CN203940689U - The equipment of the dirty nitrogen purification of high extraction and low energy consumption nitrogen - Google Patents
The equipment of the dirty nitrogen purification of high extraction and low energy consumption nitrogen Download PDFInfo
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- CN203940689U CN203940689U CN201420335643.7U CN201420335643U CN203940689U CN 203940689 U CN203940689 U CN 203940689U CN 201420335643 U CN201420335643 U CN 201420335643U CN 203940689 U CN203940689 U CN 203940689U
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- nitrogen
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Classifications
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/08—Separating gaseous impurities from gases or gaseous mixtures or from liquefied gases or liquefied gaseous mixtures
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2200/00—Processes or apparatus using separation by rectification
- F25J2200/04—Processes or apparatus using separation by rectification in a dual pressure main column system
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2210/00—Processes characterised by the type or other details of the feed stream
- F25J2210/04—Mixing or blending of fluids with the feed stream
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2215/00—Processes characterised by the type or other details of the product stream
- F25J2215/42—Nitrogen or special cases, e.g. multiple or low purity N2
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2220/00—Processes or apparatus involving steps for the removal of impurities
- F25J2220/44—Separating high boiling, i.e. less volatile components from nitrogen, e.g. CO, Ar, O2, hydrocarbons
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2230/00—Processes or apparatus involving steps for increasing the pressure of gaseous process streams
- F25J2230/30—Compression of the feed stream
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2235/00—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
- F25J2235/42—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams the fluid being nitrogen
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2245/00—Processes or apparatus involving steps for recycling of process streams
- F25J2245/42—Processes or apparatus involving steps for recycling of process streams the recycled stream being nitrogen
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- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Mechanical Engineering (AREA)
- Thermal Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Separation By Low-Temperature Treatments (AREA)
Abstract
The utility model discloses the equipment of the dirty nitrogen purification of a kind of high extraction and low energy consumption nitrogen, comprise dirty nitrogen compressor, be connected to the main heat exchanger on dirty nitrogen compressor, be connected to the king-tower on main heat exchanger, be connected to secondary tower and subcooler on king-tower, described king-tower is provided with king-tower condenser, described secondary tower is provided with secondary tower condenser, the dirty nitrogen outlet of described dirty nitrogen compressor is connected with the dirty nitrogen inlet of main heat exchanger by pipeline, the dirty nitrogen outlet of described main heat exchanger is connected with the dirty nitrogen inlet of king-tower by pipeline, the pure nitrogen gas outlet of described king-tower is connected with the pure nitrogen gas import of main heat exchanger by pipeline, the liquid nitrogen fraction outlet of described king-tower is connected with the liquid nitrogen fraction import of subcooler by pipeline, the liquid nitrogen fraction outlet of described subcooler is connected with the liquid nitrogen fraction import of king-tower condenser and the liquid nitrogen fraction import of secondary tower condenser by pipeline respectively.It is high that the utility model not only extracts nitrogen recovery rate, and it is low, cost-saving to extract the required energy consumption of nitrogen.
Description
Technical field
The utility model relates to and belongs to industrial gasses manufacture field, relates in particular to the equipment of the dirty nitrogen purification of a kind of high extraction and low energy consumption nitrogen.
Background technology
The original throwing of user has air separation unit, its original air separation unit cannot produce nitrogen or original nitrogen output cannot meet Production requirement, if a set of nitrogen-making device of sole investment again, its cost of investment and operating cost are all higher, therefore considered utility model dirty nitrogen waste gas reclaim the nitrogen-making device of purifying again.
Utility model content
Defect and deficiency that the utility model exists in order to solve above-mentioned prior art, provide a kind of technique advanced person, investment and operating cost are low, recovery rate is high, energy-saving and cost-reducing high extraction and the equipment of the dirty nitrogen purification of low energy consumption nitrogen.
For solving the problems of the technologies described above, the equipment of dirty nitrogen purification nitrogen of the present utility model, comprise dirty nitrogen compressor, be connected to the main heat exchanger on dirty nitrogen compressor, be connected to the king-tower on main heat exchanger, be connected to secondary tower and subcooler on king-tower, described king-tower is provided with king-tower condenser, described secondary tower is provided with secondary tower condenser, the dirty nitrogen outlet of described dirty nitrogen compressor is connected with the dirty nitrogen inlet of main heat exchanger by pipeline, the dirty nitrogen outlet of described main heat exchanger is connected with the dirty nitrogen inlet of king-tower by pipeline, the pure nitrogen gas outlet of described king-tower is connected with the pure nitrogen gas import of main heat exchanger by pipeline, the liquid nitrogen fraction outlet of described king-tower is connected with the liquid nitrogen fraction import of subcooler by pipeline, the liquid nitrogen fraction outlet of described subcooler is connected with the liquid nitrogen fraction import of king-tower condenser and the liquid nitrogen fraction import of secondary tower condenser by pipeline respectively, the liquid nitrogen fraction outlet of described secondary tower is connected with the liquid nitrogen fraction import of secondary tower condenser by pipeline, the dirty nitrogen outlet of described king-tower condenser is connected with the dirty nitrogen inlet of secondary tower by pipeline, the dirty nitrogen outlet of described secondary tower condenser is passed subcooler and is connected with the dirty nitrogen inlet of dirty nitrogen compressor after main heat exchanger successively by pipeline, the liquid nitrogen fraction outlet of described king-tower condenser is connected with the liquid nitrogen fraction import of king-tower by pipeline, the liquid nitrogen fraction outlet of described secondary tower condenser is connected with the liquid nitrogen fraction import of secondary tower and the liquid nitrogen fraction import of king-tower by pipeline respectively.
Preferably, the pure nitrogen gas outlet of described king-tower is also connected with the pure nitrogen gas import of king-tower condenser by pipeline, and the pure nitrogen gas outlet of described secondary tower is connected with the pure nitrogen gas import of secondary tower condenser by pipeline.
Its purification step of equipment of dirty nitrogen purification nitrogen of the present utility model is as follows:
A) dirty nitrogen is introduced main heat exchanger and after uniform temperature, is sent into king-tower by the gas low temperature that backflows after compressor compresses;
B) dirty nitrogen enters after king-tower, carries out heat and mass from below to up at king-tower on column plate or filler with top-down liquid, tower top extract out a part of pressure nitrogen gas after main heat exchanger re-heat as product;
C) from king-tower bottom liquid nitrogen fraction out entered subcooler cross cold, a part is sent into king-tower condenser, the dirty nitrogen that king-tower condenser is evaporated is sent into secondary tower, this dirty nitrogen carries out heat and mass with top-down liquid from below to up at secondary tower on column plate or filler, the dirty nitrogen that tower top produces is through secondary tower condenser condenses, a condensed liquid part is returned to secondary tower as phegma, and another part liquid is squeezed into king-tower as phegma;
D) another part subcooler is crossed cold liquid nitrogen fraction mixing secondary tower bottom out liquid nitrogen fraction out and is sent into secondary tower condenser, and the dirty nitrogen that secondary tower condenser is evaporated is sent into dirty nitrogen compressor and recycled after subcooler and main heat exchanger re-heat;
E) in order to maintain the balance of cold, pour into a part of liquid nitrogen at the top of king-tower and remove to maintain cold as king-tower phegma.
Preferably, the dirty nitrogen waste gas of user's discharge is as unstripped gas; The liquid nitrogen fraction that the condenser low-temperature receiver of king-tower and secondary tower adopts king-tower bottom to produce; The dirty nitrogen that the condenser of king-tower is evaporated is as the source of the gas of secondary tower; The liquid part condensing in the condenser of secondary tower is returned to king-tower as phegma; Cold directly supplements and maintains with liquid nitrogen, has cancelled expander refrigeration.
In the utility model, the liquid of heat and mass is common liquid nitrogen in the time of top of tower, and it,, by after column plate heat and mass, becomes oxygen enrichment liquid nitrogen fraction to tower bottom.
The utility model utilizes dirty nitrogen as unstripped gas, because higher than nitrogen content in air in dirty nitrogen, the therefore nitrogen-making device of same scale, adopts dirty nitrogen higher than the nitrogen that adopts air to produce, and adopts this technological process, and its nitrogen recovery rate is up to more than 90%.
The utility model has increased the equipment of dirty nitrogen purification nitrogen on the basis of original air separation unit, the liquid nitrogen fraction that dirty nitrogen is produced as the king-tower bottom that is recycled of toxic emission, a part is as the low-temperature receiver of king-tower condenser, the dirty nitrogen that king-tower condenser is evaporated is as the unstripped gas of secondary tower, thereby reduce like this evaporation side temperature of king-tower condenser, reduce pneumatics unit pressure at expulsion, thereby effectively reduce energy consumption index.
Brief description of the drawings
Fig. 1 is the process chart of dirty nitrogen purification nitrogen gas preparing of the present utility model.
Mark in figure: 1. dirty nitrogen compressor, 2. main heat exchanger, 3. king-tower, 4. king-tower condenser, 5. subcooler, 6. secondary tower, 7. secondary tower condenser.
Detailed description of the invention
Below in conjunction with accompanying drawing, the utility model is described in further detail, but this should be interpreted as to the scope of above-mentioned theme of the present utility model only limits to following embodiment.
As shown in Figure 1, the equipment of the dirty nitrogen purification of a kind of high extraction and low energy consumption nitrogen, comprise dirty nitrogen compressor 1, be connected to the main heat exchanger 2 on dirty nitrogen compressor 1, be connected to the king-tower 3 on main heat exchanger 2, be connected to secondary tower 6 and subcooler 5 on king-tower 3, king-tower 3 is provided with king-tower condenser 4, secondary tower 6 is provided with secondary tower condenser 7, the dirty nitrogen outlet of dirty nitrogen compressor 1 is connected with the dirty nitrogen inlet of main heat exchanger 2 by pipeline, the dirty nitrogen outlet of main heat exchanger 2 is connected with the dirty nitrogen inlet of king-tower 3 by pipeline, the pure nitrogen gas outlet of king-tower 3 is connected with the pure nitrogen gas import of main heat exchanger 2 by pipeline, the liquid nitrogen fraction outlet of king-tower 3 is connected with the liquid nitrogen fraction import of subcooler 5 by pipeline, the liquid nitrogen fraction outlet of subcooler 5 is connected with the liquid nitrogen fraction import of king-tower condenser 4 and the liquid nitrogen fraction import of secondary tower condenser 7 by pipeline respectively, the liquid nitrogen fraction outlet of secondary tower 6 is connected with the liquid nitrogen fraction import of secondary tower condenser 7 by pipeline, the dirty nitrogen outlet of king-tower condenser 4 is connected with the dirty nitrogen inlet of secondary tower 6 by pipeline, the dirty nitrogen outlet of secondary tower condenser 7 is connected with the dirty nitrogen inlet of dirty nitrogen compressor 1 with after main heat exchanger 2 through subcooler 5 successively by pipeline, the liquid nitrogen fraction outlet of king-tower condenser 4 is connected with the liquid nitrogen fraction import of king-tower 3 by pipeline, the liquid nitrogen fraction outlet of secondary tower condenser 7 is connected with the liquid nitrogen fraction import of secondary tower 6 and the liquid nitrogen fraction import of king-tower 3 by pipeline respectively.The pure nitrogen gas outlet of king-tower 3 is also connected with the pure nitrogen gas import of king-tower condenser 4 by pipeline, and the pure nitrogen gas outlet of secondary tower 6 is connected with the pure nitrogen gas import of secondary tower condenser 7 by pipeline.
In the utility model figure, CWN is dirty nitrogen compressor; E1 is main heat exchanger; C1 is king-tower; K1 is king-tower condenser; E2 is subcooler; C2 is secondary tower; K2 is secondary tower condenser.Those parts are the common components of making nitrogen gas preparing in prior art, describe therefore those parts are not done to further expansion.
The purifying technique flow process of dirty nitrogen purification nitrogen gas preparing of the present utility model is as follows:
From the former free point of dirty nitrogen waste gas emitting of user mix the brilliant nitrogen compressor compression of dirty nitrogen that this device returns laggard enter main heat exchanger, backflowed gas cooled to approaching the laggard tower bottom of becoming owner of of dew-point temperature.In king-tower, through rectifying, obtain pure nitrogen gas at tower top, at the bottom of tower, obtain oxygen enrichment liquid nitrogen fraction.Oxygen enrichment liquid nitrogen fraction is crossed cold rear portion throttling and is entered king-tower condenser and nitrogen phase-change heat-exchange through subcooler, and oxygen enrichment liquid nitrogen fraction is evaporated to dirty nitrogen, after nitrogen condensation as king-tower phegma.
The dirty nitrogen being evaporated by king-tower condenser overhead enters secondary tower bottom, through rectifying, obtains Low Voltage Pure nitrogen at tower top, obtains oxygen enrichment liquid nitrogen fraction at the bottom of tower.Liquid nitrogen fraction enters secondary tower condenser and nitrogen phase-change heat-exchange after mixing with the remainder liquid nitrogen fraction of high-pressure tower bottom after subcooler is crossed cold throttling, the dirty vaporized nitrogen of oxygen enrichment is the dirty nitrogen of low pressure, nitrogen condensation rear section is as secondary tower phegma, and remainder is assisted rectifying through the laggard top of tower of becoming owner of of liquid nitrogen pump supercharging.
Product nitrogen gas is drawn from king-tower tower top, and cooling box after main heat exchanger re-heat directly enters user's nitrogen pipe network.
The dirty nitrogen of low pressure cooling box after subcooler and main heat exchanger re-heat of being drawn by secondary tower condenser overhead, returns to nitrogen compressor import as unstripped gas.
The cold of device is to be maintained by liquid nitrogen.The king-tower top that the pure liquid nitrogen supplementing enters in ice chest provides cold, simultaneously auxiliary rectifying.
Claims (2)
1. the equipment of the dirty nitrogen purification of a high extraction and low energy consumption nitrogen, it is characterized in that: it comprises dirty nitrogen compressor, be connected to the main heat exchanger on dirty nitrogen compressor, be connected to the king-tower on main heat exchanger, be connected to secondary tower and subcooler on king-tower, described king-tower is provided with king-tower condenser, described secondary tower is provided with secondary tower condenser, the dirty nitrogen outlet of described dirty nitrogen compressor is connected with the dirty nitrogen inlet of main heat exchanger by pipeline, the dirty nitrogen outlet of described main heat exchanger is connected with the dirty nitrogen inlet of king-tower by pipeline, the pure nitrogen gas outlet of described king-tower is connected with the pure nitrogen gas import of main heat exchanger by pipeline, the liquid nitrogen fraction outlet of described king-tower is connected with the liquid nitrogen fraction import of subcooler by pipeline, the liquid nitrogen fraction outlet of described subcooler is connected with the liquid nitrogen fraction import of king-tower condenser and the liquid nitrogen fraction import of secondary tower condenser by pipeline respectively, the liquid nitrogen fraction outlet of described secondary tower is connected with the liquid nitrogen fraction import of secondary tower condenser by pipeline, the dirty nitrogen outlet of described king-tower condenser is connected with the dirty nitrogen inlet of secondary tower by pipeline, the dirty nitrogen outlet of described secondary tower condenser is passed subcooler and is connected with the dirty nitrogen inlet of dirty nitrogen compressor after main heat exchanger successively by pipeline, the liquid nitrogen fraction outlet of described king-tower condenser is connected with the liquid nitrogen fraction import of king-tower by pipeline, the liquid nitrogen fraction outlet of described secondary tower condenser is connected with the liquid nitrogen fraction import of secondary tower and the liquid nitrogen fraction import of king-tower by pipeline respectively.
2. the equipment of the dirty nitrogen purification of a kind of high extraction according to claim 1 and low energy consumption nitrogen, it is characterized in that: the pure nitrogen gas outlet of described king-tower is also connected with the pure nitrogen gas import of king-tower condenser by pipeline, the pure nitrogen gas outlet of described secondary tower is connected with the pure nitrogen gas import of secondary tower condenser by pipeline.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420335643.7U CN203940689U (en) | 2014-06-23 | 2014-06-23 | The equipment of the dirty nitrogen purification of high extraction and low energy consumption nitrogen |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420335643.7U CN203940689U (en) | 2014-06-23 | 2014-06-23 | The equipment of the dirty nitrogen purification of high extraction and low energy consumption nitrogen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203940689U true CN203940689U (en) | 2014-11-12 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420335643.7U Withdrawn - After Issue CN203940689U (en) | 2014-06-23 | 2014-06-23 | The equipment of the dirty nitrogen purification of high extraction and low energy consumption nitrogen |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203940689U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104048478A (en) * | 2014-06-23 | 2014-09-17 | 浙江大川空分设备有限公司 | Device for extracting pure nitrogen from polluted nitrogen high in extraction rate and low in energy consumption and extracting method thereof |
-
2014
- 2014-06-23 CN CN201420335643.7U patent/CN203940689U/en not_active Withdrawn - After Issue
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104048478A (en) * | 2014-06-23 | 2014-09-17 | 浙江大川空分设备有限公司 | Device for extracting pure nitrogen from polluted nitrogen high in extraction rate and low in energy consumption and extracting method thereof |
| CN104048478B (en) * | 2014-06-23 | 2016-03-30 | 浙江大川空分设备有限公司 | The equipment of high extraction and the dirty nitrogen purification nitrogen of low energy consumption and extracting method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| AV01 | Patent right actively abandoned |
Granted publication date: 20141112 Effective date of abandoning: 20160330 |
|
| AV01 | Patent right actively abandoned |
Granted publication date: 20141112 Effective date of abandoning: 20160330 |
|
| C25 | Abandonment of patent right or utility model to avoid double patenting |