CN203083902U - Magnetic force suspension density tester - Google Patents

Magnetic force suspension density tester Download PDF

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Publication number
CN203083902U
CN203083902U CN 201320019229 CN201320019229U CN203083902U CN 203083902 U CN203083902 U CN 203083902U CN 201320019229 CN201320019229 CN 201320019229 CN 201320019229 U CN201320019229 U CN 201320019229U CN 203083902 U CN203083902 U CN 203083902U
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permanent magnets
glass column
density
sample
dasymeter
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王军
林雄
李乐
宁爱凤
李发根
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Ningbo University
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Ningbo University
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Abstract

The utility model discloses a magnetic force suspension density tester which is characterized by comprising two vertical polar permanent magnets of which the polarities are opposite to each other, wherein a hollow glass column is arranged between the two permanent magnets; and a transparent magnetic liquid for measuring the density of a sample is filled into the glass column. As the density is measured according to the height that the sample is suspended in the magnetic liquid, the magnetic force suspension density tester has the characteristics of simplicity in structure and convenience in operation, the density of the sample can be conveniently and rapidly tested or the content of one component in the sample is estimated and tested, an extreme small amount of the sample is needed, the range of substances which can be analyzed is wide, the tester is applicable to solid, liquids, adhesives, gels, paste and the like, and samples of irregular shapes can also be tested. The magnetic force suspension density tester solves the problems that the conventional density testing is large in expense, the operation is complex or the precision is not high and the like, is high in measurement precision, convenient and rapid to measure, low in expense and worthy of wide popularization.

Description

磁力悬浮密度测量器Magnetic Levitation Density Meter

技术领域technical field

本实用新型涉及密度测量器技术领域,具体是一种磁力悬浮密度测量器,是通过样品在磁力悬浮装置中悬浮的位置或高度来检测物质的密度。The utility model relates to the technical field of density measuring devices, in particular to a magnetic suspension density measurement device, which detects the density of a substance through the position or height of a sample suspended in a magnetic suspension device.

背景技术Background technique

当前,虽然有很多种测量固体、液体密度和测量溶液浓度的仪器,如:密度梯度柱,浮球湿度计,震荡管密度计,悬浮微谐振器等,但是这些检测技术都有各自的缺点和不足,如花费较高、操作复杂、精度不高、只能对特定的样品进行测量等等。密度梯度柱有高精密度(10-4g/cm3),但此方法花费高,操作复杂,需要受过专业训练的测试员操作,才能在实验室测出精确的数据;以震荡管技术为基础的现代设备精度高,方便快捷,但是花费很高,一般都要几千元的测试费,而且只能检测确定粘度范围内的液体;悬浮微谐振器是迄今为止测量密度精度最高的仪器,但是该技术只限于分析小于3~15微米的物质,而且需要国家最先进的设备和精心的光学检测;所以迫切需要一种能够快捷、准确而且花费低的检测设备或仪器用于检测固体液体的密度。At present, although there are many kinds of instruments for measuring the density of solids and liquids and measuring the concentration of solutions, such as: density gradient column, float hygrometer, oscillating tube density meter, suspended microresonator, etc., these detection technologies have their own shortcomings and limitations. Disadvantages, such as high cost, complicated operation, low precision, only specific samples can be measured, etc. Density gradient columns have high precision (10 -4 g/cm 3 ), but this method is expensive and complicated to operate, and requires professionally trained testers to measure accurate data in the laboratory; The basic modern equipment has high precision, convenient and quick, but the cost is very high. Generally, it costs several thousand yuan for testing, and it can only detect liquids within a certain viscosity range; the suspended microresonator is the instrument with the highest density measurement accuracy so far. However, this technology is limited to the analysis of substances smaller than 3-15 microns, and requires state-of-the-art equipment and careful optical detection; so there is an urgent need for a fast, accurate and low-cost detection equipment or instrument for detecting solid liquids density.

发明内容Contents of the invention

本实用新型所要解决的技术问题是针对上述的技术现状而提供一种结构简单、操作方便的磁力悬浮密度测量器,能够方便快捷的检测出物质的密度或估测物质中某种成分的含量,而且成本低,测量精度高,所需样品量极少。The technical problem to be solved by this utility model is to provide a magnetic levitation density measuring device with simple structure and convenient operation in view of the above-mentioned technical status, which can detect the density of a substance or estimate the content of a certain component in a substance conveniently and quickly. Moreover, the cost is low, the measurement accuracy is high, and the amount of sample required is extremely small.

本实用新型解决上述技术问题所采用的技术方案为:一种磁力悬浮密度测量器,其特征在于包括上下二块极性相对设置的永磁体,二块永磁体之间设有一中空的玻璃柱,玻璃柱内填装满用于测量样品密度的透明的磁性液体。The technical scheme adopted by the utility model to solve the above-mentioned technical problems is: a magnetic levitation density measuring device, which is characterized in that it includes two permanent magnets with opposite polarities on the upper and lower sides, and a hollow glass column is arranged between the two permanent magnets. The glass column is filled with a transparent magnetic liquid used to measure the density of the sample.

作为改进,所述玻璃柱的下端封口,上端开口,玻璃柱的下端固定于下方的永磁体的上端中间位置,上方的永磁体套置在玻璃柱的上端,所述玻璃柱的上下两端与二块永磁体的连接处分别设有橡皮圈进行密封。As an improvement, the lower end of the glass column is sealed and the upper end is open. The lower end of the glass column is fixed at the middle position of the upper end of the permanent magnet below, and the upper permanent magnet is sleeved on the upper end of the glass column. The joints of the two permanent magnets are respectively provided with rubber rings for sealing.

作为改进,所述永磁体呈立方体,长为2.5~3.5cm,宽为2.5~3.5cm,高为0.8~1.2cm,二块永磁体的间距为4.5~5.5cm,所述玻璃柱的长度为与二块永磁体的间距相对应的4.5~5.5cm。As an improvement, the permanent magnet is a cube with a length of 2.5 to 3.5 cm, a width of 2.5 to 3.5 cm, and a height of 0.8 to 1.2 cm. The distance between the two permanent magnets is 4.5 to 5.5 cm. The length of the glass column is 4.5-5.5 cm corresponding to the distance between two permanent magnets.

再改进,所述永磁体长为3cm,宽为3cm,高为1cm,二块永磁体的间距为5cm,所述玻璃柱的长度为与二块永磁体的间距相对应的5cm。Further improvement, the length of the permanent magnet is 3cm, the width is 3cm, the height is 1cm, the distance between the two permanent magnets is 5cm, and the length of the glass column is 5cm corresponding to the distance between the two permanent magnets.

进一步改进,所述二块永磁体的外侧套设有一用于支撑固定的外壳,在外壳内二块永磁体的前后设有支撑板进行固定,所述支撑板的中间对应与玻璃柱的位置镂空,镂空处分别安装有用于保护玻璃柱的透明玻璃。As a further improvement, the outer sides of the two permanent magnets are provided with a housing for supporting and fixing, and support plates are provided before and after the two permanent magnets in the housing for fixing, and the middle of the support plates is hollowed out corresponding to the position of the glass column , and the transparent glass used to protect the glass column is respectively installed in the hollow.

最后,所述透明玻璃上标有便于读数的刻度。Finally, the clear glass is marked with graduations for easy reading.

与现有技术相比,本实用新型的优点在于:本实用新型通过样品悬浮在磁性液体的高度来测出密度,具有结构简单、操作方便的特点,能够方便快捷的检测出物质的密度或估测物质中某种成分的含量,所需样品量极少,可以分析的物质范围广,可适用于固体,液体,胶体,凝胶剂,浆糊等等,还可以测量形状不规则的样品。本实用新型测量精度高(根据不同的实验条件可以精确到±0.02~±0.0002g/cm3),测量方便快捷且费用低廉,值得大量推广。Compared with the prior art, the utility model has the advantages that: the utility model measures the density by suspending the sample in the height of the magnetic liquid, has the characteristics of simple structure and convenient operation, and can detect the density or estimate the density of the substance conveniently and quickly To measure the content of a certain component in a substance, the amount of sample required is very small, and a wide range of substances can be analyzed. It is applicable to solids, liquids, colloids, gels, pastes, etc., and can also measure samples with irregular shapes. The utility model has high measurement precision (accurate to ±0.02-±0.0002g/cm3 according to different experimental conditions), convenient and quick measurement and low cost, and is worthy of mass promotion.

附图说明Description of drawings

图1为本实用新型的结构示意图;Fig. 1 is the structural representation of the utility model;

图2为本实用新型的外观结构示意图。Fig. 2 is a schematic diagram of the appearance structure of the utility model.

具体实施方式Detailed ways

以下结合附图实施例对本实用新型作进一步详细描述。The utility model is described in further detail below in conjunction with the accompanying drawings.

如图所示,一种磁力悬浮密度测量器,包括上下二块永磁体1和7、设置在二块永磁体1和7之间的一根中空的玻璃柱2,二块永磁体1和7呈N极、N极相对,或者S极、S极相对的极性相对设置,永磁体1和7呈立方体,长为3cm,宽为3cm,高为1cm,二块永磁体1和7的间距为5cm,玻璃柱2的长度为5cm,玻璃柱2的下端封口,上端开口,玻璃柱2内填装满用于测量样品密度的透明的磁性液体4,玻璃柱2的下端固定于下方的永磁体7的上端中间位置,上方的永磁体1套置在玻璃柱2的上端,在玻璃柱的上下两端与二块永磁体1和7的连接处分别设有橡皮圈进行密封;二块永磁体1和7的外侧套设有一用于支撑固定的外壳3,外壳3采用塑料制成,在外壳3内二块永磁体1和7的前后设有支撑板5进行固定,支撑板5的中间对应与玻璃柱2的位置镂空,镂空处分别安装有用于保护玻璃柱2的透明玻璃6,在透明玻璃6上标有便于读数的刻度。As shown in the figure, a magnetic levitation density measuring instrument includes two permanent magnets 1 and 7, a hollow glass column 2 arranged between the two permanent magnets 1 and 7, and two permanent magnets 1 and 7 The N poles and N poles are opposite, or the S poles and S poles are opposite to each other. The permanent magnets 1 and 7 are cubes, with a length of 3cm, a width of 3cm, and a height of 1cm. The distance between the two permanent magnets 1 and 7 The length of the glass column 2 is 5cm, the lower end of the glass column 2 is sealed, and the upper end is open. The transparent magnetic liquid 4 used to measure the density of the sample is filled in the glass column 2, and the lower end of the glass column 2 is fixed on the permanent below. At the middle position of the upper end of the magnet 7, the permanent magnet 1 above is sleeved on the upper end of the glass column 2, and rubber rings are respectively provided at the joints between the upper and lower ends of the glass column and the two permanent magnets 1 and 7 for sealing; The outer cover of magnet 1 and 7 is provided with a shell 3 for supporting and fixing, and shell 3 adopts plastics to make, is provided with support plate 5 before and after two permanent magnets 1 and 7 in shell 3 and fixes, and the middle of support plate 5 The position corresponding to the glass column 2 is hollowed out, and transparent glass 6 for protecting the glass column 2 is respectively installed in the hollowed out place, and a scale for easy reading is marked on the transparent glass 6 .

使用时,从上部打开玻璃柱2,将样品放入磁性液体4中,由于磁力作用,样品会悬浮在磁性液体4中,观察它离玻璃柱2底部的高h,然后根据公式:When in use, open the glass column 2 from the top, put the sample into the magnetic liquid 4, due to the magnetic force, the sample will be suspended in the magnetic liquid 4, observe its height h from the bottom of the glass column 2, and then according to the formula:

hh == (( ρρ sthe s -- ρρ mm )) gg μμ 00 dd 22 (( χχ sthe s -- χχ mm )) 44 BB 00 22 ++ dd 22 -- -- -- (( 11 ))

计算出ρs(即样品的密度):Calculate ρs (i.e. the density of the sample):

ρρ sthe s == 44 BB 00 22 (( hh -- dd 22 )) (( χχ sthe s -- χχ mm )) gg μμ 00 dd 22 ++ ρρ mm -- -- -- (( 22 ))

其中h是样品在磁性液体中的高度,ρm是磁性液体的密度,g是重力加速度,μ0是真空磁导率,d是两磁体间的距离,B0是磁体表面的磁感应强度,χs是样品的磁化率,χm是磁性液体的磁化率。Wherein h is the height of the sample in the magnetic liquid, ρ m is the density of the magnetic liquid, g is the acceleration of gravity, μ 0 is the vacuum permeability, d is the distance between the two magnets, B 0 is the magnetic induction intensity on the surface of the magnet, χ s is the magnetic susceptibility of the sample and χ m is the magnetic susceptibility of the magnetic liquid.

公式的具体推导过程是:The specific derivation process of the formula is:

对公式(1)可进行推导,样品在磁性液体中受到的磁力可表示为:Formula (1) can be deduced, and the magnetic force on the sample in the magnetic liquid can be expressed as:

Ff →&Right Arrow; magmag == (( χχ sthe s -- χχ mm )) μμ 00 VV (( BB →&Right Arrow; ·· ▿▿ →&Right Arrow; )) BB →&Right Arrow; -- -- -- (( 33 ))

地球对样品的作用力为:The force exerted by the earth on the sample is:

Ff →&Right Arrow; gg == (( ρρ sthe s -- ρρ mm )) VV gg →&Right Arrow; -- -- -- (( 44 ))

当样品受力平衡时:When the sample is balanced by force:

Ff →&Right Arrow; magmag ++ Ff →&Right Arrow; gg == (( ρρ sthe s -- ρρ mm )) VV gg →&Right Arrow; ++ (( χχ sthe s -- χχ mm )) μμ 00 VV (( BB →&Right Arrow; ·&Center Dot; ▿▿ →&Right Arrow; )) BB →&Right Arrow; == 00 -- -- -- (( 55 ))

-- (( ρρ sthe s -- ρρ mm )) gg ++ (( χχ sthe s -- χχ mm )) μμ 00 (( BB xx ∂∂ BB zz ∂∂ xx ++ BB ythe y ∂∂ BB zz ∂∂ ythe y ++ BB zz ∂∂ BB zz ∂∂ zz )) == 00 -- -- -- (( 66 ))

BB →&Right Arrow; ≡≡ BB xx BB ythe y BB zz == 00 00 -- 22 BB 00 dd zz ++ BB 00 -- -- -- (( 77 ))

由公式(6)和公式(7)推导得出:It is derived from formula (6) and formula (7):

hh == (( ρρ sthe s -- ρρ mm )) gg μμ 00 dd 22 (( χχ sthe s -- χχ mm )) 44 BB 00 22 ++ dd 22 -- -- -- (( 88 ))

Claims (6)

1. magnetic levitation dasymeter is characterized in that comprising two permanent magnets that polarity is oppositely arranged up and down, is provided with the glass column of a hollow between two permanent magnets, and filling completely is used for the transparent magnetic liquid of measuring samples density in the glass column.
2. magnetic levitation dasymeter according to claim 1, the following end closure that it is characterized in that described glass column, upper end open, the centre position, upper end of the permanent magnet of below is fixed in the lower end of glass column, the permanent magnet of top is nested with the upper end at glass column, and the two ends up and down of described glass column and the junction of two permanent magnets are respectively equipped with rubber band and seal.
3. magnetic levitation dasymeter according to claim 1, it is characterized in that described permanent magnet is cube, length is 2.5~3.5cm, wide is 2.5~3.5cm, height is 0.8~1.2cm, the spacing of two permanent magnets is 4.5~5.5cm, and the length of described glass column is and the corresponding 4.5~5.5cm of the spacing of two permanent magnets.
4. magnetic levitation dasymeter according to claim 3 is characterized in that the long 3cm of being of described permanent magnet, and wide is 3cm, and height is 1cm, and the spacing of two permanent magnets is 5cm, and the length of described glass column is and the corresponding 5cm of the spacing of two permanent magnets.
5. according to the described magnetic levitation dasymeter of the arbitrary claim of claim 1 to 3; the outside that it is characterized in that described two permanent magnets is arranged with a shell that is used for support fixation; the front and back of two permanent magnets are provided with back up pad and fix in the enclosure; the position hollow out of correspondence and glass column in the middle of the described back up pad, the hollow out place is equipped with the clear glass that is used for the cover glass post respectively.
6. according to the described magnetic levitation dasymeter of the arbitrary claim of claim 1 to 3, it is characterized in that described clear glass is marked with easy-to-read scale.
CN 201320019229 2013-01-14 2013-01-14 Magnetic force suspension density tester Expired - Fee Related CN203083902U (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103743651A (en) * 2013-12-27 2014-04-23 广西科技大学 Device for measuring average density of micro objects
CN106563565A (en) * 2016-09-11 2017-04-19 浙江大学 High polymer material separation method based on magnetic-Archimedes principle
CN106568681A (en) * 2016-06-14 2017-04-19 浙江大学 Precise measurement method for density of antimagnetic material
CN106568680A (en) * 2016-06-14 2017-04-19 浙江大学 Magnetic suspension detection method for density detection
CN108120660A (en) * 2017-12-04 2018-06-05 浙江大学 A kind of magnetic method of operating based on magnetic Archimedes
CN111412831A (en) * 2020-03-27 2020-07-14 北京交通大学 Impact-resistant magnetic liquid touch sensor

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103743651A (en) * 2013-12-27 2014-04-23 广西科技大学 Device for measuring average density of micro objects
CN103743651B (en) * 2013-12-27 2016-04-13 广西科技大学 A kind of minim block average density measurement mechanism
CN106568681A (en) * 2016-06-14 2017-04-19 浙江大学 Precise measurement method for density of antimagnetic material
CN106568680A (en) * 2016-06-14 2017-04-19 浙江大学 Magnetic suspension detection method for density detection
CN106568681B (en) * 2016-06-14 2019-06-11 浙江大学 A Precise Measurement Method of Density of Diamagnetic Substances
CN106563565A (en) * 2016-09-11 2017-04-19 浙江大学 High polymer material separation method based on magnetic-Archimedes principle
CN106563565B (en) * 2016-09-11 2018-05-29 浙江大学 A kind of high molecular material separation method based on magnetic-Archimedes principle
CN108120660A (en) * 2017-12-04 2018-06-05 浙江大学 A kind of magnetic method of operating based on magnetic Archimedes
CN108120660B (en) * 2017-12-04 2019-09-24 浙江大学 A kind of magnetic method of operating based on magnetic Archimedes
CN111412831A (en) * 2020-03-27 2020-07-14 北京交通大学 Impact-resistant magnetic liquid touch sensor

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