CN203483902U - Spiniform still head capable of quickly replacing liquid bottle for preparing essences and perfumes - Google Patents
Spiniform still head capable of quickly replacing liquid bottle for preparing essences and perfumes Download PDFInfo
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- CN203483902U CN203483902U CN201320610847.2U CN201320610847U CN203483902U CN 203483902 U CN203483902 U CN 203483902U CN 201320610847 U CN201320610847 U CN 201320610847U CN 203483902 U CN203483902 U CN 203483902U
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- thorn
- cucurbit
- spiniform
- still head
- tube connector
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Abstract
The utility model discloses a spiniform still head capable of quickly replacing a liquid bottle for preparing essences and perfumes. The spiniform still head comprises a distilling flask connecting pipe, an inclined elbow pipe and a spiniform fractional column, wherein a distilling flask connection end is formed at the lower end of the distilling flask connecting pipe; a ventilation end is arranged at the upper end of the distilling flask connecting pipe; the lower end of the inclined elbow pipe is communicated with the middle part of the distilling flask connecting pipe; the upper end is communicated with the lower end of the spiniform fractional column; a thermometer inserting end is formed at the upper end of the spiniform fractional column; a glass thorn is formed at the inner wall of the lower part; a condenser connecting branch pipe is arranged at the lateral part; a ventilation plug is arranged at the ventilation end of the distilling flask connecting pipe; a vent hole is formed in the ventilation plug; an airway tube is inserted into the vent hole; an open and close valve is arranged on the airway tube. The spiniform still head does not need to interrupt vacuum when the liquid bottle needs to be replaced, the replacement time is reduced, a stable air pressure change inside the distilling head is achieved as long as the open and close valve of the airway tube is slowly closed in the process of continuing to distill, and the material rushing phenomenon is avoided.
Description
Technical field
The utility model relates to for essence and flavoring agent production distillation apparatus, relates in particular to a kind of thorn shape fractional still head.
Background technology
Along with the development of social life, essence and flavoring agent extensive use in social life, people have all proposed more and more higher requirement to the production efficiency of essence and flavoring agent and quality.And in the production process of essence and flavoring agent, the rectifying between different component or fractionation are important steps in whole production process, the purity of product shunting directly affects the final mass of product.
Existing fractionating device generally comprises thorn shape fractional still head, thermometer, condenser pipe, adapter and connects liquid bottle, and adapter is provided with vacuum pumping hole.Thorn shape fractional still head is connected with cucurbit, thermometer and condenser pipe, and adapter is connected with condenser pipe end, connects liquid bottle and is connected with adapter end.Existing thorn shape fractional still head is provided with cucurbit link, ventilation end, thermometer link and condenser pipe link, and ventilation end is provided with rubber stopper; In thorn shape fractional still head, be provided with glass thorn.
During fractionating device decompression distillation, in whole fractionating device, be vacuum state.After the solvent of fractionation seethes with excitement in cucurbit, steam enters thorn shape fractional still head, and partial condensation becomes liquid, and the content due to low boiling point component in this liquid is more, so its boiling point is also just low than the fluid temperature in cucurbit.When another part steam in cucurbit rises in thorn shape fractional still head, just carry out heat exchange with the liquid of these condensations, it is seethed with excitement again, the steam itself rising is partly condensed, therefore, produced again once new liquid-steam balance, the low boiling point component of result in steam increases again to some extent.Steam finally connects liquid bottle through condenser pipe and adapter inflow.
In above-mentioned fractional distillation process, the structure of thorn shape fractional still head is crucial.In above-mentioned fractional distillation process, when connecing liquid bottle graft and needing to change after full, must first disconnect vacuum, then take out the rubber stopper of thorn shape fractional still head ventilation end, make whole fractionating device recover normal pressure, just can connect liquid bottle and change.Connect after the replacing of liquid bottle, must again rubber stopper be got back into thorn shape fractional still head ventilation end, then recover vacuum, proceed above-mentioned decompression distillation.Whole process needs constantly to open, disconnect vacuum, causes process extremely loaded down with trivial details, inefficiency; And when vacuum is recovered, can cause fractional still head internal gas pressure sharply to change, and the liquid distilling in stoste and thorn shape fractional still head is inhaled in condenser pipe and adapter, rear inflow connects liquid bottle, just greatly reduces the purity of fractionation, directly affects the quality of essence and flavoring agent.
Summary of the invention
The utility model is for complex steps during changing-over liquid bottle more in prior art, must first disconnect vacuum, recover again the obvious deficiency of vacuum, and be prone to punching material while again recovering vacuum and affect the defect of fractionating effect, provide a kind of essence and flavoring agent to prepare the thorn shape fractional still head that connects liquid bottle with fast changeable.
In order to solve the problems of the technologies described above, the utility model is solved by following technical proposals:
Essence and flavoring agent preparation connects a thorn shape fractional still head for liquid bottle with fast changeable, comprise cucurbit tube connector, oblique bend pipe and thorn shape still; Described cucurbit tube connector lower end is cucurbit link, and upper end is ventilation end; The lower end of described oblique bend pipe is communicated with cucurbit tube connector middle part, and upper end is communicated with the lower end of thorn shape still; The upper end of described thorn shape distillation column is thermometer insertion end, and lower inner wall is provided with glass thorn, and sidepiece is provided with condenser connecting branch; The ventilation end of described cucurbit tube connector is provided with breather plug, and described breather plug is provided with passage, on described passage, is inserted with wireway, and described wireway is provided with open and close valve.
The above-described configuration, the ventilation connecting pipe ends distillation flask provided vent plug and vent plug in the plug has a vent opening and closing valve guide tube, inside the head can be achieved using this distillation airway with the atmosphere, so that when the distillation process needs to be replaced when wetted bottled, simply open the airway opening and closing the valve, so that the air entering the distillation head, so that internal recovery atmospheric distillation head, without disconnecting the vacuum, you can replace the wetted bottled reduce replacement time, and distillation continued, gradually closed as long as the opening and closing of the valve guide tube, distillation head, a smooth change of internal pressure, to avoid the appearance of the phenomenon of red material.
As preferably, the inwall of described cucurbit tube connector is being provided with the first spacing glass thorn near cucurbit link place, and described the first spacing glass thorn top is provided with the first separation net; The inwall of described cucurbit tube connector is tiltedly being provided with the second spacing glass thorn above bend pipe interconnecting part; The glass thorn bottom of described thorn shape still is provided with the second separation net; Between described the first separation net, the second separation net and the second spacing glass thorn, be filled with inserts.In said structure, in thorn shape fractional still head, increased after filler, when more changing-over liquid bottle restarts fractionation, while making distillate toward upper punch due to the rapid variation of air pressure moment, filler plays certain iris action, make distillate cannot enter condenser pipe, guaranteed to enter the purity of the component fractionating out of condenser pipe, thereby played the effect of real fractionation; The rectifying action that simultaneously filler has increased, the low boiling point component in steam constantly increases, thereby realizes highly purified fractionation.
As preferably, described inserts is spring-type glass body.Adopt this structure, guaranteed the circulation of retort gas and fully contacted in inserts.Use glass material, utilized the corrosion resistance of glass, guarantee the purity of final fractionation product.
As preferably, described the first separation net and the second separation net are stainless steel spring sheet.Guaranteed like this corrosion resistance, cleannes and the intensity of separation net, inserts can not dropped.
According to the technical solution of the utility model, that only need open wireway can open and close valve, just can realize still head air pressure inside and get back to normal pressure, to reach the object that can take receiving vessel away, realize light, quick-replaceable, after changing simultaneously, recover after vacuum, can open and close valve as long as slowly close, just can guarantee the steady decline of still head air pressure, to avoid punching to expect the appearance of phenomenon.In addition, in thorn shape fractional still head, be filled with inserts, while so just making vacuum system open, still head internal pressure changes more steady, even and if can guarantee appearance punching material phenomenon, due to the obstruct of inserts, the liquid in the distillation stoste of upper punch and thorn shape fractional still head can not enter condenser pipe yet, has guaranteed the purity of fractionation; Can utilize the condensation of inserts, further improve purity simultaneously.
Accompanying drawing explanation
Fig. 1 is the structural representation of the utility model embodiment.
The specific embodiment
Below in conjunction with accompanying drawing and the specific embodiment, the utility model is described in further detail:
embodiment:
Essence and flavoring agent preparation connects a thorn shape fractional still head for liquid bottle with fast changeable, comprise cucurbit tube connector 1, oblique bend pipe 2 and thorn shape still 3; Described cucurbit tube connector 1 lower end 11 is cucurbit link, and upper end 12 is ventilation end; The lower end 21 of described oblique bend pipe 2 is communicated with cucurbit tube connector 1 middle part, and upper end 22 is communicated with the lower end 31 of thorn shape still 3; The upper end 32 of described thorn shape still 3 is thermometer insertion end, and lower inner wall is provided with glass thorn 33, and sidepiece is provided with condenser connecting branch 34; The ventilation end 12 of described cucurbit tube connector is provided with breather plug 4, and described breather plug 4 is provided with passage 41, on described passage 41, is inserted with wireway 42, and described wireway 42 is provided with open and close valve 43.
The inwall of described cucurbit tube connector 1 is being provided with the first spacing glass thorn 13 near cucurbit link place, described the first spacing glass thorn top is provided with the first separation net 61; The inwall of described cucurbit tube connector 1 is tiltedly being provided with the second spacing glass thorn 14 above bend pipe 2 interconnecting parts; The glass of described thorn shape still 3 stings 33 bottoms and is provided with the second separation net 62; Between described the first separation net 61, the second separation net 62 and the second spacing glass thorn 14, be filled with inserts 5, described inserts 5 is spring-type glass body, and described the first separation net 61 and the second separation net 62 are stainless steel spring sheet.
In a word, the foregoing is only preferred embodiment of the present utility model, all equalizations of doing according to the utility model claim change and modify, and all should belong to the covering scope of the utility model patent.
Claims (4)
1. essence and flavoring agent preparation connects a thorn shape fractional still head for liquid bottle with fast changeable, it is characterized in that: comprise cucurbit tube connector (1), oblique bend pipe (2) and thorn shape still (3); Described cucurbit tube connector (1) lower end (11) is cucurbit link, and upper end (12) are ventilation end; The lower end (21) of described oblique bend pipe (2) is communicated with cucurbit tube connector (1) middle part, and upper end (22) are communicated with the lower end (31) of thorn shape distillation column (3); The upper end (32) of described thorn shape still (3) is thermometer insertion end, and lower inner wall is provided with glass thorn (33), and sidepiece is provided with condenser connecting branch (34); The ventilation end (12) of described cucurbit tube connector is provided with breather plug (4), and described breather plug (4) is provided with passage (41), is inserted with wireway (42) on described passage (41), and described wireway (42) is provided with open and close valve (43).
2. thorn shape fractional still head according to claim 1, it is characterized in that: the inwall of described cucurbit tube connector (1) is being provided with the first spacing glass thorn (13) near cucurbit link place, described the first spacing glass thorn top is provided with the first separation net (61); The inwall of described cucurbit tube connector (1) is tiltedly being provided with the second spacing glass thorn (14) above bend pipe (2) interconnecting part; Glass thorn (33) bottom of described thorn shape still (3) is provided with the second separation net (62); Between described the first separation net (61), the second separation net (62) and the second spacing glass thorn (14), be filled with inserts (5).
3. thorn shape fractional still head according to claim 2, is characterized in that: described inserts (5) is spring-type glass body.
4. thorn shape fractional still head according to claim 2, is characterized in that: described the first separation net (61) and the second separation net (62) are stainless steel spring sheet.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320610847.2U CN203483902U (en) | 2013-09-30 | 2013-09-30 | Spiniform still head capable of quickly replacing liquid bottle for preparing essences and perfumes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320610847.2U CN203483902U (en) | 2013-09-30 | 2013-09-30 | Spiniform still head capable of quickly replacing liquid bottle for preparing essences and perfumes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203483902U true CN203483902U (en) | 2014-03-19 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320610847.2U Expired - Fee Related CN203483902U (en) | 2013-09-30 | 2013-09-30 | Spiniform still head capable of quickly replacing liquid bottle for preparing essences and perfumes |
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| CN (1) | CN203483902U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105181432A (en) * | 2015-09-08 | 2015-12-23 | 上海应用技术学院 | Concentration method for Jinjunmei black tea aroma component |
| CN105203684A (en) * | 2015-09-16 | 2015-12-30 | 上海应用技术学院 | Maotai liquor aroma component concentrating method |
| CN105259015A (en) * | 2015-09-16 | 2016-01-20 | 上海应用技术学院 | Concentration method for aroma components of oolong tea Tie Guanyin |
| CN105255590A (en) * | 2015-09-16 | 2016-01-20 | 上海应用技术学院 | Concentration method for aroma components of West Lake Longjing Tea |
-
2013
- 2013-09-30 CN CN201320610847.2U patent/CN203483902U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105181432A (en) * | 2015-09-08 | 2015-12-23 | 上海应用技术学院 | Concentration method for Jinjunmei black tea aroma component |
| CN105203684A (en) * | 2015-09-16 | 2015-12-30 | 上海应用技术学院 | Maotai liquor aroma component concentrating method |
| CN105259015A (en) * | 2015-09-16 | 2016-01-20 | 上海应用技术学院 | Concentration method for aroma components of oolong tea Tie Guanyin |
| CN105255590A (en) * | 2015-09-16 | 2016-01-20 | 上海应用技术学院 | Concentration method for aroma components of West Lake Longjing Tea |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee | ||
| CP01 | Change in the name or title of a patent holder |
Address after: Hangzhou City, Zhejiang Province, 311201 blocks south of Xiaoshan Economic Development Zone, Jiang Road No. 18 Patentee after: Zhejiang bio Polytron Technologies Inc Address before: Hangzhou City, Zhejiang Province, 311201 blocks south of Xiaoshan Economic Development Zone, Jiang Road No. 18 Patentee before: ARTSCI BIOLOGY TECHNOLOGIES (ZHEJIANG) CORPORATION |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140319 Termination date: 20170930 |