CN203923157U - A kind of white wine decompression distillation system - Google Patents

A kind of white wine decompression distillation system Download PDF

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Publication number
CN203923157U
CN203923157U CN201420205878.4U CN201420205878U CN203923157U CN 203923157 U CN203923157 U CN 203923157U CN 201420205878 U CN201420205878 U CN 201420205878U CN 203923157 U CN203923157 U CN 203923157U
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China
Prior art keywords
retort
vacuum
heating steam
condenser
distillation
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CN201420205878.4U
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Chinese (zh)
Inventor
郭波
谢敏
何国良
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GUANGDONG SHIWAN WINE GROUP Co Ltd
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GUANGDONG SHIWAN WINE GROUP Co Ltd
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Abstract

The utility model discloses a kind of white wine decompression distillation system, comprise retort and the condenser being communicated with described retort sealing, the bottom of described condenser connects wine liquid basin by pipeline, and this white wine decompression distillation system also comprises vacuum buffer tank and vacuum pump; The vacuum distilling system that is communicated with successively and forms sealing at retort described in vacuum distillation process, condenser, wine liquid basin and vacuum buffer tank, and the vacuum pump being connected with described vacuum buffer tank provides negative pressure of vacuum environment for this vacuum distilling system.The technical solution of the utility model reduces the temperature of distillation significantly, and by the reasonable setting of decompression distillation system structure being made to large as far as possible the distillating of low-boiling point material in soybean-flavor liquor, other cannot distillate high boiling substance and also can under the condition of decompression, distillate under normal pressure, change the formation of each composition in original vegetarian wine, formed a kind of local flavor of uniqueness.

Description

A kind of white wine decompression distillation system
Technical field
The utility model relates to fermentation technical field, relates in particular to a kind of white wine decompression distillation system and the distillating method in wine industry, used.
Background technology
The temperature when vapour pressure that the boiling temperature of liquid refers to liquid equates with external pressure.When external pressure reduces, its boiling temperature decreases.In distillation procedure, if water distilling apparatus is connected on a set of depressurized system, before distillation starts, first make whole system pressure decreased to ten part to tens/mono-that only have normal pressure, this type organic just can distill at the temperature much lower compared with its normal boiling point so.Underpressure distillation mode is more extensive in petrochemical industry application, but less in the application of food service industry.Soybean-flavor liquor is a kind of very popular alcohol product, in prior art, such white wine generally adopts the method for air distillation to make, and adopt existing air distillation method to distill the interpretation of result from judging, generally believe the just slightly punching of air distillation, there is slight burnt odor, taste is assorted, can not meet the growing taste demand of people.
For the foregoing reasons, designing a kind of white wine decompression distillation system, can guarantee good temperature control effect, can be industry problem demanding prompt solution in the even rolling that is difficult for realizing under the condition of microbiological contamination white wine decompression distillation system body materials inside again.
Utility model content
In view of this, technical problem to be solved in the utility model is to provide a kind of white wine decompression distillation system and distillating method, reduce significantly the temperature of distillation, and pass through temperature, the isoparametric optimum combination of pressure in the optimization setting of decompression distillation system structure and vacuum distillation process, make large as far as possible the distillating of low-boiling point material in soybean-flavor liquor, other cannot distillate high boiling substance and also can under the condition of decompression, distillate under normal pressure, change the formation of each composition in original vegetarian wine, formed a kind of local flavor of uniqueness.
For solving the problems of the technologies described above, on the one hand, embodiment of the present utility model provides a kind of white wine decompression distillation system, comprise retort and the condenser being communicated with described retort sealing, the bottom of described condenser connects wine liquid basin by pipeline, this white wine decompression distillation system also comprises vacuum buffer tank, and described vacuum buffer tank one end is connected with described wine liquid basin by sealing-duct, and the other end is connected with vacuum pump by sealing-duct; The vacuum distilling system that is communicated with successively and forms sealing at retort described in vacuum distillation process, condenser, wine liquid basin and vacuum buffer tank, and the vacuum pump being connected with described vacuum buffer tank provides negative pressure of vacuum environment for this vacuum distilling system;
Between described retort and condenser, by the condensing tower seal of tube, be communicated with, described condensing tower pipe is bending setting, one end of described condensing tower pipe is connected with the top of described retort, the other end of described condensing tower pipe is connected with the condenser inlet mouth that is arranged at described condenser overhead one side, the kink of condensing tower pipe is its vertex, and the height of this vertex is higher than the height of condenser inlet mouth;
On described retort, also offer manhole, heating steam entrance, condensed water level outlet, distiller's wort entrance and lees outlet, between described heating steam entrance and described condensation-water drain, be connected with steam-pipe; Thereby heat occurs the distiller's wort in the heating steam in steam-pipe and retort transmits distiller's wort in heating retort, the distiller's wort that the described distiller's wort entrance external world obtains after zymamsis; The raffinate that distiller's wort produces after completing underpressure distillation is discharged retort by lees outlet; On described retort, be also provided with by maintaining and changing the vacuum valve that prevents that counterweight maintained and changed vacuum tightness in retort;
In described condenser, be provided with snakelike water-cooled tube of arranging, the cooling water inlet of this water-cooled tube is positioned at the central authorities of described condenser bottom, and the cooling water outlet of described water-cooled tube is positioned at the edge of described condenser bottom; The water coolant containing in wine fraction and described water-cooled tube that described retort enters condenser carries out heat exchange and is condensed into wine liquid, and wine liquid enters in wine liquid basin by connecting the sealing-duct of described condenser and wine liquid basin.
Preferably, described heating steam entrance comprises direct heating steam-in and indirect heating steam-in, described indirect heating steam-in is connected with described condensation-water drain, between indirect heating steam-in and condensation-water drain, be connected with indirect heating steam-pipe, this indirect heating steam-pipe is snakelike and is arranged in described retort; At distiller's wort, add after retort, distillation temperature when distiller's wort in retort is heated in the heating steam being entered by direct direct heating steam-in and indirect heating steam-in jointly to pressure distillation, opening vacuum pump enters after underpressure distillation operation, cut off the heating steam of direct heating steam-in, the distillation temperature when heating steam entering by indirect heating steam-in maintains underpressure distillation.
On the other hand, the utility model also provides a kind of white wine vacuum distillation method, this white wine vacuum distillation method is realized the underpressure distillation of white wine by white wine decompression distillation system, described white wine decompression distillation system, comprise retort and the condenser being communicated with described retort sealing, the bottom of described condenser connects wine liquid basin by pipeline, this white wine decompression distillation system also comprises vacuum buffer tank, described vacuum buffer tank one end is connected with described wine liquid basin by sealing-duct, and the other end is connected with vacuum pump by sealing-duct; The vacuum distilling system that is communicated with successively and forms sealing at retort described in vacuum distillation process, condenser, wine liquid basin and vacuum buffer tank, and the vacuum pump being connected with described vacuum buffer tank provides negative pressure of vacuum environment for this vacuum distilling system;
Between described retort and condenser, by the condensing tower seal of tube, be communicated with, described condensing tower pipe is bending setting, one end of described condensing tower pipe is connected with the top of described retort, the other end of described condensing tower pipe is connected with the condenser inlet mouth that is arranged at described condenser overhead one side, the kink of condensing tower pipe is its vertex, and the height of this vertex is higher than the height of condenser inlet mouth;
On described retort, also offer manhole, heating steam entrance, condensed water level outlet, distiller's wort entrance and lees outlet, between described heating steam entrance and described condensation-water drain, be connected with steam-pipe; Thereby heat occurs the distiller's wort in the heating steam in steam-pipe and retort transmits distiller's wort in heating retort, and the raffinate that distiller's wort produces after completing underpressure distillation is discharged retort by lees outlet; On described retort, be also provided with by maintaining and changing the vacuum valve that prevents that counterweight maintained and changed vacuum tightness in retort;
In described condenser, be provided with snakelike water-cooled tube of arranging, the cooling water inlet of this water-cooled tube is positioned at the central authorities of described condenser bottom, and the cooling water outlet of described water-cooled tube is positioned at the edge of described condenser bottom; The water coolant containing in wine fraction and described water-cooled tube that described retort enters condenser carries out heat exchange and is condensed into wine liquid, and wine liquid enters in wine liquid basin by connecting the sealing-duct of described condenser and wine liquid basin;
Described heating steam entrance comprises direct heating steam-in and indirect heating steam-in, described indirect heating steam-in is connected with described condensation-water drain, between indirect heating steam-in and condensation-water drain, be connected with indirect heating steam-pipe, this indirect heating steam-pipe is snakelike and is arranged in described retort; At distiller's wort, add after retort, distillation temperature when distiller's wort in retort is heated in the heating steam being entered by direct direct heating steam-in and indirect heating steam-in jointly to pressure distillation, opening vacuum pump enters after underpressure distillation operation, cut off the heating steam of direct heating steam-in, the distillation temperature when heating steam entering by indirect heating steam-in maintains underpressure distillation;
This white wine vacuum distillation method specifically comprises the steps:
Operation before step 1, underpressure distillation:
(1) before underpressure distillation, first start condenser cooling water water supplying pump, check water pump pressure of supply water and discharge, check that all valves, the steam valve of distiller's wort delivery system can start to drop into distillation under good situations;
(2) close lees outlet valve, open distiller's wort inlet valve, toward the interior charging of retort, every rice steamer time distillation amount is not more than 3.5m 3or, forbid distiller's wort face to exceed set(ting)value;
(3) retort charging is complete, close distiller's wort inlet valve and pass through the fresh feed pump of distiller's wort inlet valve charging, open retort heating steam inlet valve and be heated to 40~60 ℃, then close direct heating steam-in valve, keep indirect heating steam-in valve opening, open wine storing jar valve, start distillation;
(4) in surge tank, add suitable quantity of water 0.05-0.10 m 3, vacuum tightness when whether the counterweight that prevents vacuum valve on inspection retort enough maintains underpressure distillation;
(5) before starting vacuum pump, guarantee that described retort, condenser, wine liquid basin and vacuum buffer tank are communicated with and form the vacuum distilling system of sealing successively, then open vacuum pump and make to maintain in vacuum distillation process the intrasystem vacuum tightness of vacuum distilling at-70kpa~-90kpa;
Step 2, underpressure distillation: maintain the intrasystem vacuum tightness of vacuum distilling between-70kpa~-90kpa, and the distiller's wort temperature maintaining in retort is carried out underpressure distillation between 40~60 ℃; When reach-90kpa of retort, prevent that vacuum valve from must start release, be that the counterweight that prevents vacuum valve meets the requirements of vacuum tightness, or close the valve on vacuum pump admission passage, suspend suction motor and restart again when lower than-70kpa.Circulating, this is operated to distillation end;
Step 3, underpressure distillation aftertreatment:
(1) first close after the valve of indirect heating steam-in, then close the cooling water valve of condenser;
(2) close successively the admission passage valve of vacuum pump, close water-supply line valve, pump remains in operation 1~2 minute, after discharge section working fluid, closes pump motor;
(3) slowly reduce and prevent that the counterweight of vacuum valve from shedding vacuum gradually to normal atmosphere step by step, open lees outlet valve, emit poor water, finally close the valve on wine storing jar.
Compared with prior art, the technical solution of the utility model at least has following beneficial effect:
White wine decompression distillation system of the present utility model and distillating method reduce the temperature of distillation significantly, and pass through temperature, the isoparametric optimum combination of pressure in the optimization setting of decompression distillation system structure and vacuum distillation process, make large as far as possible the distillating of low-boiling point material in soybean-flavor liquor, other cannot distillate high boiling substance and also can under the condition of decompression, distillate under normal pressure, change the formation of each composition in original vegetarian wine, formed a kind of local flavor of uniqueness.
Accompanying drawing explanation
Fig. 1 is the structural representation of the white wine decompression distillation system of the utility model embodiment.
Embodiment
Below in conjunction with accompanying drawing, describe the utility model in detail, it illustrates principle of the present utility model as the part of this specification sheets by embodiment, and other aspects of the present utility model, feature and advantage thereof will become very clear by this detailed description.In the accompanying drawing of institute's reference, in different figure, same or analogous parts represent by identical drawing reference numeral, and accompanying drawing does not produce restriction to the global design of white wine decompression distillation system of the present utility model.
As shown in Figure 1, embodiment 1 of the present utility model provides a kind of white wine decompression distillation system, comprise retort 10 and the condenser 20 being communicated with retort sealing, the bottom of condenser connects wine liquid basin 30 by pipeline, this white wine decompression distillation system also comprises vacuum buffer tank 40, vacuum buffer tank one end is connected with wine liquid basin 30 by sealing-duct, and the other end is connected with vacuum pump 50 by sealing-duct; In vacuum distillation process, retort 10, condenser 20, wine liquid basin 30 and vacuum buffer tank 40 are communicated with and form the vacuum distilling system of sealing successively, and the vacuum pump 50 being connected with vacuum buffer tank provides negative pressure of vacuum environment for this vacuum distilling system.During specific implementation, vacuum pump maintains the intrasystem vacuum tightness of vacuum distilling at-70kpa~-90kpa in vacuum distillation process.
In the utility model preferred embodiment, between retort 10 and condenser 20, by 60 sealings of condensing tower pipe, be communicated with, condensing tower pipe 60 is bending setting, one end of condensing tower pipe 60 is connected with the top of retort 10, the other end of condensing tower pipe 60 is connected with the condenser inlet mouth 21 that is arranged at condenser 20 top one sides, the kink 61 of condensing tower pipe 60 is its vertex, and the height of this vertex is higher than the height of condenser inlet mouth, thereby cut can be shunted and reflux admirably.
On retort, also offer manhole, heating steam entrance 12, condensed water level outlet 13, distiller's wort entrance 14 and lees outlet 15, between heating steam entrance 12 and condensation-water drain 13, be connected with steam-pipe; Thereby heat occurs the distiller's wort in the heating steam in steam-pipe and retort transmits distiller's wort in heating retort, and the heating steam in vacuum distillation process in retort maintains 40~60 ℃ by the distiller's wort temperature in retort and carries out underpressure distillation; The distiller's wort that distiller's wort entrance 14 external worlds obtain after zymamsis; The raffinate that distiller's wort produces after completing underpressure distillation is discharged retort by lees outlet 15; On retort, be also provided with and prevent vacuum valve 17, by maintaining and changing the counterweight that prevents vacuum valve 17, maintain and change vacuum tightness in retort.
In condenser 20, be provided with snakelike water-cooled tube of arranging, the cooling water inlet 22 of this water-cooled tube is positioned at the central authorities of condenser bottom, and the cooling water outlet 23 of water-cooled tube is positioned at the edge of condenser bottom; The water coolant containing in wine fraction and water-cooled tube that retort enters condenser carries out heat exchange and is condensed into wine liquid, and wine liquid enters in wine liquid basin with the sealing-duct of wine liquid basin 30 by connecting condenser 20.
In the utility model preferred embodiment, heating steam entrance 12 comprises direct heating steam-in 121 and indirect heating steam-in 122, indirect heating steam-in 122 is connected with condensation-water drain 13, between indirect heating steam-in 122 and condensation-water drain, be connected with indirect heating steam-pipe, this indirect heating steam-pipe is snakelike and is arranged in retort.At distiller's wort, add after retort 10, distillation temperature when distiller's wort in retort 10 is heated in the heating steam being entered by direct direct heating steam-in 121 and indirect heating steam-in 122 jointly to pressure distillation, opening vacuum pump enters after underpressure distillation operation, cut off the heating steam of direct heating steam-in 121, the distillation temperature when heating steam entering by indirect heating steam-in 122 maintains underpressure distillation.
Above-mentioned white wine decompression distillation system is by following operation steps, to realize the underpressure distillation of white wine:
Operation before step 1, underpressure distillation:
(1) before underpressure distillation, first start condenser cooling water water supplying pump, check water pump pressure of supply water and discharge, check that all valves, the steam valve of distiller's wort delivery system can start to drop into distillation under good situations;
(2) close lees outlet valve, open distiller's wort inlet valve, toward the interior charging of retort, every rice steamer time distillation amount is not more than 3.5m 3or, forbid distiller's wort face to exceed set(ting)value;
(3) retort charging is complete, close distiller's wort inlet valve and pass through the fresh feed pump of distiller's wort inlet valve charging, open retort heating steam inlet valve and be heated to 40~60 ℃, then close direct heating steam-in valve, keep indirect heating steam-in valve opening, open wine storing jar valve, start distillation;
(4) in surge tank, add suitable quantity of water 0.05-0.10 m 3, vacuum tightness when whether the counterweight that prevents vacuum valve on inspection retort enough maintains underpressure distillation;
(5) before starting vacuum pump, guarantee that described retort, condenser, wine liquid basin and vacuum buffer tank are communicated with and form the vacuum distilling system of sealing successively, then open vacuum pump and make to maintain in vacuum distillation process the intrasystem vacuum tightness of vacuum distilling at-70kpa~-90kpa;
Step 2, underpressure distillation: maintain the intrasystem vacuum tightness of vacuum distilling between-70kpa~-90kpa, and the distiller's wort temperature maintaining in retort is carried out underpressure distillation between 40~60 ℃; When reach-90kpa of retort, prevent that vacuum valve from must start release, be that the counterweight that prevents vacuum valve meets the requirements of vacuum tightness, or close the valve on vacuum pump admission passage, suspend suction motor and restart again when lower than-70kpa.Circulating, this is operated to distillation end;
Step 3, underpressure distillation aftertreatment:
(1) first close after the valve of indirect heating steam-in, then close the cooling water valve of condenser;
(2) close successively the admission passage valve of vacuum pump, close water-supply line valve, pump remains in operation 1~2 minute, after discharge section working fluid, closes pump motor;
(3) slowly reduce and prevent that the counterweight of vacuum valve from shedding vacuum gradually to normal atmosphere step by step, open lees outlet valve, emit poor water, finally close the valve on wine storing jar.
Compared with prior art, the white wine decompression distillation system that above-described embodiment discloses reduces the temperature of distillation significantly, and pass through temperature, the isoparametric optimum combination of pressure in the optimization setting of decompression distillation system structure and vacuum distillation process, make large as far as possible the distillating of low-boiling point material in soybean-flavor liquor, other cannot distillate high boiling substance and also can under the condition of decompression, distillate under normal pressure, change the formation of each composition in original vegetarian wine, formed a kind of local flavor of uniqueness.
The above is preferred implementation of the present utility model; it should be pointed out that for those skilled in the art, do not departing under the prerequisite of the utility model principle; can also make some improvements and modifications, these improvements and modifications are also considered as protection domain of the present utility model.

Claims (2)

1. a white wine decompression distillation system, comprises retort and the condenser being communicated with described retort sealing, and the bottom of described condenser connects wine liquid basin by pipeline, it is characterized in that:
This white wine decompression distillation system also comprises vacuum buffer tank, and described vacuum buffer tank one end is connected with described wine liquid basin by sealing-duct, and the other end is connected with vacuum pump by sealing-duct; The vacuum distilling system that is communicated with successively and forms sealing at retort described in vacuum distillation process, condenser, wine liquid basin and vacuum buffer tank, and the vacuum pump being connected with described vacuum buffer tank provides negative pressure of vacuum environment for this vacuum distilling system;
Between described retort and condenser, by the condensing tower seal of tube, be communicated with, described condensing tower pipe is bending setting, one end of described condensing tower pipe is connected with the top of described retort, the other end of described condensing tower pipe is connected with the condenser inlet mouth that is arranged at described condenser overhead one side, the kink of condensing tower pipe is its vertex, and the height of this vertex is higher than the height of condenser inlet mouth;
On described retort, also offer manhole, heating steam entrance, condensed water level outlet, distiller's wort entrance and lees outlet, between described heating steam entrance and described condensation-water drain, be connected with steam-pipe; Thereby heat occurs the distiller's wort in the heating steam in steam-pipe and retort transmits distiller's wort in heating retort, the distiller's wort that the described distiller's wort entrance external world obtains after zymamsis; The raffinate that distiller's wort produces after completing underpressure distillation is discharged retort by lees outlet; On described retort, be also provided with by maintaining and changing the vacuum valve that prevents that counterweight maintained and changed vacuum tightness in retort;
In described condenser, be provided with snakelike water-cooled tube of arranging, the cooling water inlet of this water-cooled tube is positioned at the central authorities of described condenser bottom, and the cooling water outlet of described water-cooled tube is positioned at the edge of described condenser bottom; The water coolant containing in wine fraction and described water-cooled tube that described retort enters condenser carries out heat exchange and is condensed into wine liquid, and wine liquid enters in wine liquid basin by connecting the sealing-duct of described condenser and wine liquid basin.
2. white wine decompression distillation system according to claim 1, it is characterized in that: described heating steam entrance comprises direct heating steam-in and indirect heating steam-in, described indirect heating steam-in is connected with described condensation-water drain, between indirect heating steam-in and condensation-water drain, be connected with indirect heating steam-pipe, this indirect heating steam-pipe is snakelike and is arranged in described retort; At distiller's wort, add after retort, distillation temperature when distiller's wort in retort is heated in the heating steam being entered by direct direct heating steam-in and indirect heating steam-in jointly to pressure distillation, opening vacuum pump enters after underpressure distillation operation, cut off the heating steam of direct heating steam-in, the distillation temperature when heating steam entering by indirect heating steam-in maintains underpressure distillation.
CN201420205878.4U 2014-04-25 2014-04-25 A kind of white wine decompression distillation system Expired - Lifetime CN203923157U (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106754184A (en) * 2017-02-15 2017-05-31 合肥步之道商贸有限公司 A kind of liquor distilling apparatus
CN107653165A (en) * 2016-07-25 2018-02-02 田高 White spirit by solid state method tunnel type stepwise distillation smart machine
CN111269794A (en) * 2020-04-08 2020-06-12 劲牌有限公司 Atmospheric and vacuum distillation method for solid Xiaoqu liquor
CN111560298A (en) * 2020-05-14 2020-08-21 宜昌杰威机械设备有限公司 Intelligent brewing system for Maotai-flavor liquor
CN113462511A (en) * 2021-07-19 2021-10-01 江苏今世缘酒业股份有限公司 Fermented glutinous rice distillation system

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107653165A (en) * 2016-07-25 2018-02-02 田高 White spirit by solid state method tunnel type stepwise distillation smart machine
CN106754184A (en) * 2017-02-15 2017-05-31 合肥步之道商贸有限公司 A kind of liquor distilling apparatus
CN111269794A (en) * 2020-04-08 2020-06-12 劲牌有限公司 Atmospheric and vacuum distillation method for solid Xiaoqu liquor
CN111269794B (en) * 2020-04-08 2021-07-20 劲牌有限公司 Atmospheric and vacuum distillation method for solid Xiaoqu liquor
CN111560298A (en) * 2020-05-14 2020-08-21 宜昌杰威机械设备有限公司 Intelligent brewing system for Maotai-flavor liquor
CN113462511A (en) * 2021-07-19 2021-10-01 江苏今世缘酒业股份有限公司 Fermented glutinous rice distillation system

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