CN203816636U - Reaction kettle for semi-dry-method production of agricultural sodium humate - Google Patents
Reaction kettle for semi-dry-method production of agricultural sodium humate Download PDFInfo
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- CN203816636U CN203816636U CN201420214784.3U CN201420214784U CN203816636U CN 203816636 U CN203816636 U CN 203816636U CN 201420214784 U CN201420214784 U CN 201420214784U CN 203816636 U CN203816636 U CN 203816636U
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- sodium humate
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- discharging opening
- agricultural
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Abstract
The utility model belongs to the technical field of production equipment of sodium humate and particularly relates to a reaction kettle for semi-dry-method production of agricultural sodium humate. The reaction kettle comprises a left stand column, a right stand column and a reaction chamber erected between the left stand column and the right stand column, wherein the reaction chamber comprises an outer ball and an inner ball and a cavity is formed between the outer ball and the inner ball; hollow rotary shafts which are communicated with the cavity are arranged at the two sides of the outer ball; the rotary shafts are mounted on the left stand column and the right stand column by bearings; a driven wheel is arranged on the rotary shaft at one side; the reaction kettle further comprises a feeding opening with a sealing door and a discharging opening; the feeding opening and the discharging opening are communicated with the inner cavity of the inner ball and the outer walls of the feeding opening and the discharging opening are fixedly connected with the outer ball in a sealing manner; the reaction kettle further comprises an exhausting nozzle, a thermometer and a pressure gauge; the inner ends of the exhausting nozzle, the thermometer and the pressure gauge are located in the inner cavity of the inner ball; connectors are arranged at the outer ends of the rotary shafts; one connector is connected with an oil inlet pipe and the other connector is connected with an oil returning pipe; the reaction kettle further comprises a driving machine for driving the driven wheel to rotate.
Description
Technical field
The utility model belongs to sodium humate production equipment technical field, relates in particular to a kind of reactor of using sodium humate Semi-dry process for agricultural.
Background technology
Agricultural with the production process of sodium humate mainly comprise double decomposition, quench get, the processing step such as extracting.All adopt now retort uncovered or that add a cover (also can claim reactor) to take solid, liquid than the concentration as 1:5-9, under 85-90 ℃ of liquid temperature situation, carry out liquid phase reactor, double decomposition, quench and get, extract the monovalent salt liquid that contains a certain amount of water-insoluble, this liquid will pass through nature standing sedimentation or centrifugal separation, water insoluble matter content in liquid is reached after HG/T3287-2011 technical requirement, then with different drying means, aforesaid liquid is dried to solid sodium humate powder product.Above-mentioned reactor equipment energy consumption is high, water is many, cost is high, seriously polluted.
Utility model content
The utility model provides a kind of HG/T3278-2011 of meeting agricultural to require under the prerequisite of index by sodium humate product quality for solving the technical problem existing in known technology, and energy consumption is low, water is few, production cost is low, pollute few reactor with sodium humate Semi-dry process for agricultural.
The utility model for the technical scheme that solves the technical problem that exists in known technology and take is: a kind ofly for agricultural, with the reactor of sodium humate Semi-dry process, comprise left column, right column and be erected at reative cell between the two; Described reative cell comprises outer sphere and interior spheroid, between forms cavity, in the both sides of outer sphere, be equipped with that communicate with cavity, hollow rotating shaft, described rotating shaft is arranged on left column and right column by bearing, and the rotating shaft of a side is therein provided with driven pulley; Also comprise feeding mouth and discharging opening with hermatic door, both all connect with the inner chamber of interior spheroid, outer wall is all affixed with outer sphere sealing; Also comprise exhaust nozzle, thermometer and Pressure gauge, the inner of three is all positioned at the inner chamber of interior spheroid; Outer end in rotating shaft is equipped with connector, is connected with on oil inlet pipe, another connector and is connected with oil return pipe therein on a connector; Also comprise the driving machine that drives driven pulley rotation.
Advantage of the present utility model and good effect are: the utility model provides a kind of reactor for sodium humate Semi-dry process simple and compact for structure, chamber designs is for stablize the spherical form continue rotating, the flow through conduction oil of cavity between two spheroids of thermal source employing.Compare with conventional production equipment, this reactor by promoting reaction, double decomposition in production process, quench get, the temperature and pressure value of extracting, make full use of heat energy, the in-depth extent of reaction that reaction produces, reached the effect of saving the energy, make raw-material utilization more abundant simultaneously.The steam of being extracted out by exhaust nozzle, after liquefaction condensation, reclaims and utilizes, has saved water resource.The reflection directly perceived of above-mentioned advantage is that the production cost of product has reduced.In whole production process, reactor does not discharge any pollutant in atmosphere, and environment protecting is outstanding.
Preferably: the centerline collineation of described feeding mouth and discharging opening, this center line is by the centre of sphere of interior spheroid.
Preferably: be also included in the aging bunker that porch, top is provided with funnel, reative cell rotates while making discharging opening move to low spot, and described funnel and discharging opening align.
Preferably: also comprise conducting oil circulation apparatus, oil return opening, the oil inlet pipe that oil return pipe is connected to this device is connected to the hydraulic fluid port that send of this device.
Preferably: also comprise the brake gear that countershaft brakes.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: 1, oil return pipe; 2, connector; 3, driven pulley; 4, left column; 5, driving machine; 6, outer sphere; 7, exhaust nozzle; 8, feeding mouth; 9, thermometer; 10, interior spheroid; 11, discharging opening; 12, funnel; 13, aging bunker; 14, Pressure gauge; 15, right column; 16, rotating shaft; 17, oil inlet pipe.
The specific embodiment
For further understanding summary of the invention of the present utility model, Characteristic, hereby exemplify following examples and be described in detail as follows:
Refer to Fig. 1, the utility model comprises left column 4, right column 15 and is erected at reative cell between the two.
Reative cell comprises outer sphere 6 and interior spheroid 10, and between forms cavity.In the both sides of outer sphere 6, be equipped with that communicate with cavity, hollow rotating shaft 16, rotating shaft 16 is arranged on left column 4 and right column 15 by bearing, and the rotating shaft 16 of a side is therein provided with driven pulley 3.Also comprise the driving machine 5 that drives driven pulley 3 rotations, under the effect of driving machine 5, reative cell is done 360 ° of rotations centered by rotating shaft 16.On concrete structure, driven pulley 3 and driving machine 5 can adopt gear to carry out tradition, also can adopt rope sheave etc. to carry out transmission.
Also comprise feeding mouth 8 and discharging opening 11 with hermatic door, both all connect with the inner chamber of interior spheroid 10, outer wall is all affixed with outer sphere 6 sealings.Raw material enter the inner chamber of interior spheroid 10 via feeding mouth 8, after production process finishes, discharged by discharging opening 11 again.In the present embodiment, both centerline collineations of feeding mouth 8 and discharging opening 11, this center line is by the centre of sphere of interior spheroid 10.
Also comprise exhaust nozzle 7, thermometer 9 and Pressure gauge 14, the inner of three is all positioned at the inner chamber of interior spheroid 10.Wherein, exhaust nozzle 7 is discharged the extraction of steam in reative cell for coordinating with external dehumidifier to realize, and while not accessing dehumidifier, exhaust nozzle 7 is in closed state.Thermometer 9 and Pressure gauge 14 are respectively used to Current Temperatures and the force value that monitoring shows reative cell.
This reactor adopts conduction oil as thermal source, in the outer end of rotating shaft 16, be equipped with connector 2, on a connector 2, be connected with on oil inlet pipe 17, another connector 2 and be connected with oil return pipe 1 therein, wherein connector 2 does not affect the rotation of rotating shaft 16 for guaranteeing pipeline when connecting.In order to realize thermal cycle, in the present embodiment, also comprise external conducting oil circulation apparatus, oil return pipe 1 is connected to the oil return opening of this device, the hydraulic fluid port that send that oil inlet pipe 17 is connected to this device.Conducting oil circulation apparatus should comprise oil oven and oil temperature control system.
After production process, whole reactor shuts down, and now discharging opening 11 should run to low spot, is convenient to the smooth discharge of product.In order to promote the stability of reactor when parked, in the present embodiment, also comprise the brake gear that countershaft 16 brakes.
The product of discharging can be delivered to subsequent processing: ageing operation.In the present embodiment, in order to promote the compactedness of production process, by aging device and the supporting setting of reactor.Aging device is included in the aging bunker 13 that porch, top is provided with funnel 12, and when reative cell rotates and to make discharging opening 11 move to low spot, funnel 12 aligns with discharging opening 11, and while opening discharging opening 11, product enters and in aging bunker 13, carries out ageing via funnel 12.
Production process: will add from feeding mouth 8 after the raw material by calculating, NaOH solution measures, and build hermatic door.Addition should be less than or equal to 3/4ths of kettle net volume, and the material total moisture content (comprising raw material water content NaOH, KOH solution water content) that participates in reaction in still should be 1:0.6-1.Start to start driving machine 5.Opening and sending hot system is conducting oil circulation apparatus.When thermometer 9 displays temperatures reach 140 ℃, Pressure gauge 14 and show that pressure reach 1-2kg, start timing 20-120min (because of various raw materials different, reaction time and difference), after the time, stop driving machine 5 and thermal source.Open afterwards dehumidifier, when dehumidifier exhaust outlet is shown as zero without steam and Pressure gauge 14, then open thermal source and driving machine 5 running 5min, shut down.Opening discharging opening 11 blowings enters aging bunker 13 ageing 48-168h through funnel 12 and obtains dry products.
Claims (5)
1. the reactor with sodium humate Semi-dry process for agricultural, is characterized in that: comprise left column (4), right column (15) and be erected at reative cell between the two; Described reative cell comprises outer sphere (6) and interior spheroid (10), between forms cavity, in the both sides of outer sphere (6), be equipped with that communicate with cavity, hollow rotating shaft (16), described rotating shaft (16) is arranged on left column (4) by bearing and right column (15) is upper, and the rotating shaft of a side therein (16) is provided with driven pulley (3); Also comprise feeding mouth (8) and discharging opening (11) with hermatic door, both all connect with the inner chamber of interior spheroid (10), outer wall all seals affixed with outer sphere (6); Also comprise exhaust nozzle (7), thermometer (9) and Pressure gauge (14), the inner of three is all positioned at the inner chamber of interior spheroid (10); In the outer end of rotating shaft (16), be equipped with connector (2), on a connector (2), be connected with on oil inlet pipe (17), another connector (2) and be connected with oil return pipe (1) therein; Also comprise the driving machine (5) that drives driven pulley (3) rotation.
2. the reactor of using sodium humate Semi-dry process for agricultural as claimed in claim 1, is characterized in that: described feeding mouth (8) and both centerline collineations of discharging opening (11), this center line is by the centre of sphere of interior spheroid (10).
As claimed in claim 1 for agricultural the reactor with sodium humate Semi-dry process, it is characterized in that: be also included in the aging bunker (13) that porch, top is provided with funnel (12), reative cell rotates while making discharging opening (11) move to low spot, and described funnel (12) aligns with discharging opening (11).
As claimed in claim 1 for agricultural the reactor with sodium humate Semi-dry process, it is characterized in that: also comprise conducting oil circulation apparatus, oil return pipe (1) is connected to the oil return opening of this device, the hydraulic fluid port that send that oil inlet pipe (17) is connected to this device.
5. the reactor of using sodium humate Semi-dry process for agricultural as claimed in claim 1, is characterized in that: also comprise the brake gear that countershaft (16) brakes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420214784.3U CN203816636U (en) | 2014-04-29 | 2014-04-29 | Reaction kettle for semi-dry-method production of agricultural sodium humate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420214784.3U CN203816636U (en) | 2014-04-29 | 2014-04-29 | Reaction kettle for semi-dry-method production of agricultural sodium humate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203816636U true CN203816636U (en) | 2014-09-10 |
Family
ID=51472180
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420214784.3U Expired - Fee Related CN203816636U (en) | 2014-04-29 | 2014-04-29 | Reaction kettle for semi-dry-method production of agricultural sodium humate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203816636U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107262016A (en) * | 2017-08-09 | 2017-10-20 | 无锡殷达尼龙有限公司 | A kind of solid state polycondensation device |
| CN109571383A (en) * | 2018-06-20 | 2019-04-05 | 新奥科技发展有限公司 | A kind of rotary type reaction unit |
-
2014
- 2014-04-29 CN CN201420214784.3U patent/CN203816636U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107262016A (en) * | 2017-08-09 | 2017-10-20 | 无锡殷达尼龙有限公司 | A kind of solid state polycondensation device |
| CN109571383A (en) * | 2018-06-20 | 2019-04-05 | 新奥科技发展有限公司 | A kind of rotary type reaction unit |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140910 Termination date: 20180429 |