CN203683125U - Acid-soluble reaction system for producing polyaluminum chloride by employing automatic aggregating van-type press filter - Google Patents

Acid-soluble reaction system for producing polyaluminum chloride by employing automatic aggregating van-type press filter Download PDF

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Publication number
CN203683125U
CN203683125U CN201320762756.0U CN201320762756U CN203683125U CN 203683125 U CN203683125 U CN 203683125U CN 201320762756 U CN201320762756 U CN 201320762756U CN 203683125 U CN203683125 U CN 203683125U
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filter
chamber
type press
acid
press filter
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CN201320762756.0U
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Chinese (zh)
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邹宏
魏小兵
邹鹏
谷飞
王明冬
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Chongqing Lanjie Guangshun Water Purification Materials Co Ltd
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Chongqing Lanjie Guangshun Water Purification Materials Co Ltd
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Abstract

The utility model discloses an acid-soluble reaction system for producing polyaluminum chloride by employing an automatic aggregating van-type press filter. The acid-soluble reaction system comprises a reaction tank, a transfer tank of the reaction tank, a flocculant preparation tank, an automatic aggregating van-type press filter and a one-step liquid tank. Since the acid-soluble reaction system disclosed by the utility model is internally provided with the devices such as the transfer tank of the reaction tank, the flocculant preparation tank and the automatic aggregating van-type press filter, the content of insoluble substances in the one-step solution can be effectively controlled and reduced by separating the insoluble residues generated in the acid-soluble reaction in these devices via coagulation and sedimentation and press filtration, thereby improving the yield and quality of the polyaluminum chloride products; the press filter utilized in the acid-soluble reaction system disclosed by the utility model is the automatic aggregating van-type press filter which is provided with a liquid receiving tank communicated with the filtrate chamber and used for automatically collecting filtrate, and is also provided with a filter residue receiving hopper which directly faces to the press filtration set and is used for automatically collecting filter residues, thus filter residues and filtrate can be efficiently and automatically collected, labor costs is reduced and working efficiency is improved.

Description

A kind of poly aluminium chloride that uses the chamber-type press filter that automatically gathers materials is produced acid-soluble reactive system
Technical field
The utility model belongs to poly aluminium chloride production technical field, relates to a kind of poly aluminium chloride that uses the chamber-type press filter that automatically gathers materials and produces acid-soluble reactive system.
Background technology
Poly aluminium chloride, is commonly called as water purification agent, has another name called polymerize aluminum chloride, is called for short poly-aluminium, english name PAC; It is the cationic inorganic polymer flocculant of a kind of poly-hydroxy, multinuclear complexing body, and solid phase prod outward appearance is sorrel, yellow or white solid powder, and its chemical molecular formula is [AL 2(OH) ncL 6-n] m(in formula, 1≤n≤5, m≤10), wherein m represents extent of polymerization, and n represents the neutral degree of PAC product, soluble in water, there is stronger bridge formation adsorptivity, in hydrolytic process, follow the physicsization such as electrochemistry, cohesion, absorption and precipitation to change, the final [AL that generates 2(OH) 3(OH) 3], thereby reach purification object.
The fundamental difference of poly aluminium chloride and traditional inorganic coagulant is that traditional inorganic coagulant is low molecular crystal salt, and the structure of poly aluminium chloride is made up of the changeable polynary carboxyl complex compound of form, flocculation sediment speed is fast, be suitable for pH value wide ranges, to pipe-line equipment non-corrosiveness, purifying water effect is obvious, can effectively prop up the heavy metal ion such as middle chromaticness SS, COD, BOD and arsenic, mercury that dewater, and this product is widely used in tap water, process water and sewage treatment area.
Poly aluminium chloride is divided into form and is divided into two kinds: a. liquid poly aluminium chloride is undried form, have and need not dilute, load and unload advantage easy to use, price is relatively cheap, shortcoming is traffic requirements tank car, and unit cost increases (solid per ton is equivalent to 2-3 ton liquid); B. solid poly aluminium chloride is dried form, has the advantage of convenient transportation, while not needing tank car, shortcoming to be use, also needs dilution, increases working strength.
The raw material of producing poly aluminium chloride mainly contains two large classes: a class is aluminum-containing mineral, comprises bauxite (gibbsite, boehmite, diaspore), clay, kaolin, alunite etc.; Another kind of is other aluminum-containing raw material, comprises metallic aluminium, aluminium scrap bits, grey aluminium, aluminium hydroxide, aluminum chloride, coal gangue, flyash etc.The method of producing at present poly aluminium chloride mainly contains metallic aluminium (comprising aluminium ash, lead skim) method, active aluminium hydroxide method, aluminium sesquioxide (comprising bauxitic clay, coal gangue etc.) method, crystal aluminum chloride method etc.
Built poly aluminium chloride production equipment at present, majority is the device that bauxitic clay and calcium aluminate two-step approach are produced poly aluminium chloride, the following shortcoming of its ubiquity:
1) in the acid-soluble reaction of the first step, can produce a large amount of calcium chloride suspended substances and be difficult to effectively separate with single step reaction liquid (aluminum chloride reaction solution), cause insolubles severe overweight in final poly aluminium chloride product;
2) although existing poly aluminium chloride production equipment generally adopts the press filtration device separates such as pressure filter to remove reaction insolubles residue, but, these pressure filter all do not have material-gathering device, the filter residue particularly separating for press filtration, generally directly fall earthward, getting up carries out again then to collect (normally manually using spade).This mode is polluted production environment, and artificially collect time-consuming, increase production cost; In addition, acid-soluble reacted pickling liquor meeting volatilizes the more sour waste gas that contains, and corresponding absorption disposal facility is not set when press filtration, can cause Working environment to worsen and environmental pollution.
Summary of the invention
In view of this, the purpose of this utility model is to provide a kind of poly aluminium chloride that uses the chamber-type press filter that automatically gathers materials to produce acid-soluble reactive system, separate the insolubles residue producing in acid-soluble reaction by coagulating sedimentation, press filtration, and can efficiently automatically collect filter residue, filtrate, reduce cost of labor, increase work efficiency.
For achieving the above object, the utility model provides following technical scheme:
The utility model discloses a kind of poly aluminium chloride that uses the chamber-type press filter that automatically gathers materials and produce acid-soluble reactive system, described acid-soluble reactive system comprises reaction tank, reaction tank transfer pond, flocculating agent formulation tank, gather materials chamber-type press filter and a step liquid pool automatically;
The described chamber-type press filter that automatically gathers materials comprises frame, rack-mounted two crossbeams and be arranged on the hydraulic compressing device in frame, between two crossbeams, be provided with slurcocks and stop plate, between slurcocks and prevention plate, be provided with the press filtration group being formed by several filter press plates, every two filter press plates are combined into a filter chamber, filter chamber is provided with filter cloth, the described chamber-type press filter that automatically gathers materials also comprises and connects liquid pool, be arranged on connecing liquid bath and being arranged at the dreg-accepting hopper under press filtration group in frame, the described liquid bath that connects is communicated with filter chamber by flexible pipe, describedly connect liquid pool and connect liquid bath and be communicated with,
Described reaction tank is provided with bauxitic clay charging opening and acid solution charging opening, described reaction tank is communicated with reaction tank transfer pond, flocculating agent formulation tank is communicated with reaction tank transfer pond, reaction tank transfer pond is communicated with the chamber-type press filter that automatically gathers materials by the muddy material pump of a step liquid, and the liquid pool that connects of the chamber-type press filter that automatically gathers materials is communicated with a step liquid pool.
Further, described acid-soluble reactive system also comprises slag wash trough, and the dreg-accepting hopper of the described chamber-type press filter that automatically gathers materials is communicated with slag wash trough by rotary conveyor.
Further, the described dreg-accepting hopper that automatically gathers materials chamber-type press filter is shaped as the shape of falling truncated rectangular pyramids.
Further, described acid-soluble reactive system also comprises tail gas absorber, directly over the press filtration group of the described chamber-type press filter that automatically gathers materials, be provided with gas skirt, the exhaust gas entrance of described tail gas absorber is communicated with the gas skirt of reaction tank, reaction tank transfer pond and the chamber-type press filter that automatically gathers materials respectively.
Further, described reaction tank, reaction tank transfer pond and flocculating agent formulation tank are equipped with agitator.
The beneficial effects of the utility model are:
1) the utility model is provided with reaction tank transfer pond, flocculating agent formulation tank and the devices such as chamber-type press filter that automatically gather materials in acid-soluble reactive system, the insolubles residue producing separate acid-soluble reaction by coagulating sedimentation, press filtration in these devices in, effectively control and reduced the insolubles content in a step liquid, having improved output and the quality of poly aluminium chloride product;
2) pressure filter that the utility model adopts is the chamber-type press filter that automatically gathers materials, automatically the chamber-type press filter that gathers materials is provided with the liquid bath that connects being communicated with filter chamber and automatically collects filtrate, just be provided with the dreg-accepting hopper of press filtration group is collected to filter residue automatically, therefore can efficiently automatically collect filter residue, filtrate, reduce cost of labor, improved working efficiency;
3) the utility model is also provided with gas skirt directly over press filtration group, and what during by acid-soluble reaction, volatilize in the time that pickling liquor press filtration operates absorbs to tail gas absorber disposal together with sour waste gas, has avoided Working environment to worsen and environmental pollution.
Brief description of the drawings
In order to make the purpose of this utility model, technical scheme and beneficial effect clearer, the utility model provides following accompanying drawing to describe:
Fig. 1 is structural representation of the present utility model.
Embodiment
Below in conjunction with accompanying drawing, preferred embodiment of the present utility model is described in detail.
Fig. 1 is structural representation of the present utility model, as shown in the figure, automatically the gather materials poly aluminium chloride of chamber-type press filter of use of the present utility model is produced acid-soluble reactive system, comprises reaction tank 1, reaction tank transfer pond 2, flocculating agent formulation tank 3, gather materials chamber-type press filter and a step liquid pool 4 automatically;
The described chamber-type press filter that automatically gathers materials comprises frame 5, be arranged on two crossbeams 6 in frame 5 and be arranged on the hydraulic compressing device 7 in frame 5, between two crossbeams 6, be provided with slurcocks 8 and stop plate 9, between slurcocks 8 and prevention plate 9, be provided with the press filtration group 10 being formed by several filter press plates, every two filter press plates are combined into a filter chamber, filter chamber is provided with filter cloth, the described chamber-type press filter that automatically gathers materials also comprises and connects liquid pool 11, be arranged on connecing liquid bath 12 and being arranged at the dreg-accepting hopper 13 under press filtration group 10 in frame 5, the described liquid bath 12 that connects is communicated with filter chamber by flexible pipe 14, describedly connect liquid pool 11 and connect liquid bath 12 and be communicated with,
Described reaction tank 1 is provided with bauxitic clay charging opening 15 and acid solution charging opening 16, described reaction tank 1 is communicated with reaction tank transfer pond 2, flocculating agent formulation tank 3 is communicated with reaction tank transfer pond 2, reaction tank transfer pond 2 is communicated with the chamber-type press filter that automatically gathers materials by the muddy material pump 17 of a step liquid, and the liquid pool 11 that connects of the chamber-type press filter that automatically gathers materials is communicated with a step liquid pool 4; Described reaction tank 1, reaction tank transfer pond 2 and flocculating agent formulation tank 3 are equipped with agitator.
As further improvement of the utility model, described acid-soluble reactive system also comprises slag wash trough 18, and the dreg-accepting hopper 13 of the described chamber-type press filter that automatically gathers materials is communicated with slag wash trough 18 by rotary conveyor 19; The dreg-accepting hopper 13 of the described chamber-type press filter that automatically gathers materials is shaped as the shape of falling truncated rectangular pyramids.
As further improvement of the utility model, described acid-soluble reactive system also comprises tail gas absorber 20, directly over the press filtration group 10 of the described chamber-type press filter that automatically gathers materials, be provided with gas skirt 21, the exhaust gas entrance of described tail gas absorber 20 is communicated with the gas skirt 21 of reaction tank 1, reaction tank transfer pond 2 and the chamber-type press filter that automatically gathers materials respectively.
Production Flow Chart of the present utility model is: in reaction tank 1, add hydrochloric acid, then drop into the bauxitic clay of formula ratio, reacting by heating, reaction product is taked to put into reaction tank transfer pond 2 from stream mode, add poly-propionic acid amide flocculation agent flocculation by flocculating agent formulation tank 3, then pump into and automatically gather materials in chamber-type press filter by the muddy material pump 17 of a step liquid, reaction tank product is carried out to the separation of slag liquid; Filtrate is flowed into and is connect liquid bath 12 by flexible pipe 14, then flows into and connect in liquid pool 11, then flows in a step liquid pool 4; And filter residue directly falls in dreg-accepting hopper 13, be then delivered to slag wash trough 18 carrying out washing treatment; Together with what acid-soluble when reaction volatilized in the time that pickling liquor press filtration operate contain sour waste gas, absorb to tail gas absorber 20 and dispose.
Finally explanation is, above preferred embodiment is only unrestricted in order to the technical solution of the utility model to be described, although the utility model is described in detail by above preferred embodiment, but those skilled in the art are to be understood that, can make various changes to it in the form and details, and not depart from the utility model claims limited range.

Claims (5)

1. automatically the gather materials poly aluminium chloride of chamber-type press filter of use is produced an acid-soluble reactive system, it is characterized in that: described acid-soluble reactive system comprises reaction tank, reaction tank transfer pond, flocculating agent formulation tank, gather materials chamber-type press filter and a step liquid pool automatically;
The described chamber-type press filter that automatically gathers materials comprises frame, rack-mounted two crossbeams and be arranged on the hydraulic compressing device in frame, between two crossbeams, be provided with slurcocks and stop plate, between slurcocks and prevention plate, be provided with the press filtration group being formed by several filter press plates, every two filter press plates are combined into a filter chamber, filter chamber is provided with filter cloth, the described chamber-type press filter that automatically gathers materials also comprises and connects liquid pool, be arranged on connecing liquid bath and being arranged at the dreg-accepting hopper under press filtration group in frame, the described liquid bath that connects is communicated with filter chamber by flexible pipe, describedly connect liquid pool and connect liquid bath and be communicated with,
Described reaction tank is provided with bauxitic clay charging opening and acid solution charging opening, described reaction tank is communicated with reaction tank transfer pond, flocculating agent formulation tank is communicated with reaction tank transfer pond, reaction tank transfer pond is communicated with the chamber-type press filter that automatically gathers materials by the muddy material pump of a step liquid, and the liquid pool that connects of the chamber-type press filter that automatically gathers materials is communicated with a step liquid pool.
2. automatically the gather materials poly aluminium chloride of chamber-type press filter of use according to claim 1 is produced acid-soluble reactive system, it is characterized in that: described acid-soluble reactive system also comprises slag wash trough, the dreg-accepting hopper of the described chamber-type press filter that automatically gathers materials is communicated with slag wash trough by rotary conveyor.
3. automatically the gather materials poly aluminium chloride of chamber-type press filter of use according to claim 2 is produced acid-soluble reactive system, it is characterized in that: the described dreg-accepting hopper that automatically gathers materials chamber-type press filter is shaped as the shape of falling truncated rectangular pyramids.
4. automatically the gather materials poly aluminium chloride of chamber-type press filter of use according to claim 1 is produced acid-soluble reactive system, it is characterized in that: described acid-soluble reactive system also comprises tail gas absorber, directly over the press filtration group of the described chamber-type press filter that automatically gathers materials, be provided with gas skirt, the exhaust gas entrance of described tail gas absorber is communicated with the gas skirt of reaction tank, reaction tank transfer pond and the chamber-type press filter that automatically gathers materials respectively.
5. automatically the gather materials poly aluminium chloride of chamber-type press filter of use according to claim 1 is produced acid-soluble reactive system, it is characterized in that: described reaction tank, reaction tank transfer pond and flocculating agent formulation tank are equipped with agitator.
CN201320762756.0U 2013-11-28 2013-11-28 Acid-soluble reaction system for producing polyaluminum chloride by employing automatic aggregating van-type press filter Expired - Fee Related CN203683125U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106345158A (en) * 2016-11-18 2017-01-25 广西金邦泰科技有限公司 Environment-friendly modernized filter pressing device capable of orderly collecting solid and liquid

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106345158A (en) * 2016-11-18 2017-01-25 广西金邦泰科技有限公司 Environment-friendly modernized filter pressing device capable of orderly collecting solid and liquid

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Granted publication date: 20140702

Termination date: 20171128