal Pharmaceutical Co., Ltd.

Registration number: 2016990001115

EC01 Cancellation of recordation of patent licensing contract
EC01 Cancellation of recordation of patent licensing contract

Assignee: Shangqiu Meilan Biological Engineering Co., Ltd.

Assignor: Henan Zhongsheng Animal Pharmaceutical Co., Ltd.

Contract record no.: 2016410000015

Date of cancellation: 20170428

PC01 Cancellation of the registration of the contract for pledge of patent right

Date of cancellation: 20180320

Granted publication date: 20141203

Pledgee: Bank of China Limited by Share Ltd Zhecheng branch

Pledgor: Henan Zhongsheng Animal Pharmaceutical Co., Ltd.

Registration number: 2016990001115

PC01 Cancellation of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: Alcohol precipitation tank

Effective date of registration: 20180320

Granted publication date: 20141203

Pledgee: Bank of China Limited by Share Ltd Zhecheng branch

Pledgor: Henan Zhongsheng Animal Pharmaceutical Co., Ltd.

Registration number: 2018990000207

PE01 Entry into force of the registration of the contract for pledge of patent right
PC01 Cancellation of the registration of the contract for pledge of patent right
PC01 Cancellation of the registration of the contract for pledge of patent right

Date of cancellation: 20190318

Granted publication date: 20141203

Pledgee: Bank of China Limited by Share Ltd Zhecheng branch

Pledgor: Henan Zhongsheng Animal Pharmaceutical Co., Ltd.

Registration number: 2018990000207

PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: Alcohol precipitation tank

Effective date of registration: 20190318

Granted publication date: 20141203

Pledgee: Bank of China Limited by Share Ltd Zhecheng branch

Pledgor: Henan Zhongsheng Animal Pharmaceutical Co., Ltd.

Registration number: 2019990000228

PC01 Cancellation of the registration of the contract for pledge of patent right
PC01 Cancellation of the registration of the contract for pledge of patent right

Date of cancellation: 20200310

Granted publication date: 20141203

Pledgee: Bank of China Limited by Share Ltd Zhecheng branch

Pledgor: HENAN ZHONGSHENG ANIMAL PHARMACEUTICAL Co.,Ltd.

Registration number: 2019990000228

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20141203

Termination date: 20210623

CF01 Termination of patent right due to non-payment of annual fee