CN203513547U - Silicone rubber production equipment - Google Patents

Silicone rubber production equipment Download PDF

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Publication number
CN203513547U
CN203513547U CN201320604700.2U CN201320604700U CN203513547U CN 203513547 U CN203513547 U CN 203513547U CN 201320604700 U CN201320604700 U CN 201320604700U CN 203513547 U CN203513547 U CN 203513547U
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communicated
powder
storage tank
outlet
materials
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Expired - Fee Related
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CN201320604700.2U
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Chinese (zh)
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丁大宏
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Shandong Feidu Glue Industry Science & Technology Co Ltd
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Shandong Feidu Glue Industry Science & Technology Co Ltd
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Abstract

The utility model provides silicone rubber production equipment. The equipment comprises a reaction kettle and a storage tank, wherein a powder inlet and a powder outlet are respectively formed in the top and the bottom of the reaction kettle; the powder outlet is communicated with a screw conveyor; an adsorption port is formed in the upper part of the discharge end of the screw conveyor; a raw material return port is formed in the top of the reaction kettle; a storage tank inlet and a storage tank outlet are respectively formed in the top and the bottom of the storage tank; the storage inlet is communicated with the adsorption port through a feed pipeline; the storage tank outlet is communicated with the raw material return port through a discharge pipeline; a pressure gauge and a vacuum pump communicated with the cavity of the storage tank are arranged on the storage tank; a powder splash prevention device is arranged at the powder inlet, and the inlet of the powder splash prevention device is communicated with a powder feed device; a jacket outlet of the reaction kettle is communicated with a residual heat recycling device. The silicone rubber production equipment relates to the technical field of silicone rubber, and can be used for solving the problems of overfall of added powder, continuous feed unavailability, reaction remained liquid raw material collection, and extra energy in drying and insulation of reacting raw materials in the prior art.

Description

Silicon rubber production unit
Technical field
The utility model relates to silicon rubber technical field, refers to especially a kind of silicon rubber production unit.
Background technology
Organosilicon material refers to polysiloxane compounds, and its molecular structure had both contained organic group, contains again inorganic structure, and this special composition and molecular structure make it integrate the function of organic characteristic and inorganics.Compare with other macromolecular materials, the outstanding properties of organosilicon product is good heatproof characteristic (60 ℃~250 ℃), electrical insulation capability, its dielectric loss, proof voltage, resistance to electric arc, resistance to corona, volume resistivity and surface resistivity etc. all come out at the top in insulating material.This material can reach decades in work-ing life under physical environment, and its resistance to biological aging without rejection, has good anticoagulation function with animal body, so the Application Areas of organosilicon material also comprises sealing, encapsulation, bonding etc.
The development of organosilicon material is keeping higher speed always, and market mainly concentrates on the U.S., Europe, San Ge region, Asia, and nineteen forty-seven is 1000 tons, to 2005, has reached 1,500,000 tons.
Silicone adhesive english name is SILICONE, is organosilicon material product, and the bonding force of silicone glass cement is strong, and tensile strength is large, has again weathering resistance, vibration resistance simultaneously, and moistureproof, anti-foul smell and adapt to the feature that cold and hot variation is large.In addition its suitability more widely, can realize bonding between most of building material products, so using value is very large.Produce silicone adhesive except 107 gum, in other constituents, the overwhelming majority is powder, and powder is nano level, and adularescent, black also have other pigment.
The opening for feed of existing reactor is generally a larger ring flange, generally, by operator, directly packed powder is directly rendered to reactor inside by opening for feed, this feeding mode flour dust overflow is the most serious, on the infringement of environment be also maximum on the healthy impact of operator; Existing feeding mode also has and to feed intake by transmission rig, because reactor opening for feed is standard interface, that can not seal with transmission rig is connected, therefore this mode feeds intake and when being transferred to opening for feed, has equally the problem of flour dust overflow, and just impact is slightly less than the direct input of operator.
In the production or reaction process of existing silicon rubber, all need to add the raw material of powder, in powder adition process, have a large amount of flour dust overflows, cause the waste of material, excessive dust can affect operating environment health simultaneously, and can cause damage to operator's health.Also the device that has at present vacuum suck charging, but these devices do not have for silicon rubber preparation field, and current vacuum absorption device can not continuous charging.
In the production or reaction process of existing silicon rubber, need use DMC, DMC is dimethyl ring siloxane mixture, chemical formula is [(CH3) 2SIO] n, n=3, 4, 5, 6 Primary Speciation dimethyl ring body siloxanes are to take dimethyldichlorosilane(DMCS) as main raw material, through hydrolysis, silica (Si-O) key of take is main chain, on Siliciumatom, directly connect the organic and inorganic compound of organic radical, Primary Speciation dimethyl ring body siloxane molecule structure presents ring-type, mainly comprise hexamethyl cyclotrisiloxane (D3), octamethylcyclotetrasiloxane (D4), decamethylcyclopentaandoxane (D5), ten diformazan basic ring six siloxanes (D6), hexamethyl cyclotrisiloxane (D3), octamethylcyclotetrasiloxane (D4), decamethylcyclopentaandoxane (D5), ten diformazan basic ring six siloxanes (D6) content reach more than 50% water white transparency or milky white liquid, flammable, free from extraneous odour, water insoluble, be dissolved in the organic solvents such as benzene.Be mainly used in carrying out silicone oil, silicon rubber and the silicone resin etc. that ring-opening polymerization becomes different polymerization degree.DMC is liquid material, in reaction process, in order to determine the abundant reaction of another kind of reactant, the DMC adding is excessive adding, in reacted silicon rubber, DMC has residue, existing treatment process normally by the silicon rubber of preparation and unnecessary DMC simultaneously from material outlet take out and transfer to container, carry out separated, DMC after separation can add reactor for the preparation of the reaction of silicon rubber again, the separation of this DMC and again utilize cumbersome, waste a large amount of human and material resources, and efficiency is not high.
The production reaction raw materials used of existing silicon rubber, need to be kept in 17 ℃ of above environment, if the environment of preserving, lower than 17 ℃, easily freezes or caking, is unfavorable for follow-up reaction while preparing silicon rubber.In the lower region of temperature or winter, also need these raw materials to be additionally incubated processing, existing preserving type is all kept at material in kiln or moist closet, at kiln or inner the increasing of moist closet, regulates the device of temperature to regulate, and this mode need to additionally provide the energy.The steam of reactor is after heating reactor, and the secondary steam of discharging by Jacket outlet also has the temperature of 60 ℃ of left and right, and the processing mode of existing secondary steam is all directly emptying substantially, causes the waste of the energy.
Utility model content
The utility model proposes a kind of silicon rubber production unit, solved powder in prior art add fashionable excessive, can not continuous charging, utilize the problem of additional energy source when reacting that remaining liquid starting material is collected, reaction raw materials is dried and being incubated.
The technical solution of the utility model is achieved in that
Silicon rubber production unit, comprise reactor, described reactor top and bottom are respectively equipped with powder opening for feed and discharge port, described discharge port is communicated with worm conveyor, the discharge end top of described worm conveyor is provided with adsorption orifice, described reactor top is also provided with raw material return port, also comprise storage tank, described storage tank top and bottom are respectively equipped with storage tank import and storage tank outlet, described storage tank import is communicated with by feed pipe with described adsorption orifice, described storage tank outlet is communicated with by discharge pipe with described raw material return port, described storage tank is provided with tensimeter and the vacuum pump being communicated with storage tank inner chamber, described powder opening for feed is provided with and prevents powder splinter device, describedly prevent that the import of powder splinter device is communicated with powder feeder, the Jacket outlet of described reactor is communicated with heat recycling device.
Described feed pipe is provided with negative-pressure adsorption control valve.Described discharge pipe is provided with discharging control valve.
As the improvement to technique scheme, described in prevent that the powder feeding unit that splashes from comprising: round shape dw, the bottom of described round shape dw is connected with described powder opening for feed, top is provided with dust guard; Charging vertical tube, is located at described round shape dw inner chamber, and described charging riser upper portions runs through described dust guard; Feeding bent pipe, top is communicated with the bottom of described charging vertical tube, and bottom extends downward in described reactor; Described charging vertical tube outer wall is provided with downward-sloping baffle plate, and the base of described baffle plate is connected with the inwall of described round shape dw.Between the bottom of described round shape dw and described opening for feed, be provided with seal gasket.Described charging vertical tube and feeding bent pipe removably connect.
As the further improvement to technique scheme, described reactor one side is provided with fixed support, and described fixed support comprises vertical rack and horizontal support, and described round shape dw is fixedly connected with described horizontal support.
As the improvement to technique scheme, described powder feeder comprises: the first materials-stored box, bottom by powder feed pipe with described in prevent that the import of powder splinter device is communicated with; The second materials-stored box, is located at described the first materials-stored box one side, and is equipped with Link Port on described the first materials-stored box and the adjoining sidewall of described the second materials-stored box; Pusher, be located at described the second materials-stored box, with described the first materials-stored box back to a side, described pusher comprises: moving conduit, run through the sidewall of described the second materials-stored box; Control lever, is located in described moving conduit, and the inner is fixedly connected with promoting piston, and outer end is connected with drive unit, and described promotion piston is corresponding in position with described Link Port.
As the further improvement to technique scheme, the sidewall of described the first materials-stored box is provided with vibrator.
As the improvement to technique scheme, described heat recycling device comprises: moist closet, be provided with moist closet import and moist closet outlet, and described moist closet import is communicated with by gas-liquid separator with described Jacket outlet; Thermo-insulating pipe line, is located at described moist closet inner chamber, comprises pipeline import and pipeline outlet, and described pipeline import is communicated with described moist closet import, and described pipeline outlet is communicated with moist closet outlet.
As the further improvement to technique scheme, described thermo-insulating pipe line comprises the steam branch road that at least two-way is set up in parallel, and described steam branch road is provided with drain valve.The metal tube that described steam branch road is hollow.
As the improvement to technique scheme, described reactor inside is provided with whipping appts, and described whipping appts consists of stir shaft and the stirring rake that is fixed on stir shaft bottom, and described stirring rake comprises stirring rake and lower stirring paddle from top to bottom.
As the further improvement to technique scheme, described stir shaft top extends upwardly to reactor outside and is connected with drive-motor by step-down gear.
Adopted after technique scheme, the beneficial effects of the utility model are:
The utility model has been set up a storage tank, storage tank is adsorbed onto remaining liquid starting material in worm conveyor in storage tank by vacuum suck, when needs are used, directly by storage tank, the liquid starting material of storage is sent in reactor, for reaction next time, the collection of remaining liq raw material and the efficiency of second stage employ in reactor have been improved greatly.
The utility model is provided with round shape dw, avoids flour dust overflow; Also be provided with charging vertical tube and feeding bent pipe, better solved the problem of flour dust overflow, when powder is entered reactor inside and is fallen by feeding-passage like this, not directly to fall, but carried out a buffering by curved surface feed-pipe, after buffering, drop into the situation that reactor inside causes flour dust overflow and improved preferably, further reduced the phenomenon of flour dust overflow.Can reduce the excessive material waste causing of powder, can avoid excessive dust to affect the problem of environmental health, infringement operator ' s health simultaneously.Be provided with fixed support, can play the effect of stationary cylinder shape dw.Also be provided with seal gasket, by the buffering of seal gasket, can avoid the hard problem that contacts easy damage device or equipment of seal closure bottom and opening for feed end face.
The secondary steam that the utility model is discharged reactor heating jacket carries out second stage employ, first by gas-liquid separator, partial condensation water is discharged, steam is introduced in moist closet by pipeline, and by thermo-insulating pipe line by the thermal radiation of steam in moist closet, can guarantee that temperature in moist closet, more than 20 ℃, does not need additionally to take Insulation can solve the storage problem of silicon rubber reaction raw materials.Thermo-insulating pipe line comprises the steam branch road that at least two-way is set up in parallel, and the better distribution of heat energy and the radiation of steam in keeping pipeline are conducted in moist closet, and steam branch road is more, is more convenient to distribute.Certainly, also can adopt a vapour line, this pipeline is tortuous setting in moist closet, but arranges like this, may cause vapor pressure not and the long problem that causes producing water of condensation of vapour line.Steam branch road of the present utility model is provided with drain valve, and better the efficiency of the water of condensation in discharged steam branch road and raising steam cycle, preferably resolves the problem that the interior generation of steam branch road water of condensation affects steam cycle.
Accompanying drawing explanation
In order to be illustrated more clearly in the utility model embodiment or technical scheme of the prior art, to the accompanying drawing of required use in embodiment or description of the Prior Art be briefly described below, apparently, accompanying drawing in the following describes is only embodiment more of the present utility model, for those of ordinary skills, do not paying under the prerequisite of creative work, can also obtain according to these accompanying drawings other accompanying drawing.
Fig. 1 is the structural representation of a kind of embodiment of the utility model;
Fig. 2 prevents the structural representation of powder splinter device in the utility model;
In figure: 1. reactor, 11. powder opening for feeds, 12. discharge ports, 13. raw material return ports, 14. stir shafts, 15. Jacket outlet, 2. worm conveyor, 21. adsorption orifices, 3. storage tank, 31. feed pipes, 32. discharge pipes, 33. tensimeters, 34. vacuum pumps, 4. prevent powder splinter device, 41. round shape dw, 42. dust guards, 43. charging vertical tubes, 44. feeding bent pipes, 45. baffle plates, 5. powder feeder, 51. first materials-stored box, 52. second materials-stored box, 53. Link Ports, 54. moving conduits, 55. control levers, 56. vibrators, 6. fixed support, 61. vertical racks, 62. horizontal supports, 7. moist closet, 71. moist closet imports, 72. moist closet outlets, 73. steam branch roads, 74. drain valves, 8. gas-liquid separator.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the utility model embodiment is clearly and completely described, obviously, described embodiment is only the utility model part embodiment, rather than whole embodiment.Embodiment based in the utility model, those of ordinary skills are not making the every other embodiment obtaining under creative work prerequisite, all belong to the scope of the utility model protection.
Embodiment:
As depicted in figs. 1 and 2, silicon rubber production unit, comprise reactor 1, reactor 1 top and bottom are respectively equipped with powder opening for feed 11 and discharge port 12, discharge port 12 is communicated with worm conveyor 2, the discharge end top of worm conveyor 2 is provided with adsorption orifice 21, reactor 1 top is also provided with raw material return port 13, also comprise storage tank 3, storage tank 3 tops and bottom are respectively equipped with storage tank import and storage tank outlet, storage tank import is communicated with by feed pipe 31 with adsorption orifice 21, storage tank outlet is communicated with by discharge pipe 32 with raw material return port 13, storage tank 3 is provided with tensimeter 33 and the vacuum pump 34 being communicated with storage tank 3 inner chambers, powder opening for feed 11 is provided with and prevents powder splinter device 4, the import that prevents powder splinter device 4 is communicated with powder feeder 5, the Jacket outlet 15 of reactor 1 is communicated with heat recycling device.
Feed pipe 31 is provided with negative-pressure adsorption control valve.Discharge pipe 32 is provided with discharging control valve.
Prevent that the powder feeding unit that splashes from comprising: round shape dw 41, the bottom of round shape dw 41 is connected with powder opening for feed 11, and top is provided with dust guard 42; Charging vertical tube 43, is located at round shape dw 41 inner chambers, and dust guard 42 is run through on charging vertical tube 43 tops; Feeding bent pipe 44, top is communicated with the bottom of charging vertical tube 43, and bottom extends downward in reactor 1; Charging vertical tube 43 outer walls are provided with downward-sloping baffle plate 45, and the base of baffle plate 45 is connected with the inwall of round shape dw 41.Between the bottom of round shape dw 41 and opening for feed, be provided with seal gasket.Charging vertical tube 43 and feeding bent pipe 44 removably connect.
Reactor 1 one sides are provided with fixed support 6, and fixed support 6 comprises vertical rack 61 and horizontal support 62, and round shape dw 41 is fixedly connected with horizontal support 62.
Powder feeder 5 comprises: the first materials-stored box 51, and bottom is communicated with the import that prevents powder splinter device 4 by powder feed pipe; The second materials-stored box 52, is located at the first materials-stored box 51 1 sides, and is equipped with Link Port 53 on the first materials-stored box 51 and the adjoining sidewall of the second materials-stored box 52; Pusher, be located at the second materials-stored box 52, with the first materials-stored box 51 back to a side, pusher comprises: moving conduit 54, run through the sidewall of the second materials-stored box 52; Control lever 55, is located in moving conduit 54, and the inner is fixedly connected with promoting piston, and outer end is connected with drive unit, promotes piston corresponding in position with Link Port 53.
The sidewall of the first materials-stored box 51 is provided with vibrator 56.
Heat recycling device comprises: moist closet 7, be provided with moist closet import 71 and moist closet outlet 72, and moist closet import 71 is communicated with by gas-liquid separator 8 with Jacket outlet 15; Thermo-insulating pipe line, is located at moist closet 7 inner chambers, comprises pipeline import and pipeline outlet, and pipeline import is communicated with moist closet import 71, and pipeline outlet is communicated with moist closet outlet 72.
Thermo-insulating pipe line comprises the steam branch road 73 that at least two-way is set up in parallel, and steam branch road 73 is provided with drain valve 74.The metal tube that steam branch road 73 is hollow.
Reactor 1 inside is provided with whipping appts, and whipping appts consists of stir shaft 14 and the stirring rake that is fixed on stir shaft 14 bottoms, and stirring rake comprises stirring rake and lower stirring paddle from top to bottom.
Stir shaft 14 tops extend upwardly to reactor 1 outside and are connected with drive-motor by step-down gear.
The foregoing is only preferred embodiment of the present utility model; not in order to limit the utility model; all within spirit of the present utility model and principle, any modification of doing, be equal to replacement, improvement etc., within all should being included in protection domain of the present utility model.

Claims (9)

1. silicon rubber production unit, comprise reactor, described reactor top and bottom are respectively equipped with powder opening for feed and discharge port, described discharge port is communicated with worm conveyor, it is characterized in that: the discharge end top of described worm conveyor is provided with adsorption orifice, described reactor top is also provided with raw material return port, also comprise storage tank, described storage tank top and bottom are respectively equipped with storage tank import and storage tank outlet, described storage tank import is communicated with by feed pipe with described adsorption orifice, described storage tank outlet is communicated with by discharge pipe with described raw material return port, described storage tank is provided with tensimeter and the vacuum pump being communicated with storage tank inner chamber, described powder opening for feed is provided with and prevents powder splinter device, describedly prevent that the import of powder splinter device is communicated with powder feeder, the Jacket outlet of described reactor is communicated with heat recycling device.
2. silicon rubber production unit as claimed in claim 1, is characterized in that: described in prevent that the powder feeding unit that splashes from comprising:
Round shape dw, the bottom of described round shape dw is connected with described powder opening for feed, and top is provided with dust guard;
Charging vertical tube, is located at described round shape dw inner chamber, and described charging riser upper portions runs through described dust guard;
Feeding bent pipe, top is communicated with the bottom of described charging vertical tube, and bottom extends downward in described reactor;
Described charging vertical tube outer wall is provided with downward-sloping baffle plate, and the base of described baffle plate is connected with the inwall of described round shape dw.
3. silicon rubber production unit as claimed in claim 2, is characterized in that: described reactor one side is provided with fixed support, and described fixed support comprises vertical rack and horizontal support, and described round shape dw is fixedly connected with described horizontal support.
4. silicon rubber production unit as claimed in claim 1, is characterized in that: described powder feeder comprises:
The first materials-stored box, bottom by powder feed pipe with described in prevent that the import of powder splinter device is communicated with;
The second materials-stored box, is located at described the first materials-stored box one side, and is equipped with Link Port on described the first materials-stored box and the adjoining sidewall of described the second materials-stored box;
Pusher, be located at described the second materials-stored box, with described the first materials-stored box back to a side, described pusher comprises: moving conduit, run through the sidewall of described the second materials-stored box; Control lever, is located in described moving conduit, and the inner is fixedly connected with promoting piston, and outer end is connected with drive unit, and described promotion piston is corresponding in position with described Link Port.
5. silicon rubber production unit as claimed in claim 4, is characterized in that: the sidewall of described the first materials-stored box is provided with vibrator.
6. silicon rubber production unit as claimed in claim 1, is characterized in that: described heat recycling device comprises:
Moist closet, is provided with moist closet import and moist closet outlet, and described moist closet import is communicated with by gas-liquid separator with described Jacket outlet;
Thermo-insulating pipe line, is located at described moist closet inner chamber, comprises pipeline import and pipeline outlet, and described pipeline import is communicated with described moist closet import, and described pipeline outlet is communicated with moist closet outlet.
7. silicon rubber production unit as claimed in claim 6, is characterized in that: described thermo-insulating pipe line comprises the steam branch road that at least two-way is set up in parallel, and described steam branch road is provided with drain valve.
8. the silicon rubber production unit as described in claim 1-7 any one, it is characterized in that: described reactor inside is provided with whipping appts, described whipping appts consists of stir shaft and the stirring rake that is fixed on stir shaft bottom, and described stirring rake comprises stirring rake and lower stirring paddle from top to bottom.
9. silicon rubber production unit as claimed in claim 8, is characterized in that: described stir shaft top extends upwardly to reactor outside and is connected with drive-motor by step-down gear.
CN201320604700.2U 2013-09-27 2013-09-27 Silicone rubber production equipment Expired - Fee Related CN203513547U (en)

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Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104368292A (en) * 2014-11-07 2015-02-25 广德瑞邦涂料有限公司 Anodic electrophoretic paint resin synthesis reaction kettle
CN107487598A (en) * 2016-11-15 2017-12-19 中煤第五建设有限公司 A kind of concrete material discharging of roadway construction, feeding system
CN112742334A (en) * 2020-12-14 2021-05-04 湖南福千府生物科技有限公司 Sodium sulfite preparation is with raw materials device that mixes equally

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104368292A (en) * 2014-11-07 2015-02-25 广德瑞邦涂料有限公司 Anodic electrophoretic paint resin synthesis reaction kettle
CN107487598A (en) * 2016-11-15 2017-12-19 中煤第五建设有限公司 A kind of concrete material discharging of roadway construction, feeding system
CN112742334A (en) * 2020-12-14 2021-05-04 湖南福千府生物科技有限公司 Sodium sulfite preparation is with raw materials device that mixes equally

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Granted publication date: 20140402

Termination date: 20170927