CN203916115U - A kind of dirty alcohol distillation column - Google Patents

A kind of dirty alcohol distillation column Download PDF

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Publication number
CN203916115U
CN203916115U CN201420393257.3U CN201420393257U CN203916115U CN 203916115 U CN203916115 U CN 203916115U CN 201420393257 U CN201420393257 U CN 201420393257U CN 203916115 U CN203916115 U CN 203916115U
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CN
China
Prior art keywords
valve member
tower
chamber
charging aperture
pump
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Expired - Lifetime
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CN201420393257.3U
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Chinese (zh)
Inventor
乔仁蛟
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QINGDAO WANTUMING BIOLOGICAL PRODUCTS Co Ltd
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QINGDAO WANTUMING BIOLOGICAL PRODUCTS Co Ltd
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Priority to CN201420393257.3U priority Critical patent/CN203916115U/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/10Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working

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  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model discloses a kind of dirty alcohol distillation column, comprise feed pump, valve member a, valve member b, heat exchanger a, heating clamber a, heating clamber b, salt discharge valve a, salt discharge valve b, vaporization chamber a, vaporization chamber b, tower a, heat exchanger b, moisture trap a, reflux pump a, cooler, tower b, condenser a, moisture trap b, reflux pump b, vavuum pump, condenser b, collecting tank, steam trap, this dirt alcohol distillation column is used titanium material to solve etching problem on the parts that contact with dirty alcohol stoste, by steam heat being recycled to the high problem of energy consumption that solved, dirty alcohol stoste form with alcohol steam after the evaporation of tower external heat enters tower, avoided salt pair tower corrosion, it is high that equipment reclaims dirty alcohol efficiency, output is large.

Description

A kind of dirty alcohol distillation column
Technical field
The utility model relates to a kind of dirty alcohol distillation column, is exactly specifically the dirty alcohol distillation column that a kind of low energy consumption and efficiency are high.
Background technology
In industry manufacture process, can produce a lot of dirty alcohol, in common dirty alcohol, mainly contain the impurity such as salt, water soluble protein, concentration is 65% left and right, and has certain corrosivity.Mainly there is the problems such as perishable, energy consumption is high, alcohol organic efficiency is not high, yield poorly in traditional dirty alcohol reclaimer.
Summary of the invention
The purpose of this utility model is to provide a kind of dirty alcohol distillation column, this dirt alcohol distillation column is used titanium material to solve etching problem on the parts that contact with dirty alcohol stoste, by steam heat being recycled to the high problem of energy consumption that solved, dirty alcohol stoste form with alcohol steam after the evaporation of tower external heat enters tower, avoided salt pair tower corrosion, equipment reclaims that dirty alcohol efficiency is high, output is large.
The technical scheme in the invention for solving the technical problem is: a kind of dirty alcohol distillation column, comprise feed pump 1, valve member a2, valve member b3, heat exchanger a4, heating clamber a5, heating clamber b6, salt discharge valve a7, salt discharge valve b8, vaporization chamber a9, vaporization chamber b10, tower a11, heat exchanger b12, moisture trap a13, reflux pump a14, cooler 15, tower b16, condenser a17, moisture trap b18, reflux pump b19, vavuum pump 20, condenser b21, collecting tank 22, pump 23, exhaust outlet 24, valve member c25, valve member d26, valve member e27, valve member f28, valve member g29, valve member h30, valve member i31, valve member j32, valve member k33, valve member m34, valve member n35, steam trap 36,
There are two chambeies that are heated heat exchanger a4 inside, a heating chamber, heating clamber a5, heating clamber b6, heat exchanger b12, tower a11, there is the chamber that is heated tower b16 inside, a heating chamber, feed pump 1 charging aperture connects dirty wine fine supplement tube, feed pump 1 discharge port end is divided into two-way, two-way is connected respectively the charging aperture in inner two chambeies that are heated of heat exchanger a4 with valve member b3 by valve member a2, two chamber discharging openings that are heated connect be respectively the heated charging aperture in chamber of heating clamber a5 and heating clamber b6 in heat exchanger a4, in heat exchanger a4, heating chamber import connects tower b16 waste discharge water pipe by valve member n35, in heat exchanger a4, heating chamber outlet connects outside sewage disposal device, the be heated bottom in chamber of heating clamber a5 and heating clamber b6 inside is respectively arranged with salt discharge valve a7 and salt discharge valve b8, be heated chamber discharging opening of heating clamber a5 connects vaporization chamber a9 charging aperture, vaporization chamber a9 top discharge mouth connects the tower a11 chamber charging aperture that is heated, vaporization chamber a9 bottom return duct connects the heating clamber a5 chamber charging aperture that is heated, be heated chamber discharging opening of heating clamber b6 connects vaporization chamber b10 charging aperture, vaporization chamber b10 top discharge mouth connects the tower b16 chamber charging aperture that is heated, and vaporization chamber b10 bottom return duct connects the heating clamber b6 chamber charging aperture that is heated,
Be heated chamber discharging opening of tower a11 top connects heat exchanger b12 heating chamber charging aperture, heat exchanger b12 heating chamber discharging opening connects moisture trap a13 charging aperture, the import of heat exchanger b12 heating chamber and the bottom and the top that export the heating chamber that is connected respectively tower b16, moisture trap a13 bottom discharge mouth connects reflux pump a14 charging aperture, and moisture trap a13 top discharge mouth connects condenser b21 charging aperture; Reflux pump a14 discharging opening is divided into two-way, and a road connects by connecting the tower a11 chamber charging aperture that is heated after valve member g29, leads up to after valve member h30 and connects cooler 15 charging apertures; A pipeline communication tower b16 waste discharge mouth of a river is passed through by steam trap 36 in the waste discharge mouth of a river, tower a11 bottom; The tower b16 chamber discharging opening that is heated connects moisture trap b18 charging aperture after by condenser a17, the waste gas outlet at moisture trap b18 top connects condenser b21 charging aperture through vavuum pump 20, condenser b21 discharging opening connects collecting tank 22 charging apertures, collecting tank 22 upper ends are provided with exhaust outlet 24, collecting tank 22 bottom discharge mouths are successively by connecting moisture trap b18 charging aperture after pump 23, valve member j32, and moisture trap b18 bottom discharge mouth connects reflux pump b19 charging aperture; Reflux pump b19 discharging opening is divided into two-way, leads up to and connects the tower b16 chamber charging aperture that is heated after valve member i31, and a road connects cooler 15 charging apertures;
Whole dirty alcohol distillation column heats by steam-out (SO), steam inlet is divided into three tunnels after by valve member c25, the valve member d26 of leading up to connects the heating chamber import of heating clamber b6, and the valve member e27 of leading up to connects the heating chamber import of heating clamber a5, and the valve member f28 of leading up to connects the import of tower a11 heating chamber; Heating clamber a5 is connected respectively tower a11 and the import of tower b16 heating chamber after docking with the heating chamber outlet of heating clamber b6 with valve member m34 by valve member k33.
As optimization, described valve member a2, valve member b3, valve member c25, valve member d26, valve member e27, valve member f28, valve member g29, valve member h30, valve member i31, valve member j32, valve member k33, valve member m34, valve member n35, for leading to magnetic valve only by Electromagnetic Control.
As optimization, described pump 1, reflux pump a14, reflux pump b19, vavuum pump 20, pump 23, be any one in single-screw (single screw) pump, Quimby pump, centrifugal pump, high-pressure pump, measuring pump.
As optimization, described feed pump 1, valve member a2, valve member b3, heat exchanger a4, heating clamber a5, heating clamber b6, salt discharge valve a7, salt discharge valve b8, vaporization chamber a9, vaporization chamber b10 and be all provided with titanium coating or adopt the processing of titanium material with the connecting line between upper-part and dirty Ethanol Exposure face, recovery tower miscellaneous part adopts 304 stainless steels processing.
As optimization, described tower a11, tower b16 are bubble column structure.
The beneficial effects of the utility model are: compared with prior art, a kind of dirty alcohol distillation column of the present utility model, has solved equipment corrosion problem, and energy consumption is low, efficiency is high, output is large.
Accompanying drawing explanation
Fig. 1 is the utility model overall construction drawing.
Wherein, 1 feed pump, 2 valve member a, 3 valve member b, 4 heat exchanger a, 5 heating clamber a, 6 heating clamber b, 7 salt discharge valve a, 8 salt discharge valve b, 9 vaporization chamber a, 10 vaporization chamber b, 11 tower a, 12 heat exchanger b, 13 moisture trap a, 14 reflux pump a, 15 coolers, 16 tower b, 17 condenser a, 18 moisture trap b, 19 reflux pump b, 20 vavuum pumps, 21 condenser b, 22 collecting tanks, 23 pumps, 24 exhaust outlets, 25 valve member c, 26 valve member d, 27 valve member e, 28 valve member f, 29 valve member g, 30 valve member h, 31 valve member i, 32 valve member j, 33 valve member k, 34 valve member m, 35 valve member n, 36 steam traps.
The specific embodiment
A kind of dirty alcohol distillation column as shown in Figure 1, heat exchanger a4, heating clamber a5, heating clamber b6, vaporization chamber a9, the vaporization chamber b10 heating clamber of dirty alcohol stoste outside tower a11, tower b16 enters tower a11, tower b16 with the form of alcohol steam after processing, and avoided the corrosion of salt pair tower.This alcohol distillation column adopts Double-Tower Structure, and tower a11 adopts Steam Heating; The Steam Heating that tower b16 can adopt tower a11 not utilize; The steam that heating clamber a5, heating clamber b6 do not utilize completely, then enter tower a11, tower b16 heats to tower; The waste water of tower b16 is drained and is advanced into heat exchanger a4 for giving dirty alcohol preheating, and the waste water of tower b16 is comprised of three parts: the one, and the alcohol steam waste water that condensation forms in tower b16; The 2nd, the steam condensate (SC) in heating clamber a5 and heating clamber b6; The 3rd, the alcohol steam waste water that condensation forms in tower a11.The alcohol steam of tower a11 output heats to the steam in tower b16 by heat exchanger b12 before entering moisture trap a13.
Between dirty alcohol feed pump 1 and heat exchanger a4, be provided with valve member a2, valve member b3, control respectively the charging of heating clamber a5 and heating clamber b6, heating clamber a5 and heating clamber b6 have liquid level gauge, by computer, control dirty alcohol and enter heating clamber a5 and heating clamber b6, dirty alcohol enters vaporization chamber a9 and vaporization chamber b10 after Steam Heating, the gaseous state alcohol of evaporation enters tower a11 and tower b16 from vaporization chamber, unevaporated dirty reflow of alcohol returns heating clamber a5 and heating clamber b6 reheats, and forms circulation between heating clamber and vaporization chamber.
Tower a11 alcohol steam out enters heat exchanger b12 heat exchange and enters moisture trap a13 after cooling and carry out gas-liquid separation, and alcohol steam enters condenser b21 condensation and reclaims; Liquid alcohol enters reflux pump a14, reclaims the wine seminal concentration at initial stage when defective, and alcohol liquid anhydrates again through the reflux pump a14 tower a11 that refluxes back; When moisture trap a13 stores fullly, unnecessary alcohol also can be by the reflux pump a14 tower a11 that refluxes back.When alcohol reaches requirement concentration, Shut-off fitting g29 opens valve member h30 and makes alcohol in reflux pump a14 enter cooler 15 condensations to obtain alcohol finished product.After steam in heat exchanger b12 absorption heating tower b16 heating chamber, flow back to tower b16 heating chamber.
Alcohol steam in tower b16 enters moisture trap b18 after condenser a17 condensation, reclaims when the initial stage, wine seminal concentration was defective, and alcohol liquid anhydrates again through the reflux pump b19 tower b16 that refluxes back; When moisture trap b18 stores fullly, unnecessary alcohol also can be by the reflux pump b19 tower b16 that refluxes back.When alcohol reaches requirement concentration, Shut-off fitting i31 makes the liquid alcohol in reflux pump b19 enter the cooling alcohol finished product that obtains of cooler 15.The isolated alcohol steam of moisture trap b18 is sucked condenser b21 condensation by vavuum pump 20, the alcohol liquid obtaining enters collecting tank 22 and is back to reflux pump b19 through pump 23, remaining waste gas is spirituosity hardly, by the exhaust outlet 24 discharge systems on collecting tank 22 tops.
In dirty alcohol, contain salt, dirty alcohol enters tower a11, tower b16 with the form of alcohol steam and has avoided the corrosion to tower a11, tower b16, feed pump 1, valve member a2, valve member b3, heat exchanger a4, heating clamber a5, heating clamber b6, salt discharge valve a7, salt discharge valve b8, vaporization chamber a9, vaporization chamber b10 and be all provided with titanium coating or adopt the processing of titanium material with the connecting line between upper-part and dirty Ethanol Exposure face, recovery tower miscellaneous part adopts 304 stainless steels processing.
The be heated bottom in chamber of heating clamber a5 and heating clamber b6 inside is respectively arranged with salt discharge valve a7 and salt discharge valve b8, evaporating the impurity such as remaining salt can drain from salt discharge valve a7 and salt discharge valve b8, play the effect of automated cleaning, be conducive to the work of continuation continuity, therefore played good antisepsis.
Tower a11 bottom is provided with steam trap 36, and steam trap 36 is automatic valves of a kind of draining resistance vapour, and the waste water that tower a11 can be produced is discharged to tower b16, and the waste water in tower a11 is comprised of the condensed water of dirty alcohol steam and the steam condensate (SC) in tower a11.
Use this equipment to reclaim the finished product alcohol concentration >=90%(V/V obtaining), treating capacity can reach 120 tons/24 hours.
The above-mentioned specific embodiment is only concrete case of the present invention; scope of patent protection of the present invention includes but not limited to product form and the style of the above-mentioned specific embodiment; anyly meet a kind of dirty alcohol distillation column of the claims in the present invention book and suitable variation or the modification that any person of an ordinary skill in the technical field does it, all should fall into scope of patent protection of the present invention.

Claims (5)

1. a dirty alcohol distillation column, it is characterized in that: comprise feed pump (1), valve member a(2), valve member b(3), heat exchanger a(4), heating clamber a(5), heating clamber b(6), salt discharge valve a(7), salt discharge valve b(8), vaporization chamber a(9), vaporization chamber b(10), tower a(11), heat exchanger b(12), moisture trap a(13), reflux pump a(14), cooler (15), tower b(16), condenser a(17), moisture trap b(18), reflux pump b(19), vavuum pump (20), condenser b(21), collecting tank (22), pump (23), exhaust outlet (24), valve member c(25), valve member d(26), valve member e(27), valve member f(28), valve member g(29), valve member h(30), valve member i(31), valve member j(32), valve member k(33), valve member m(34), valve member n(35), steam trap (36),
Heat exchanger a(4) there are two chambeies that are heated inside, a heating chamber, heating clamber a(5), heating clamber b(6), heat exchanger b(12), tower a(11), tower b(16) there is the chamber that is heated inside, a heating chamber, feed pump (1) charging aperture connects dirty wine fine supplement tube, feed pump (1) discharge port end is divided into two-way, two-way is respectively by valve member a(2) with valve member b(3) be connected heat exchanger a(4) charging aperture in inner two chambeies that are heated, heat exchanger a(4) interior two chamber discharging openings that are heated connect respectively heating clamber a(5) with heating clamber b(6) charging aperture in the chamber that is heated, heat exchanger a(4) interior heating chamber import is by valve member n(35) connection tower b(16) waste discharge water pipe, heat exchanger a(4) interior heating chamber outlet connects outside sewage disposal device, heating clamber a(5) with heating clamber b(6) the be heated bottom in chamber, inside is respectively arranged with salt discharge valve a(7) with salt discharge valve b(8), heating clamber a(5) be heated chamber discharging opening connects vaporization chamber a(9) charging aperture, vaporization chamber a(9) top discharge mouth connects tower a(11) chamber charging aperture is heated, vaporization chamber a(9) bottom return duct connects heating clamber a(5) chamber charging aperture is heated, heating clamber b(6) be heated chamber discharging opening connects vaporization chamber b(10) charging aperture, vaporization chamber b(10) top discharge mouth connects tower b(16) chamber charging aperture is heated, vaporization chamber b(10) bottom return duct connects heating clamber b(6) chamber charging aperture is heated,
Tower a(11) be heated chamber discharging opening of top connects heat exchanger b(12) heating chamber charging aperture, heat exchanger b(12) heating chamber discharging opening connects moisture trap a(13) charging aperture, heat exchanger b(12) heating chamber import is connected respectively tower b(16 with outlet) bottom and the top of heating chamber, moisture trap a(13) bottom discharge mouth connects reflux pump a(14) charging aperture, moisture trap a(13) top discharge mouth connection condenser b(21) charging aperture, reflux pump a(14) discharging opening is divided into two-way, and a road connects by valve member g(29) after connect tower a(11) the chamber charging aperture that is heated, lead up to valve member h(30) after connection cooler (15) charging aperture, tower a(11) a pipeline communication tower b(16 is passed through by steam trap (36) in the waste discharge mouth of a river, bottom) the waste discharge mouth of a river, tower b(16) be heated chamber discharging opening by condenser a(17) the rear moisture trap b(18 that connects) charging aperture, moisture trap b(18) waste gas outlet at top connects condenser b(21 through vavuum pump (20)) charging aperture, condenser b(21) discharging opening connects collecting tank (22) charging aperture, collecting tank (22) upper end is provided with exhaust outlet (24), collecting tank (22) bottom discharge mouth is successively by pump (23), valve member j(32) after, connect moisture trap b(18) charging aperture, moisture trap b(18) bottom discharge mouth connects reflux pump b(19) charging aperture, reflux pump b(19) discharging opening is divided into two-way, leads up to valve member i(31) after connect tower b(16) the chamber charging aperture that is heated, a road connects cooler (15) charging aperture,
Whole dirty alcohol distillation column heats by steam-out (SO), steam inlet is by valve member c(25) after be divided into three tunnels, lead up to valve member d(26) connect heating clamber b(6) heating chamber import, lead up to valve member e(27) connect heating clamber a(5) heating chamber import, lead up to valve member f(28) connect tower a(11) heating chamber import; Heating clamber a(5) with heating clamber b(6) heating chamber outlet docking after respectively by valve member k(33) with valve member m(34) be connected tower a(11) and tower b(16) heating chamber import.
2. a kind of dirty alcohol distillation column according to claim 1, it is characterized in that: described valve member a(2), valve member b(3), valve member c(25), valve member d(26), valve member e(27), valve member f(28), valve member g(29), valve member h(30), valve member i(31), valve member j(32), valve member k(33), valve member m(34), valve member n(35), for lead to magnetic valve only by Electromagnetic Control.
3. a kind of dirty alcohol distillation column according to claim 1, it is characterized in that: described pump (1), reflux pump a(14), reflux pump b(19), vavuum pump (20), pump (23), be any one in single-screw (single screw) pump, Quimby pump, centrifugal pump, high-pressure pump, measuring pump.
4. a kind of dirty alcohol distillation column according to claim 1, it is characterized in that: described feed pump (1), valve member a(2), valve member b(3), heat exchanger a(4), heating clamber a(5), heating clamber b(6), salt discharge valve a(7), salt discharge valve b(8), vaporization chamber a(9), vaporization chamber b(10) and be all provided with titanium coating or adopt the processing of titanium material with the connecting line between upper-part and dirty Ethanol Exposure face, recovery tower miscellaneous part adopts 304 stainless steels processing.
5. a kind of dirty alcohol distillation column according to claim 1, is characterized in that: described tower a(11), tower b(16) be bubble column structure.
CN201420393257.3U 2014-07-17 2014-07-17 A kind of dirty alcohol distillation column Expired - Lifetime CN203916115U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420393257.3U CN203916115U (en) 2014-07-17 2014-07-17 A kind of dirty alcohol distillation column

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Application Number Priority Date Filing Date Title
CN201420393257.3U CN203916115U (en) 2014-07-17 2014-07-17 A kind of dirty alcohol distillation column

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107537168A (en) * 2017-10-19 2018-01-05 榆林学院 A kind of regulation and control fixed gas scapus dynamic characteristic promotes the device of steam condensation

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107537168A (en) * 2017-10-19 2018-01-05 榆林学院 A kind of regulation and control fixed gas scapus dynamic characteristic promotes the device of steam condensation

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C14 Grant of patent or utility model
GR01 Patent grant
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: Polluted alcohol recovering tower

Effective date of registration: 20161207

Granted publication date: 20141105

Pledgee: Qingdao high technology financing Company limited by guarantee

Pledgor: QINGDAO WANTUMING BIOLOGICAL PRODUCTS Co.,Ltd.

Registration number: 2016990001084

PLDC Enforcement, change and cancellation of contracts on pledge of patent right or utility model
PC01 Cancellation of the registration of the contract for pledge of patent right

Date of cancellation: 20171213

Granted publication date: 20141105

Pledgee: Qingdao high technology financing Company limited by guarantee

Pledgor: QINGDAO WANTUMING BIOLOGICAL PRODUCTS Co.,Ltd.

Registration number: 2016990001084

PC01 Cancellation of the registration of the contract for pledge of patent right
CX01 Expiry of patent term

Granted publication date: 20141105

CX01 Expiry of patent term