CN203191348U - Fuel oil hydrocarbon tester - Google Patents

Fuel oil hydrocarbon tester Download PDF

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Publication number
CN203191348U
CN203191348U CN 201320143487 CN201320143487U CN203191348U CN 203191348 U CN203191348 U CN 203191348U CN 201320143487 CN201320143487 CN 201320143487 CN 201320143487 U CN201320143487 U CN 201320143487U CN 203191348 U CN203191348 U CN 203191348U
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CN
China
Prior art keywords
temperature
carbon
fuel oil
determination
furnace
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Expired - Fee Related
Application number
CN 201320143487
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Chinese (zh)
Inventor
李新林
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TAIZHOU WANSHENG ANALYTICAL INSTRUMENT Co Ltd
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TAIZHOU WANSHENG ANALYTICAL INSTRUMENT Co Ltd
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Priority to CN 201320143487 priority Critical patent/CN203191348U/en
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Publication of CN203191348U publication Critical patent/CN203191348U/en
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Abstract

The utility model discloses a fuel oil hydrocarbon tester consisting of a sample gasification pyrolysis system, a gas purifier, a carbon dioxide conversion device, a detection device, a data acquiring and processing system and a control system, wherein the sample gasification pyrolysis system comprises an oxygen feeding device, a temperature-controllable sample gasification furnace, a high-temperature cracking furnace, a special cracking pipe and a sample charging device; the gas purifier comprises an oxysulfide removing device and an oxynitride removing device; and the carbon dioxide conversion device comprises a temperature-controllable high-temperature furnace and a conversion pipe in which lithium hydroxide is filled. The fuel oil hydrocarbon tester disclosed by the utility model has the advantages that hydrogen and carbon determination on liquid or solid fuel oil samples, such as gasoline, diesel oil, heavy oil and residual oil can be simultaneously carried out by one tester under the changeless working conditions, so that the purposes of reducing the energy consumption and improving the working efficiency are realized.

Description

The fuel oil apparatus for determination of carbon and hydrogen
Technical field
The present invention relates to a kind of chemical analysis instrument, be specifically related to a kind of fuel oil apparatus for determination of carbon and hydrogen.
Background technology
Carbon in the material and protium can utilize coulometry to detect with behind the combustion oxidation, by the content of carbon and hydrogen in the analyzer substance for calculation.Existingly have the following disadvantages for detection of instrument hydrocarbon in the fuel oil: can only detect the not high fuel oil material of volatility, for high-volatile materials such as gasoline or diesel oil, then be difficult to maybe can't detect, and instrument cost height, inefficiency, complicated operation does not meet low-carbon (LC), energy-conservation, social demand efficiently.
Summary of the invention
The present invention is in order to overcome above-mentioned deficiency, to provide a kind of working stability reliable, degree of accuracy, the high fuel oil apparatus for determination of carbon and hydrogen of accuracy, it utilizes same high-temperature cracking furnace, a special-purpose cracking tube, and detecting device, can realize carbon and hydrogen simple, measure fast.
The present invention is achieved through the following technical solutions goal of the invention: a kind of fuel oil apparatus for determination of carbon and hydrogen, formed by sample gasification cracking system, gas cleaning unit, carbon dioxide reforming unit, detection system, data Collection ﹠ Processing System and control system.Described sample gasification cracking system contains sample gasification furnace and high-temperature cracking furnace, special-purpose cracking tube and the sampling device of oxygen feedway, controllable temperature, and sampling device can be artificial sampling device, but also automatic sampling apparatus; Described gas cleaning unit contains the sulphur removal oxide device and denitrogenates oxide device; Described carbon dioxide reforming unit refers to that carbon dioxide changes into the device of water, and it comprises in the high temperature furnace, of a controllable temperature is equipped with conversion tube of lithium hydroxide etc.; Described detection system contains two electrolytic cells: first electrolytic cell be used for to be surveyed hydrogen, second electrolytic cell and is used for carbon determination (be used for surveying the hydrogen number of the water that carbon dioxide changes into, this measured value can convert the measured value of carbon by calculating to); Described data Collection ﹠ Processing System contains to be handled the acquisition process of the electric signal of two electrolytic cells, temperature signal collection.Described control system contains the control of electrolytic process control, data acquisition and the processing of sample auto injection, Control for Kiln Temperature, two electrolytic cells, and as calculated machine or single-chip microcomputer handle, the output measurement result.
In the said structure, the sample feeding device is sent into gasification furnace, the high-temperature cracking furnace of Pintsch process system, and pyrolysis furnace is laid cracking tube, and furnace temperature can reach 1000 ℃ under the excess oxygen, sample perfect combustion.Input was at first electrolytic cell that is connected with the cracking tube endpiece after products of combustion was removed sulfur oxide, and first electrolytic cell is connected with nitrogen removing device, is connected with the carbon dioxide reforming unit then, is connected with second electrolytic cell again.
The present invention compared with prior art has following good effect:
1, can detect volatile substances such as gasoline, diesel oil;
2, simple to operate, the data validity that detects gained is strong, and testing result is accurate;
3, the measuring process controllability is strong, detects easy, quick;
5, by computing machine or the whole testing process of Single-chip Controlling, handle and detect data, simple and convenient.
Description of drawings
Fig. 1 is functional-block diagram of the present invention.
Embodiment
Below with reference to the accompanying drawings shown in, in conjunction with example, the present invention is described further.
As shown in Figure 1, a kind of fuel oil apparatus for determination of carbon and hydrogen is made up of sample gasification cracking system, gas cleaning unit, carbon dioxide reforming unit, detection system, data Collection ﹠ Processing System and computer control system.Described gasification cracking system is furnished with automatic sample handling system 1 and oxygenato 6 based on gasification cracking system 2.Described detection system contains surveys hydrogen electrolytic cell 3 and carbon determination electrolytic cell 7.Described gas cleaning unit contains desulfurizing device 3 and nitrogen removing device 9.Described data Collection ﹠ Processing System contains data Collection ﹠ Processing System 11 and data conveyer line 5,15.Data conveyer line 5 with survey hydrogen electrolytic cell 4 and link to each other, 15 of conveyer lines link to each other the collection electric signal with the carbon determination electrolytic cell.Conveyer line 14 is used for transmitting data to computer control system.Described computer control system contains computer control system 10 data conveyer lines 12,13, and data conveyer line 12 and 1 two-way connection of automatic sample handling system are used for control and Information Monitoring; Data conveyer line 13 and gasification cracking system 2,8 two-way connections of carbon dioxide reforming unit are used for control and Information Monitoring; Automatic sample handling system 1, temperature gasification and high cracking system 2, data Collection ﹠ Processing System 11 carry data to handle the output measurement result to computer control system by data conveyer line 12,13,14.
When the present invention moves, sent by computing machine or single-chip microcomputer and to measure instruction, load weighted sample is sent into the high-temperature region of gasification cracking system 2 gradually, sample burns in furnace temperature reaches 1000 ℃ pyrolysis furnace under excess oxygen.Sample dissociation product water and carbon dioxide are respectively by surveying hydrogen electrolytic cell 4 and 7 detections of carbon determination electrolytic cell in the present embodiment.Determination data sends computing machine or single-chip computer control system 10 to after gathering by data Collection ﹠ Processing System 11, calculates and print measurement result by computing machine or single-chip microcomputer.
The present invention is primarily aimed at intelligent radio and launches the improvement of carrying out with receiving equipment, the above only is preferred embodiment of the present invention, non-so namely limit to claim of the present invention, so simple and easy variation and the equivalent transformation of doing with instructions of the present invention and graphic content all should be contained in the claim of the present invention such as.

Claims (4)

1. fuel oil apparatus for determination of carbon and hydrogen, be made up of sample gasification cracking system, gas cleaning unit, carbon dioxide reforming unit, detection system, data Collection ﹠ Processing System and control system, it is characterized in that: described sample gasification cracking system comprises sample gasification furnace and high-temperature cracking furnace, special-purpose cracking tube and the sampling device of oxygen feedway, controllable temperature; Described gas cleaning unit comprises the sulphur removal oxide device and denitrogenates oxide device; Described carbon dioxide reforming unit comprises the conversion tube that lithium hydroxide is housed in the high temperature furnace, of a controllable temperature.
2. fuel oil apparatus for determination of carbon and hydrogen according to claim 1, it is characterized in that: described detection system comprises two electrolytic cells, wherein first electrolytic cell is used for surveying hydrogen, second electrolytic cell is used for carbon determination.
3. fuel oil apparatus for determination of carbon and hydrogen according to claim 1, it is characterized in that: described data Collection ﹠ Processing System links to each other with detection system, is used for acquisition process, the temperature signal collection of the electric signal of two electrolytic cells of detection system are handled.
4. fuel oil apparatus for determination of carbon and hydrogen according to claim 1, it is characterized in that: described control system comprises the control of electrolytic process control, data acquisition and the processing of sample auto injection, Control for Kiln Temperature, two electrolytic cells, and measurement result is handled, exported to machine or single-chip microcomputer as calculated.
CN 201320143487 2013-03-27 2013-03-27 Fuel oil hydrocarbon tester Expired - Fee Related CN203191348U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201320143487 CN203191348U (en) 2013-03-27 2013-03-27 Fuel oil hydrocarbon tester

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201320143487 CN203191348U (en) 2013-03-27 2013-03-27 Fuel oil hydrocarbon tester

Publications (1)

Publication Number Publication Date
CN203191348U true CN203191348U (en) 2013-09-11

Family

ID=49108201

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201320143487 Expired - Fee Related CN203191348U (en) 2013-03-27 2013-03-27 Fuel oil hydrocarbon tester

Country Status (1)

Country Link
CN (1) CN203191348U (en)

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130911

Termination date: 20150327

EXPY Termination of patent right or utility model