Pre-treatment all-in-one sample cup
Technical field
The utility model relates to a kind of sample cup, relate to specifically a kind of can be positioned in sample pre-treatments all-in-one and can pulverize food samples such as cereal, fruits and vegetables, nut, meats, the pre-treatment all-in-one sample cup of homogeneous, purification, concentration.
Background technology
Sample pre-treatments roughly comprises that sample is pulverized, extracts, purified, the process such as concentrated, and main sample is pulverized pre-processing device comminutor, homogenizer; Sample extraction pre-processing device has ultrasound wave extraction apparatus, soxhlet extraction instrument, accelerated solvent extraction etc.; Sample purification pre-processing device has solid-phase extracting instrument, gel purification instrument etc.; Sample concentration pre-processing device has rotary evaporator, Nitrogen evaporator etc.
The domestic exploitation to pre-processing device is at present devoted to each pretreatment process to realize integrated.That integrated pre-processing device not only has is quick, easy, robotization, save time, labour-saving feature, can also reduce because different personnel's operations and sample repeatedly shift the error of bringing, reduce organic solvent use amount, and can alleviate the pollution to environment.Pre-processing device only carries out intelligent integration for certain step of pre-treatment or certain several step at present, whole pretreatment process can not be realized to whole robotizations, as automatic Solid-Phase Extraction equipment only can complete the purification process of sample automatically.
In the process of pre-treatment Study on Integration, its bottleneck filters for realization that can not be smooth directly enters into filtration unit automatically by the sample after pulverizing, the utility model is for the deficiency of existing food inspection pre-processing device, design a sample cup that can be positioned in pre-treatment all-in-one, can be continuously in this sample cup disposablely complete pulverizing, homogeneous, filter, purify the processes such as concentrated, reduce sample and repeatedly shifted loss and the pollution bringing, alleviated testing staff's workload, improved pre-treatment efficiency, can be food safety Regulation strong technical support is provided.
Summary of the invention
The utility model object is to provide a kind of pre-treatment all-in-one sample cup, it coordinates pre-treatment all-in-one to use, can in same sample cup, to complex samples such as cereal, fruits and vegetables, nut, meat products, complete pulverizing, homogeneous, filters, and purifies concentrated grade for processing, do not need Other Instruments equipment, simple to operate, quick, improved pre-treatment efficiency, alleviated testing staff's workload.
To achieve these goals, technical solution of the present utility model is: a kind of pre-treatment all-in-one sample cup, comprises broken blade base, broken blade, sample Storage Cup, filtration, purification enrichment facility.
The utility model pre-treatment all-in-one sample cup, wherein, described broken blade base inside is arch design, embody centrifugal principle, centre position is broken blade, and broken blade designs for antispin, rotation axis passes in the middle of broken blade base and strictly seals with broken blade base, rotation axis connects broken blade, and broken blade base internal edge has O-ring seal, and O-ring seal periphery is screw thread.
The utility model pre-treatment all-in-one sample cup, wherein, one liquid filling hole is arranged at described sample Storage Cup top, thereby liquid filling hole need connect PE, pipe connects liquid feeding system, sample Storage Cup top is screw thread, and sample Storage Cup bottom is filter screen, and this filter screen and sample Storage Cup are integrated design, filter screen periphery is O-ring seal, and O-ring seal periphery is screw thread.
The utility model pre-treatment all-in-one sample cup, wherein, described filtration, purification enrichment facility designs for right cylinder, and screw thread is arranged at top, comprises packing area and filter tip.
The utility model pre-treatment all-in-one sample cup, wherein, described broken blade base is connected by screw thread with sample Storage Cup, O-ring seal on broken blade base guarantees that broken blade base is connected sealing afterwards with sample Storage Cup, sample Storage Cup is connected by screw thread with filtration, purification enrichment facility, the sealing after the O-ring seal assurance sample Storage Cup of filter screen periphery is connected with filtration, purification enrichment facility.
The utility model pre-treatment all-in-one sample cup, wherein, described pre-treatment all-in-one sample cup is embedded in mechanical arm by broken blade base, and while rotation axis can connect pulverizing motor makes sample cup become as a whole with pre-treatment all-in-one.
Adopt after such scheme, because the utility model pre-treatment all-in-one sample cup comprises broken blade base, broken blade, sample Storage Cup, filtration, purification enrichment facility, therefore before carrying out pre-treatment, to first pending material be put into sample Storage Cup, again sample Storage Cup is connected by thread seal with broken blade base, afterwards as required, fill area in filtration, purification enrichment facility is inserted required filler in advance, filtration, purification enrichment facility and sample Storage Cup are tightly connected, after whole sample cup connects, after sample cup is embedded on mechanical arm by broken blade base, rotation axis in sample cup is connected with pulverizing motor, open pre-treatment all-in-one power supply, by pre-treatment all-in-one machine control system, in sample cup, complete pulverizing, extract, filter, purify, the concentrated pre-treatment operation steps that waits, the utlity model has closed, integral type, the feature such as multi-functional.
Accompanying drawing explanation
Fig. 1 is pre-treatment all-in-one sample cup structure principle chart.
Fig. 2 is pre-treatment all-in-one sample cup structural representation.
Fig. 3 is broken blade base schematic top plan view.
Fig. 4 is broken blade base bottom schematic view.
Fig. 5 is sample Storage Cup bottom schematic view.
Fig. 6 is sample Storage Cup top schematic diagram.
Fig. 7 is filtration, purification enrichment facility bottom schematic view.
Fig. 8 is filtration, purification enrichment facility top schematic diagram.
Embodiment
As shown in Fig. 1 schematic diagram, sample cup comprises broken blade base 1, broken blade 2, sample Storage Cup 3, filtration, purification enrichment facility 4, broken blade 2 is arranged in the middle of broken blade base 1, rotation axis 11 passes in the middle of broken blade base 1 and strictly seals with broken blade base 1, rotation axis 11 connects broken blade 2, broken blade base 1 inside is arch design, include O-ring seal 13, broken blade base 1 is by screw thread 14, 32 are connected with sample Storage Cup 3, sample Storage Cup 3 bottoms are filter screen 33 designs, filter screen 33 is integrated design with sample Storage Cup 3, filter screen 33 peripheries are O-ring seal 34, on sample Storage Cup 3, there is liquid filling hole 31, sample Storage Cup 3 is by screw thread 35, 41 are connected with filtration, purification enrichment facility 4, filtration, purification enrichment facility 4 is right cylinder, in cylinder, there are packing area 42 and filter tip 43, whole sample cup is embedded into mechanical arm 5 by broken blade base 1, while rotation axis 11 can connect pulverizing motor 12 makes sample cup become as a whole with pre-treatment all-in-one.
The malachite green detecting in structure of fish muscle of take is example, during detection, first 10g is oppressed to sample and put into 3 li of sample Storage Cups, add one bottle of solids extract agent to 3 li of sample Storage Cups, and then sample Storage Cup 3 and broken blade base 1 are linked together, packing area 42 is inserted the concentrated required filler of malachite green filtration, purification in advance, then filtration, purification enrichment facility 4 is connected with sample Storage Cup 3, afterwards the whole sample cup connecting is embedded into mechanical arm 5 by broken blade base 1, by rotation axis 11, connect and pulverize on motor 12, then carry out software operation setting, the steps include: parameters, select sample, select test item, click and start, broken blade is pulverized sample, then liquid feeding system can be injected by liquid filling hole 31 extract through PE pipe in sample Storage Cup 3, broken blade high-speed rotation homogeneous structure of fish muscle to be checked afterwards, extract malachite green simultaneously, after homogeneous has extracted, mechanical arm 5 automatic turning turnbacks, whole sample cup is simultaneously along with mechanical arm 5 automatic turning turnbacks, now, filtration, purification enrichment facility 4 is turned to bottommost, under the pressurization of system, extract carries out filtration, purification automatically by filter screen 33 and packing area 42, efflux flows out by filter tip 43, give up efflux, after liquid to be extracted drains off, taking-up is enriched with the filtration, purification enrichment facility 4 of malachite green, carry out the subsequent operations such as wash-out extraction, go up afterwards liquid chromatography or gas chromatographic detection result.
The above embodiment is described preferred implementation of the present utility model; not scope of the present utility model is limited; do not departing under the prerequisite of the utility model design spirit; various distortion and improvement that the common engineering technical personnel in this area make the technical solution of the utility model, all should fall in the definite protection domain of claims of the present utility model.