CN203737100U - Security device for preventing harmful gas leakage in 2-nitryl-4-trifluoromethyl cyanophenyl production - Google Patents

Security device for preventing harmful gas leakage in 2-nitryl-4-trifluoromethyl cyanophenyl production Download PDF

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Publication number
CN203737100U
CN203737100U CN201420116224.4U CN201420116224U CN203737100U CN 203737100 U CN203737100 U CN 203737100U CN 201420116224 U CN201420116224 U CN 201420116224U CN 203737100 U CN203737100 U CN 203737100U
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CN
China
Prior art keywords
cooler
storage tank
liquid storage
absorption liquid
absorbing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201420116224.4U
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Chinese (zh)
Inventor
张传布
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qingdao Union Fine Chemical Co Ltd
Original Assignee
Qingdao Union Fine Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Qingdao Union Fine Chemical Co Ltd filed Critical Qingdao Union Fine Chemical Co Ltd
Priority to CN201420116224.4U priority Critical patent/CN203737100U/en
Application granted granted Critical
Publication of CN203737100U publication Critical patent/CN203737100U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model discloses a security device for preventing harmful gas leakage in 2-nitryl-4-trifluoromethyl cyanophenyl production. The device comprises a reaction kettle, a packing absorbing tower, a cooler and an absorbing liquid storage tank, wherein the reaction kettle is connected with the packing absorbing tower through a waste gas pipeline; the cooler is positioned at the lower part of the packing absorbing tower; a view lens is arranged on a pipeline for connecting the cooler and the absorbing liquid storage tank; the absorbing liquid storage tank is connected with an inlet of an absorbing ejection pump; two branch pipelines are arranged at the outlet of the absorbing ejection pump; one branch pipeline is connected to the top end of the packing absorbing tower; the other branch pipeline is connected with a Venturi tube and is connected to the top end of the absorbing liquid storage tank; a gas pipeline is connected to the bottom of the cooler and is connected with an inlet of the Venturi tube. The device adopts the Venturi principle to change the pressure of the system, the reaction kettle is kept in negative pressure, toxic and harmful gases can be directly fed into the packing absorbing tower from the reaction kettle after being generated, and are absorbed by a sprayed circulation absorbing liquid, and thus the gases are not retained inside the reaction kettle or are not directly discharged into the atmosphere.

Description

A kind of safety device that prevents poisonous gas leakage of producing for 2-nitro-4-trifluoromethyl Benzonitrile
Technical field
The utility model relates to a kind of safety device that prevents poisonous gas leakage of producing for 2-nitro-4-trifluoromethyl Benzonitrile.
Background technology
This utility model is to prevent poisonous gas leakage design during 2-nitro-4-trifluoromethyl Benzonitrile is produced.The production process of 2-nitro-4-trifluoromethyl Benzonitrile is cyanogenation, there is the potential safety hazard of emitting the toxic and harmfuls such as hydrogen cyanide in cyanogenation, design this utility model in line with the production safety management theory that people-oriented, prevent trouble before it happens, make maintenance negative pressure in reactor, can prevent toxic and harmful leakage or remain in reactor, being imported in absorption liquid and absorb completely, accomplish harmless treatment, is a set of very effectively safety precaution and emergency service.
Summary of the invention
Technical problem to be solved in the utility model is: a kind of safety device that prevents poisonous gas leakage of producing for 2-nitro-4-trifluoromethyl Benzonitrile is provided.
For solving the problems of the technologies described above, the technical solution adopted in the utility model is:
Produce a safety device that prevents poisonous gas leakage for 2-nitro-4-trifluoromethyl Benzonitrile, it is characterized in that, comprise reactor, packed absorber, cooler and absorption liquid storage tank; Reactor is connected by exhaust piping with packed absorber, cooler is positioned at the bottom of packed absorber, the pipeline connecting between cooler and absorption liquid storage tank is provided with visor, absorption liquid storage tank connects the entrance that absorbs jet pump, absorb injection delivery side of pump and have two laterals, a lateral is connected to the top of packed absorber, another lateral connects Venturi tube and is connected with the top of absorption liquid storage tank, and cooler bottom connects a gas pipeline and is connected with the porch of Venturi tube.
Cooler is provided with recirculated water reflux.
Described recirculated water reflux comprises: recirculated water water supply pipeline is installed in cooler lower end, and recirculated water water return pipeline is installed in cooler upper end.
On absorption liquid storage tank, be also provided with running water water inlet pipe.
On two laterals of absorption jet pump outlet, be all provided with valve.
The beneficial effects of the utility model are:
This utility model is mainly for preventing poisonous gas leakage design in the production of 2-nitro-4-trifluoromethyl Benzonitrile, in 2-nitro-4-trifluoromethyl Benzonitrile production process, there is the potential safety hazard of emitting toxic and harmful, may cause great harm to human and environment.This device uses venturi principle to change system air pressure, make maintenance negative pressure in reactor, after toxic and harmful γ-ray emission, can directly enter packed absorber from reactor, absorbed by Sprayer Circulation absorption liquid, guarantee that toxic and harmful gas neither can remain in reactor, also can directly not enter air.
Brief description of the drawings
Below in conjunction with accompanying drawing, detailed description of the invention of the present utility model is described in further detail.
Fig. 1 is structural representation of the present utility model.
In figure, 1. reactor; 2. packed absorber; 3. cooler; 4. visor; 5. absorption liquid storage tank; 6. Venturi tube; 7. absorb jet pump; 8. valve; 9. gas pipeline; 10. running water water inlet pipe; 11. recirculated water water supply pipelines; 12. recirculated water water return pipelines; 13. exhaust pipings.
Detailed description of the invention
As accompanying drawing 1, a kind of safety device that prevents poisonous gas leakage of producing for 2-nitro-4-trifluoromethyl Benzonitrile, comprises reactor, packed absorber, cooler and absorption liquid storage tank; Reactor is connected by exhaust piping with packed absorber, cooler is positioned at the bottom of packed absorber, the pipeline connecting between cooler and absorption liquid storage tank is provided with visor, absorption liquid storage tank connects the entrance that absorbs jet pump, absorb injection delivery side of pump and have two laterals, a lateral is connected to the top of packed absorber, another lateral connects Venturi tube and is connected with the top of absorption liquid storage tank, and cooler bottom connects a gas pipeline and is connected with the porch of Venturi tube.
Cooler is provided with recirculated water reflux.
Described recirculated water reflux comprises: recirculated water water supply pipeline is installed in cooler lower end, and recirculated water water return pipeline is installed in cooler upper end.
On absorption liquid storage tank, be also provided with running water water inlet pipe.
On two laterals of absorption jet pump outlet, be all provided with valve.
Absorption liquid is transported to Venturi tube from absorption liquid storage tank by absorbing jet pump part, absorption liquid forms vacuum in Venturi tube makes gas pipeline, cooler, packed absorber and reactor, when toxic and harmful produces, under pressure differential effect, this waste gas can enter packed absorber from reactor and neither can remain in and in reactor, also can directly not enter air.Meanwhile, another part absorption liquid is transported to packed absorber and sprays, and waste gas fully contacts after complete reaction with absorption liquid in packed absorber, and absorption liquid is got back to absorption liquid storage tank through cooler, visor.Its mesoscope can observe absorption liquid flow, thereby valve can be controlled air pressure and the absorption liquid spray flux of the absorption liquid flow control device inside of two branch roads.This device can ensure toxic and harmful to absorb, ensure safety of workers and protection of the environment completely.
The above, it is only preferred embodiment of the present utility model, be not the restriction of the utility model being made to other form, any those skilled in the art may utilize the technology contents of above-mentioned announcement to be changed or be modified as the equivalent embodiment of equivalent variations.But every technical solutions of the utility model content that do not depart from, any simple modification, equivalent variations and the remodeling above embodiment done according to technical spirit of the present utility model, still belong to the protection domain of technical solutions of the utility model.

Claims (5)

1. produce for 2-nitro-4-trifluoromethyl Benzonitrile a safety device that prevents poisonous gas leakage, it is characterized in that, comprise reactor, packed absorber, cooler and absorption liquid storage tank; Reactor is connected by exhaust piping with packed absorber, cooler is positioned at the bottom of packed absorber, the pipeline connecting between cooler and absorption liquid storage tank is provided with visor, absorption liquid storage tank connects the entrance that absorbs jet pump, absorb injection delivery side of pump and have two laterals, a lateral is connected to the top of packed absorber, another lateral connects Venturi tube and is connected with the top of absorption liquid storage tank, and cooler bottom connects a gas pipeline and is connected with the porch of Venturi tube.
2. safety device according to claim 1, is characterized in that, cooler is provided with recirculated water reflux.
3. safety device according to claim 2, is characterized in that, described recirculated water reflux comprises: recirculated water water supply pipeline is installed in cooler lower end, and recirculated water water return pipeline is installed in cooler upper end.
4. safety device according to claim 1, is characterized in that, is also provided with running water water inlet pipe on absorption liquid storage tank.
5. safety device according to claim 1, is characterized in that, on two laterals of absorption jet pump outlet, is all provided with valve.
CN201420116224.4U 2014-03-14 2014-03-14 Security device for preventing harmful gas leakage in 2-nitryl-4-trifluoromethyl cyanophenyl production Expired - Fee Related CN203737100U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420116224.4U CN203737100U (en) 2014-03-14 2014-03-14 Security device for preventing harmful gas leakage in 2-nitryl-4-trifluoromethyl cyanophenyl production

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420116224.4U CN203737100U (en) 2014-03-14 2014-03-14 Security device for preventing harmful gas leakage in 2-nitryl-4-trifluoromethyl cyanophenyl production

Publications (1)

Publication Number Publication Date
CN203737100U true CN203737100U (en) 2014-07-30

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201420116224.4U Expired - Fee Related CN203737100U (en) 2014-03-14 2014-03-14 Security device for preventing harmful gas leakage in 2-nitryl-4-trifluoromethyl cyanophenyl production

Country Status (1)

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CN (1) CN203737100U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110292833A (en) * 2019-06-14 2019-10-01 南京高源环保工程有限公司 A kind of low-concentration sulfur dioxide gas sodium citrate sulfur method and equipment

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110292833A (en) * 2019-06-14 2019-10-01 南京高源环保工程有限公司 A kind of low-concentration sulfur dioxide gas sodium citrate sulfur method and equipment

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140730

Termination date: 20170314