CN203955229U - A kind of process units of antimony pentafluoride - Google Patents
A kind of process units of antimony pentafluoride Download PDFInfo
- Publication number
- CN203955229U CN203955229U CN201420314343.0U CN201420314343U CN203955229U CN 203955229 U CN203955229 U CN 203955229U CN 201420314343 U CN201420314343 U CN 201420314343U CN 203955229 U CN203955229 U CN 203955229U
- Authority
- CN
- China
- Prior art keywords
- reactor
- cooling jacket
- antimony
- process units
- antimony pentafluoride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model relates to the process units of antimony pentafluoride, object is to provide a kind of antimony pentafluoride process units that can long-time continuous reaction, described process units, comprise the reactor of hollow, cooling jacket and filter, in described reactor, middle part is provided with pallet, described reactor upper end is provided with dog-house, described dog-house top is provided with Pressure gauge, described reactor outer upper is provided with atmospheric valve, temperature measuring unit and fluorine gas passage, described cooling jacket is coated on described reactor outer lower portion, described cooling jacket is provided with water inlet and delivery port, described filter is connected to reactor bottom by blow-off valve, described filter bottom is provided with outlet valve.The beneficial effects of the utility model are: by cooling jacket, the temperature of reactor lower part is reduced, make the antimony trifluoride gas in reactor entirely be condensed into solid, fluorine gas continues to enter reactor and antimony reaction, thereby reaction is carried out continuously.
Description
Technical field
The utility model relates to a kind of process units of antimony pentafluoride.
Background technology
Existing antimony pentafluoride process units, its device is mainly a reactor, and the material of reactor is 304 stainless steels.Inside is provided with the pallet that antimony is housed, and fluorine gas enters into reactor inside, reacts generate antimony pentafluoride with antimony, in reaction, can generate antimony trifluoride simultaneously, and rise and turn to antimony trifluoride gas under reaction high temperature, these gases leave system in the time of emptying, and reaction is further carried out.The antimony trifluoride of emitting very easily in aperture less place condense, as needle valve spool and blowdown piping inwall, cause emptying not smooth, inside reactor antimony trifluoride gas can not be discharged in time, cause fluorine gas quantity not sufficient, also be accompanied by more antimony trifluoride and generate, so vicious circle finally occurs that reaction stops carrying out.Emptying must be often gone timely in operation in the past, find when atmospheric valve is stifled to change in time, otherwise reaction cannot continuity be carried out.
Utility model content
The purpose of this utility model is to have overcome above-mentioned defect, provide a kind of can long-time continuous the antimony pentafluoride process units of reaction.
In order to solve the problems of the technologies described above, the technical solution adopted in the utility model is:
A kind of process units of antimony pentafluoride, comprise reactor, cooling jacket and the filter of hollow, in described reactor, middle part is provided with pallet, described reactor upper end is provided with dog-house, described dog-house top is provided with Pressure gauge, described reactor outer upper is provided with atmospheric valve, temperature measuring unit and fluorine gas passage, described cooling jacket is coated on described reactor outer lower portion, described cooling jacket is provided with water inlet and delivery port, described filter is connected to reactor bottom by blow-off valve, and described filter bottom is provided with outlet valve.
Further, the port of export of described fluorine gas passage is positioned at pallet top.
Further, described temperature measuring unit is positioned at pallet top.
Further, described water inlet is located at cooling jacket bottom, and described delivery port is located at cooling jacket top.
Further, described temperature measuring unit is teletransmission thermal resistance.
The beneficial effects of the utility model are: by cooling jacket, the temperature of reactor lower part is reduced, make the antimony trifluoride gas in reactor entirely be condensed into solid, fluorine gas continues to enter reactor and antimony reaction, thereby reaction is carried out continuously.
Brief description of the drawings
Fig. 1 is the structure chart of the utility model embodiment.
Label declaration:
1, reactor; 2, cooling jacket; 3, filter; 11, pallet; 12, dog-house; 121, Pressure gauge; 13, atmospheric valve; 14, temperature measuring unit; 15, fluorine gas passage; 21, water inlet; 22, delivery port; 31, blow-off valve; 32, outlet valve.
Detailed description of the invention
By describing technology contents of the present utility model, structural feature in detail, being realized object and effect, below in conjunction with embodiment and coordinate accompanying drawing to be explained in detail.
The design of the utility model most critical is: by cooling jacket 2, the temperature of reactor 1 bottom is reduced, make the antimony trifluoride gas in reactor 1 entirely be condensed into solid, fluorine gas continues to enter reactor 1 and antimony reaction, thereby reaction is carried out continuously.
Refer to Fig. 1, a kind of process units of antimony pentafluoride, comprise the reactor 1 of hollow, cooling jacket 2 and filter 3, the interior middle part of described reactor 1 is provided with pallet 11, described reactor 1 upper end is provided with dog-house 12, described dog-house 12 tops are provided with Pressure gauge 121, described reactor 1 outer upper is provided with atmospheric valve 13, temperature measuring unit 14 and fluorine gas passage 15, described cooling jacket 2 is coated on described reactor 1 outer lower portion, described cooling jacket 2 is provided with water inlet 21 and delivery port 22, described filter 3 is connected to reactor 1 bottom by blow-off valve 31, described filter 3 bottoms are provided with outlet valve 32.
Operation principle of the present utility model is: antimony is placed in pallet 11, fluorine gas enters into reactor 1 inside by fluorine gas passage 15, react with antimony and generate antimony pentafluoride, in reaction, can generate antimony trifluoride simultaneously, and rise and turn to antimony trifluoride gas under reaction high temperature, pass into cool brine in cooling jacket 2 porch, utilize the cooling jacket 2 of bottom to be cooled to subzero 30 degree, antimony trifluoride is condensed in reactor 1 bottom, flow to reactor 1 bottom together with condensed antimony pentafluoride.Now the antimony trifluoride gas in reactor is condensed into solid entirely, and fluorine gas continues to enter reactor 1 and antimony reaction, thereby reaction is carried out continuously.And the antimony trifluoride of reactor 1 bottom is in the time that finished product fills, removes by filter through bottom filters 3, thereby obtain water white antimony pentafluoride finished product.
From foregoing description, the beneficial effects of the utility model are: by cooling jacket 2, the temperature of reactor 1 bottom is reduced, make the antimony trifluoride gas in reactor 1 entirely be condensed into solid, fluorine gas continues to enter reactor 1 and antimony reaction, thereby reaction is carried out continuously.
Further, the port of export of described fluorine gas passage 15 is positioned at pallet 11 tops, is reacted, fast reaction speed the fluorine gas very first time that enters reactor 1 with antimony.
Further, described temperature measuring unit 14 is positioned at pallet top, makes temperature measuring unit 14 reaction temperature can accurately be detected.
Further, described water inlet 21 is located at cooling jacket 2 bottoms, and described delivery port 22 is located at cooling jacket 2 tops, makes the temperature of cooling jacket 2 bottoms higher compared with temperature low and top, has the cooling of gradient.
Further, described temperature measuring unit 14 is teletransmission thermal resistance.
In sum, by cooling jacket, the temperature of reactor lower part is reduced, make the antimony trifluoride gas in reactor entirely be condensed into solid, fluorine gas continues to enter reactor and antimony reaction, thereby reaction is carried out continuously, and the antimony trifluoride of reactor bottom is in the time that finished product fills, removes by filter through bottom filters, thereby obtain water white antimony pentafluoride finished product.
The foregoing is only embodiment of the present utility model; not thereby limit the scope of the claims of the present utility model; every equivalent structure or conversion of equivalent flow process that utilizes the utility model description and accompanying drawing content to do; or be directly or indirectly used in other relevant technical fields, be all in like manner included in scope of patent protection of the present utility model.
Claims (5)
1. the process units of an antimony pentafluoride, it is characterized in that: the reactor, cooling jacket and the filter that comprise hollow, in described reactor, middle part is provided with pallet, described reactor upper end is provided with dog-house, described dog-house top is provided with Pressure gauge, described reactor outer upper is provided with atmospheric valve, temperature measuring unit and fluorine gas passage, described cooling jacket is coated on described reactor outer lower portion, described cooling jacket is provided with water inlet and delivery port, described filter is connected to reactor bottom by blow-off valve, and described filter bottom is provided with outlet valve.
2. the process units of antimony pentafluoride according to claim 1, is characterized in that: the port of export of described fluorine gas passage is positioned at pallet top.
3. the process units of antimony pentafluoride according to claim 1, is characterized in that: described temperature measuring unit is positioned at pallet top.
4. the process units of antimony pentafluoride according to claim 1, is characterized in that: described water inlet is located at cooling jacket bottom, and described delivery port is located at cooling jacket top.
5. the process units of antimony pentafluoride according to claim 1, is characterized in that: described temperature measuring unit is teletransmission thermal resistance.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420314343.0U CN203955229U (en) | 2014-06-13 | 2014-06-13 | A kind of process units of antimony pentafluoride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420314343.0U CN203955229U (en) | 2014-06-13 | 2014-06-13 | A kind of process units of antimony pentafluoride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203955229U true CN203955229U (en) | 2014-11-26 |
Family
ID=51915871
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420314343.0U Expired - Fee Related CN203955229U (en) | 2014-06-13 | 2014-06-13 | A kind of process units of antimony pentafluoride |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203955229U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114655982A (en) * | 2022-04-07 | 2022-06-24 | 九江诺尔新材料科技有限公司 | Continuous production method and application of antimony pentafluoride |
-
2014
- 2014-06-13 CN CN201420314343.0U patent/CN203955229U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114655982A (en) * | 2022-04-07 | 2022-06-24 | 九江诺尔新材料科技有限公司 | Continuous production method and application of antimony pentafluoride |
| CN114655982B (en) * | 2022-04-07 | 2023-09-08 | 九江诺尔新材料科技有限公司 | Continuous production method and application of antimony pentafluoride |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN203955229U (en) | A kind of process units of antimony pentafluoride | |
| CN204522950U (en) | A kind of chemical reaction tower | |
| CN203355320U (en) | Distiller | |
| CN203043955U (en) | Vacuum feeding device | |
| CN202614559U (en) | Heat-preserving sampling device for coal gas | |
| CN205287661U (en) | Trace liquid distillation plant | |
| CN103240030A (en) | Liquid medicine mixing device | |
| CN204255412U (en) | Reactor detects measuring apparatus | |
| CN204745695U (en) | Hydrochloric acid evaporating column | |
| CN204151135U (en) | One samples anaerobic reactor easily | |
| CN202658114U (en) | Low bromide epoxy resin reaction kettle system | |
| CN209612927U (en) | A kind of trifluoromethanesulfonic acid production system | |
| CN203025162U (en) | Device for measuring oxygen content in chlorine | |
| CN204154538U (en) | A kind of reactor plain type sampling apparatus | |
| CN206199230U (en) | A kind of gas-liquid separation reflux | |
| CN205031904U (en) | Acetic acid recovery tower | |
| CN102338650B (en) | Measured medium flowing type anti-freezing liquidometer device | |
| CN201962221U (en) | Improved alcohol recovering device | |
| CN203715697U (en) | Reaction chute of nickel electrolyte purification system | |
| CN203190852U (en) | Material condensing device | |
| CN203389616U (en) | Solvent elevated measuring tank with novel dropping pipette | |
| CN207557216U (en) | Deoxidation pipe device | |
| CN204356288U (en) | A kind of weight hydrocarbon separation system | |
| CN204223557U (en) | With the wine tank of liquidometer | |
| CN203710711U (en) | Thickening cylinder with liquid level detection function for automatic thickener |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 354001 Nanping Province, Shaowu City, sun mouth new ammonia Road, No. 18 Patentee after: Fujian forever Technology Co., Ltd. Address before: 354001 Nanping Province, Shaowu City, sun mouth new ammonia Road, No. 18 Patentee before: Fujian Shaowu Yongjing Chemical Co., Ltd. |
|
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: 354001 Jinling Road, Jintong Industrial Park, Shaowu, Fujian Province, No. 6 Patentee after: Fujian permanent crystal Polytron Technologies Inc Address before: 354001 Nanping Province, Shaowu City, sun mouth new ammonia Road, No. 18 Patentee before: Fujian forever Technology Co., Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141126 Termination date: 20200613 |