CN203342438U - Plant extracting chromatographic purification device - Google Patents

Plant extracting chromatographic purification device Download PDF

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Publication number
CN203342438U
CN203342438U CN 201320356420 CN201320356420U CN203342438U CN 203342438 U CN203342438 U CN 203342438U CN 201320356420 CN201320356420 CN 201320356420 CN 201320356420 U CN201320356420 U CN 201320356420U CN 203342438 U CN203342438 U CN 203342438U
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China
Prior art keywords
pipeline
chromatographic column
tank
chromatographic
plant extract
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Expired - Fee Related
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CN 201320356420
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Chinese (zh)
Inventor
刘凤军
周迅雷
孙庆杰
熊柳
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SHANDONG YIMENG MOUNTAIN PEANUT OIL LLC
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SHANDONG YIMENG MOUNTAIN PEANUT OIL LLC
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Priority to CN 201320356420 priority Critical patent/CN203342438U/en
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Abstract

The utility model relates to a plant extracting chromatographic purification device. The plant extracting chromatographic purification device comprises a chromatographic column, wherein the lower end of the chromatographic column is connected with an eluent receiving tank through a pipe; the upper end of the chromatographic column is connected with an analytical solution column applying pump through a pipe; the analytical solution column applying pump is connected with the lower end of an analytical solution storage tank through a pipe; the upper end of the analytical solution storage tank is connected with an analytical solution pump through a pipe; the analytical solution pump is connected with an analytical solution preparing tank through a pipe; the upper end of the chromatographic column is connected with a water washing solution pump through a pipe; the water washing solution pump is connected with a water washing solution storage tank through a pipe. The plant extracting chromatographic purification device has the advantages of simple structure, easy operation, high equipment distinguishment, high selectivity, continuous flow, high efficiency, large production capacity, process stability, reasonable design, and capability of achieving activation and regeneration of the chromatographic column through simple operation, thus ensuring automation and continuousness of the production.

Description

Plant extract chromatographic purifying device
Technical field
The utility model relates to a kind of tomographic system, is specifically related to a kind of plant extract chromatographic purifying device.
Background technology
Chromatography can solve plant carry that the dosage that faces in production is large, the practical problems such as the product moisture absorption and heavy-metal residual.Resulting refining thing after chromatographic technique is processed, can make active ingredient highly enriched, and impurity is few, and extracting yield is only 2~5% of protozoa, and general water-boiling method is 30% left and right, and alcohol deposition method is 15% left and right; Can effectively remove moisture absorption composition, and strengthen the stability of product; Removal heavy metal effectively.
The industry preparation that chromatographic purifying is the largest on extracting technique of Chinese medicine impact, manufacture and design for the separation and purification of bioengineering, pharmaceuticals industry, field of fine chemical, being applicable to the separation and purification of poor complicated polymer substance, is the nucleus equipment of Chinese herbal medicine, chemical synthetic drug and bioactivator active ingredient separating-purifying.
The utility model content
The purpose of this utility model is to provide a kind of plant extract chromatographic purifying device, simple in structure, easy operating.Differentiate high, selectively good, flow continuously, efficiency is high, process that to stablize sample size variable.
Plant extract described in the utility model chromatographic purifying device, comprise chromatographic column, the chromatographic column lower end is connected with the eluent receiving tank by pipeline, upper end is connected with desorbed solution upper prop pump by pipeline, desorbed solution upper prop pump is connected with desorbed solution storage tank lower end by pipeline, desorbed solution storage tank upper end is connected with the parsing liquid pump by pipeline, resolves liquid pump and is connected with the desorbed solution preparing tank by pipeline; The chromatographic column upper end is connected with the washing liquid pump by pipeline, and the washing liquid pump is connected with the water lotion basin by pipeline.
Chromatographic column, specification:
Figure BDA00003378106000011
silica gel 60-100 order in post.
Eluent receiving tank lower end arranges end connection concentrator pipeline and pipeline is set.The waste residue produced by row of conduits to open drain.
Desorbed solution preparing tank upper end arranges solvent depositary management road, recovered alcohol storage-tank pipeline, concentrated alcohol storage-tank pipeline, purified water house steward and a supply mains; Lower end arranges pipeline.The waste residue produced by row of conduits to open drain.
The number of chromatographic column is 6-10, and each chromatographic column lower end is connected with eluent receiving tank top after connecting by pipeline; Each chromatographic column upper end after connecting by pipeline respectively with desorbed solution storage tank and water lotion basin.
Water lotion basin and parsing liquid storage tank lower end all arrange pipeline.The waste residue produced by row of conduits to open drain.
Valve all is set on each pipeline.
Water lotion basin top arranges purified water house steward, a supply mains.
Compared with prior art, the utlity model has following beneficial effect:
The utility model is simple in structure, easy operating.That equipment is differentiated is high, selectively good, flow continuously, efficiency is high, production capacity is large, processing is stable.
This device is reasonable in design, can realize activation and the regeneration of chromatographic column by simple operations, has guaranteed automation and the serialization of producing.
The accompanying drawing explanation
Fig. 1, the structural representation of chromatographic purifying device for plant extract;
In figure, 1, the water lotion basin, 2, purified water house steward, 3, a supply mains, 4, desorbed solution preparing tank, 5, solvent depositary management road, 6, the recovered alcohol storage-tank pipeline, 7, concentrated alcohol storage-tank pipeline, 8, chromatographic column, 9, the eluent receiving tank, 10, connect the pipeline of concentrator, 11-1, pipeline, 11-2, pipeline, 11-3, pipeline, 11-4, pipeline, 12-1, desorbed solution upper prop pump, 12-2, resolve liquid pump, 12-3, washing liquid pump, 13, the desorbed solution storage tank, 14, purified water house steward, 15, supply mains.
The specific embodiment
Below in conjunction with embodiment, the utility model is further described.
Embodiment 1
As Fig. 1, the described a kind of plant extract chromatographic purifying device of the present embodiment, comprise chromatographic column 8, chromatographic column 8 lower ends are connected with eluent receiving tank 9 by pipeline, upper end is connected with desorbed solution upper prop pump 12-1 by pipeline, desorbed solution upper prop pump 12-1 is connected with desorbed solution storage tank 13 lower ends by pipeline, and desorbed solution storage tank 13 upper ends are connected with parsing liquid pump 12-2 by pipeline, resolve liquid pump 12-2 and are connected with desorbed solution preparing tank 4 by pipeline; Chromatographic column 8 upper ends are connected with washing liquid pump 12-3 by pipeline, and washing liquid pump 12-3 is connected with water lotion basin 1 by pipeline.
Chromatographic column, specification:
Figure BDA00003378106000021
silica gel 60-100 order in post.
Eluent receiving tank 9 lower ends arrange end connection concentrator pipeline 10 and pipeline 11-1 are set.
Desorbed solution preparing tank 4 upper ends arrange solvent depositary management road 5, recovered alcohol storage-tank pipeline 6, concentrated alcohol storage-tank pipeline 7, purified water house steward 14 and a supply mains 15; Lower end arranges pipeline 11-3.
The number of chromatographic column 8 is 6-10, and each chromatographic column 8 lower end is connected with eluent receiving tank 9 tops after connecting by pipeline; After each chromatographic column 8 upper end connects by pipeline respectively with desorbed solution storage tank 13 and water lotion basin 1.
Water lotion basin 1 and parsing liquid storage tank 13 lower ends all arrange pipeline 11.
Valve all is set on each pipeline.
Water lotion basin 1 top arranges purified water house steward 2, a supply mains 3.
Embodiment 2
The present embodiment structure is identical with embodiment 1, and difference is, the number of chromatographic column 8 is 8.
Embodiment 3
The present embodiment structure is identical with embodiment 1, and difference is, the number of chromatographic column 8 is 10.

Claims (8)

1. a plant extract chromatographic purifying device, comprise chromatographic column (8), it is characterized in that, chromatographic column (8) lower end is connected with eluent receiving tank (9) by pipeline, upper end is connected with desorbed solution upper prop pump (12-1) by pipeline, desorbed solution upper prop pump (12-1) is connected with desorbed solution storage tank (13) lower end by pipeline, and desorbed solution storage tank (13) upper end is connected with parsing liquid pump (12-2) by pipeline, resolves liquid pump (12-2) and is connected with desorbed solution preparing tank (4) by pipeline; Chromatographic column (8) upper end is connected with washing liquid pump (12-3) by pipeline, and washing liquid pump (12-3) is connected with water lotion basin (1) by pipeline.
2. plant extract according to claim 1 chromatographic purifying device, is characterized in that, chromatographic column, and specification:
Figure FDA00003378105900011
, silica gel 60-100 order in post.
3. plant extract according to claim 1 chromatographic purifying device, is characterized in that, eluent receiving tank (9) lower end arranges end connection concentrator pipeline (10) and pipeline (11-1) are set.
4. plant extract according to claim 1 chromatographic purifying device, it is characterized in that, desorbed solution preparing tank (4) upper end arranges solvent depositary management road (5), recovered alcohol storage-tank pipeline (6), concentrated alcohol storage-tank pipeline (7), purified water house steward (14) and a supply mains (15); Lower end arranges pipeline (11-3).
5. plant extract according to claim 1 chromatographic purifying device, is characterized in that, the number of chromatographic column (8) is 6-10, and each chromatographic column (8) lower end is connected with eluent receiving tank (9) top after connecting by pipeline; After each chromatographic column (8) upper end connects by pipeline respectively with desorbed solution storage tank (13) and water lotion basin (1).
6. plant extract chromatographic purifying device according to claim 1 or 5, is characterized in that, water lotion basin (1) and resolve liquid storage tank (13) lower end pipeline (11) all is set.
7. plant extract according to claim 1 chromatographic purifying device, is characterized in that, valve all is set on each pipeline.
8. plant extract according to claim 1 chromatographic purifying device, is characterized in that, water lotion basin (1) top arranges purified water house steward (2), a supply mains (3).
CN 201320356420 2013-06-20 2013-06-20 Plant extracting chromatographic purification device Expired - Fee Related CN203342438U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201320356420 CN203342438U (en) 2013-06-20 2013-06-20 Plant extracting chromatographic purification device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201320356420 CN203342438U (en) 2013-06-20 2013-06-20 Plant extracting chromatographic purification device

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CN203342438U true CN203342438U (en) 2013-12-18

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105597369A (en) * 2016-03-01 2016-05-25 永州星辰生物科技有限公司 Chromatography tank for artemisinin extraction and efficient pressurized chromatography method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105597369A (en) * 2016-03-01 2016-05-25 永州星辰生物科技有限公司 Chromatography tank for artemisinin extraction and efficient pressurized chromatography method thereof

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20131218

Termination date: 20180620