CN203487069U - Production system of polyquaternium-10 or positive ion guar gum - Google Patents

Production system of polyquaternium-10 or positive ion guar gum Download PDF

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Publication number
CN203487069U
CN203487069U CN201320205934.XU CN201320205934U CN203487069U CN 203487069 U CN203487069 U CN 203487069U CN 201320205934 U CN201320205934 U CN 201320205934U CN 203487069 U CN203487069 U CN 203487069U
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China
Prior art keywords
polyquaternium
production system
storage tank
solid
alcohol storage
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Expired - Fee Related
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CN201320205934.XU
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Chinese (zh)
Inventor
张克伦
黄兴春
黄晓科
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CHONGQING DONGHUAN SCIENCE AND TECHNOLOGY DEVELOPMENT Co Ltd
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CHONGQING DONGHUAN SCIENCE AND TECHNOLOGY DEVELOPMENT Co Ltd
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Abstract

The utility model provides a production system of polyquaternium-10 or positive ion guar gum. The production system of polyquaternium-10 or positive ion guar gum comprises a reaction kettle, a solid-liquid separation device and a drying device, wherein the solid-liquid separation device is connected with the reaction kettle; the drying device is connected with the solid-liquid separation device. The production system of polyquaternium-10 or positive ion guar gum is characterized by also comprising a recycled alcohol storage tank, a rectifying tower and a rectifying alcohol storage tank, wherein the rectifying tower is connected with the recycled alcohol storage tank; the rectifying alcohol storage tank is connected with the rectifying tower, and is connected with the solid-liquid separation device and the drying device respectively. According to the polyquaternium-10 or positive ion guar gum produced by the production system provided by the utility model, the purity is high, the impurity content is extremely low, the granularity is homogeneous, water solubility and adsorption capability are high, the quality of polyquaternium-10 or positive ion guar gum is good, the production process is optimized, the yield is increased, raw materials and energy consumption are reduced, and 230kg of isopropanol can be saved in per ton of produced polyquaternium-10 or positive ion guar gum.

Description

The production system of a kind of Polyquaternium-10 or positively charged ion melon glue
Technical field
The utility model relates to chemical industry equipment field, is specifically related to the production system of Polyquaternium-10 or positively charged ion melon glue.
Background technology
Polyquaternium-10 is a kind of cationic cellulose polymer, can be compatible with negatively charged ion, positively charged ion, nonionic and zwitterionics, pungency is low, its unique cationic properties can be repaired impaired hair protein matrix, keep hair to moisten, give the superior carding property of hair and glossy smooth sensation.Can be applicable to skin care aspect, can keep skin moistening, prevent skin bursting by freezing, make skin smooth soft and moist.For hair, avidity is strong, and maintenance hair jag forms transparent, continuous thin film on hair.Splendid performance of keeping humidity is provided, improves impaired hair quality, for skin, splendid use rear sense, improve skin anti-uv-ray, good moisturizing performance.The production of domestic production Polyquaternium-10, take Mierocrystalline cellulose and etherifying agent as raw material.
Cation guar gum is a kind of high molecular polymer, and its chemical name is guar gum hydroxypropyl-trimethyl ammonium chloride.There is good consistency with negatively charged ion, zwitter-ion and tensio-active agent, can be used in the product of various surfactants, extremely gentle to skin and eyes, can slow down the pungency of tensio-active agent in formulation product.
At present, the production of Polyquaternium-10 or positively charged ion melon glue, often occurs that product purity is not high, bad, the problem such as raw material consumption is large, energy consumption is large.
Summary of the invention
The purpose of this utility model is to provide a kind of reduction energy consumption, the production system of the Polyquaternium-10 improving the quality of products.
The purpose of this utility model realizes by following measures:
A kind of production system, comprise reactor, the equipment for separating liquid from solid being connected with reactor, the drying installation being connected with equipment for separating liquid from solid, characterized by further comprising and reclaim alcohol storage tank, the rectifying tower being connected with recovery alcohol storage tank, the rectifying alcohol storage tank being connected with rectifying tower, described recovery alcohol storage tank is connected with equipment for separating liquid from solid, drying installation respectively.
Aforesaid reaction vessel is Double-jacketed stainless steel cauldron, and bottom chuck adopts heat-conducting oil heating, and sidewall chuck adopts circulating water cooling, double-deck stirring.Described whizzer is preferably two-stage material-pushing centrifuge.
Above-mentioned equipment for separating liquid from solid comprises the first whizzer, washing kettle, the second whizzer being connected successively, and the first whizzer is connected with reactor, and the second whizzer is connected with drying installation.
Above-mentioned drying installation comprises the rake type drier being connected with equipment for separating liquid from solid, the pneumatic drier being connected with described rake type drier.
Said flow drying machine is with cloth bag suction cleaner.
Above-mentioned production system, also comprises the cooling crush machine being connected with pneumatic drier, the vibratory screening apparatus being connected with cooling crush machine.
Above-mentioned production system, also comprises the condenser being connected with rake type drier, and above-mentioned recovery alcohol storage tank is connected with the first whizzer, the second whizzer, described condenser, pneumatic drier respectively.
beneficial effect
1. the product purity that the utility model production obtains is high, and foreign matter content is extremely low, homogeneous grain diameter, water-soluble and high adsorption capacity, superior product quality.
2. the utility model has been optimized Production Flow Chart, and output improves, and raw material, energy consumption all have minimizing, and 1 ton of product of every production can be saved 230 kilograms of Virahols.
Accompanying drawing explanation
Fig. 1 is the production system schematic diagram of embodiment.
Embodiment
A kind of production system, comprise reactor 1, the screw rod impeller pump 2 being connected with reactor 1, the first whizzer 3 being connected with screw rod impeller pump, the washing kettle 4 being connected with the first whizzer 3, the second whizzer 5 being connected with washing kettle 4, the rake type drier 6 being connected with the second whizzer 5, the pneumatic drier 7 being connected with rake type drier 6, the pulverizer 8 with refrigerating unit being connected with pneumatic drier 7, the vibratory screening apparatus being connected with pulverizer 8, also comprise the condenser 10 being connected with rake type drier 6, reclaim alcohol storage tank 11, the rectifying tower 12 being connected with recovery alcohol storage tank 11, the rectifying alcohol storage tank 13 being connected with rectifying tower 12, reclaim alcohol storage tank 11 respectively with condenser 10, the first whizzer 3, the second whizzer 5, , pneumatic drier 7 is connected.
Reactor 1 is Double-jacketed stainless steel cauldron, and bottom chuck adopts heat-conducting oil heating, and sidewall chuck adopts circulating water cooling, double-deck stirring.Described whizzer is preferably two-stage material-pushing centrifuge.
Raw material is normal-temperature reaction in reactor, product is by centrifugal pumping to the first whizzer, solvent enters to reclaim alcohol storage tank, solid product is sent into washing tower, after washed with isopropyl alcohol, send into the second whizzer separated, solvent enters to reclaim alcohol storage tank, it is dry that solid product is sent into rake type drier, residual solvent reclaims alcohol storage tank through cooling the entering of condensing tower, solid product is dry through pneumatic dryer, residual solvent enters and reclaims alcohol storage tank, , sending into pulverizer pulverizes with cooling again, cross 60-80 mesh sieve, obtain Polyquaternium-10 and positively charged ion melon glue, recovery solvent in recovery alcohol storage tank is after rectifying tower is processed, enter rectifying alcohol storage tank, standby.

Claims (5)

1. the production system of a Polyquaternium-10 or positively charged ion melon glue, comprise reactor, the equipment for separating liquid from solid being connected with reactor, the drying installation being connected with equipment for separating liquid from solid, characterized by further comprising and reclaim alcohol storage tank, the rectifying tower being connected with recovery alcohol storage tank, the rectifying alcohol storage tank being connected with rectifying tower, described recovery alcohol storage tank is connected with equipment for separating liquid from solid, drying installation respectively.
2. the production system of Polyquaternium-10 or positively charged ion melon glue as claimed in claim 1, described drying installation comprises the rake type drier being connected with equipment for separating liquid from solid, the pneumatic drier being connected with described rake type drier.
3. the production system of Polyquaternium-10 or positively charged ion melon glue as claimed in claim 2, also comprises the cooling crush machine being connected with pneumatic drier, the vibratory screening apparatus being connected with cooling crush machine.
4. the production system of Polyquaternium-10 or positively charged ion melon glue as described in claim 1,2 or 3, described equipment for separating liquid from solid comprises the first whizzer, washing kettle, the second whizzer being connected successively; The first whizzer is connected with reactor, and the second whizzer is connected with drying installation.
5. the production system of Polyquaternium-10 or positively charged ion melon glue as claimed in claim 4, also comprises the condenser being connected with rake type drier, and described recovery alcohol storage tank is connected with the first whizzer, the second whizzer, described condenser, pneumatic drier respectively.
CN201320205934.XU 2013-04-22 2013-04-22 Production system of polyquaternium-10 or positive ion guar gum Expired - Fee Related CN203487069U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201320205934.XU CN203487069U (en) 2013-04-22 2013-04-22 Production system of polyquaternium-10 or positive ion guar gum

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201320205934.XU CN203487069U (en) 2013-04-22 2013-04-22 Production system of polyquaternium-10 or positive ion guar gum

Publications (1)

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CN203487069U true CN203487069U (en) 2014-03-19

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108314637A (en) * 2018-04-17 2018-07-24 兖矿水煤浆气化及煤化工国家工程研究中心有限公司 A kind of preparation method and process units of thioacetic acid
CN108752493A (en) * 2018-05-24 2018-11-06 重庆美杉蓝科技发展有限公司 A kind of cation guar gum production technology

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108314637A (en) * 2018-04-17 2018-07-24 兖矿水煤浆气化及煤化工国家工程研究中心有限公司 A kind of preparation method and process units of thioacetic acid
CN108314637B (en) * 2018-04-17 2023-10-24 兖矿水煤浆气化及煤化工国家工程研究中心有限公司 Preparation method and production device of thioacetic acid
CN108752493A (en) * 2018-05-24 2018-11-06 重庆美杉蓝科技发展有限公司 A kind of cation guar gum production technology

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140319

Termination date: 20150422

EXPY Termination of patent right or utility model