CN203061073U - High-pressure static mixer for chromatographic instrument - Google Patents

High-pressure static mixer for chromatographic instrument Download PDF

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Publication number
CN203061073U
CN203061073U CN2012207052111U CN201220705211U CN203061073U CN 203061073 U CN203061073 U CN 203061073U CN 2012207052111 U CN2012207052111 U CN 2012207052111U CN 201220705211 U CN201220705211 U CN 201220705211U CN 203061073 U CN203061073 U CN 203061073U
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CN
China
Prior art keywords
loam cake
static mixer
lower cover
pipeline
pressure static
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2012207052111U
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Chinese (zh)
Inventor
董智勇
王风云
李乃杰
雷武
张万程
唐涛
李彤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
YILITE ANALYSIS INSTRUMENT CO Ltd DALIAN
Nanjing University of Science and Technology
Original Assignee
YILITE ANALYSIS INSTRUMENT CO Ltd DALIAN
Nanjing University of Science and Technology
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Filing date
Publication date
Application filed by YILITE ANALYSIS INSTRUMENT CO Ltd DALIAN, Nanjing University of Science and Technology filed Critical YILITE ANALYSIS INSTRUMENT CO Ltd DALIAN
Priority to CN2012207052111U priority Critical patent/CN203061073U/en
Application granted granted Critical
Publication of CN203061073U publication Critical patent/CN203061073U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model discloses a high-pressure static mixer for a chromatographic instrument. The high-pressure static mixer is characterized by comprising a mixer joint, wherein an upper cover and a lower cover which are connected with each other through sealing bolts to form a whole body are arranged on one side of the mixer joint; a sealing pad is arranged between the upper cover and the lower cover; a mixing cavity unit is arranged between the upper cover and the lower cover and consists of a columnar mixing cavity, upper connection bolts and upper pipelines which are matched with each other, and lower connection bolts and lower pipelines which are matched with each other; the columnar mixing cavity is arranged between the upper cover and the lower cover; the hollow upper connection bolts are arranged in the upper cover; the upper pipelines are inserted into the upper connection bolts; the upper pipelines are communicated with the upper end of the columnar mixing cavity; the lower end of the columnar mixing cavity is communicated with the lower pipelines which are connected to the lower cover through the lower connection bolts; and the tail ends of the lower pipelines are connected with the mixer joint. The high-pressure static mixer for the chromatographic instrument is simple in structure, ingenious in design, low in cost, high in pressure resistance, small in size and high in generality.

Description

Chromatograph high pressure static mixer
Technical field
The utility model relates to a kind of blender, particularly a kind of chromatograph high pressure static mixer.
Background technology
The chromatograph static mixer is a kind of device that two or more different solvents that high pressure constant flow pump is transported mixes.For guaranteeing the constant pressure in a whole set of chromatograph system, static mixer must tolerate certain high pressure (being generally 40MPa).In the application of reality, except requiring that the multiple solvent of input is had mixed effect preferably; Also having the internal mixer volume can not be excessive; The dead angle that not remaining solvent can't be discharged in the cavity; Requirements such as the organic solvent that is introduced into discharge as far as possible earlier.
At present, chromatograph mainly contains following three kinds with static mixer structure commonly used, all exists the not problem of degree.
One, coiled static mixer: the different organic solvent of two-way is pooled to the thinner stainless steel tube porch of internal diameter by threeway, and liquid produces diffusion in the process of pipeline of flowing through, thereby reaches the effect of mixing.Because what adopt is the nature diffusion principle, this kind static mixer can't obtain mixed effect preferably.
Two, ball-type static mixer: the ball that particle diameter is identical is filled in the tubular housing inside of sealing.In liquid is flowed through the process of tubular housing, owing to be subjected to the obstruction of ball, can only between peripheral slit, disperse, finally merge in the exit.The problem of this kind static mixer maximum is long in the holdup time of liquid in cavity, thereby can't realize " first in first out " of different solvents.
Three, multistage diaphragm type static mixer: the static mixer of this kind structure is that the stainless steel diaphragm of many identical appearance sizes is placed in the middle of the stream according to certain Cahn-Ingold-Prelog sequence rule.Liquid flow direction when impacting steel disc changes, thereby forms local little eddy current, finally reaches the effect of mixing.Because the difficulty of machining, welding, assembling is bigger, finished product is on the high side and yield rate is lower.Be subjected to structural limitations, can't adjust the internal mixer volume.
In sum, need a kind of novel static mixer that can address the above problem now.
Summary of the invention
The utility model is in order to solve the above-mentioned deficiency of existing in prior technology, proposes a kind of simple in structurely, designs ingenious, low-cost, high withstand voltage, small size, chromatograph high pressure static mixer that versatility is good.
Technical solution of the present utility model is: a kind of chromatograph high pressure static mixer, it is characterized in that: described blender comprises blender joint 1, side at blender joint 1 is provided with loam cake 3 and the lower cover 4 that connects as one structure by sealing bolt 2, between loam cake 3 and lower cover 4, be folded with sealing gasket 5, between loam cake 3 and lower cover 4, be provided with the hybrid chamber unit, described hybrid chamber unit is by column mixing chamber 6, the last connecting bolt 7 that matches, upper pipeline 8, the following connecting bolt 9 that matches, lower pipeline 10 is formed, column mixing chamber 6 is arranged between loam cake 3 and the lower cover 4, be provided with hollow last connecting bolt 7 in the loam cake 3, cross-under has upper pipeline 8 in the last connecting bolt 7, upper pipeline 8 is connected with the upper end of column mixing chamber 6, the lower end of column mixing chamber 6 is communicated with the initial end of upper pipeline 8 with the lower pipeline 10 that is connected in the lower cover 4 by following connecting bolt 9, the end of lower pipeline 10 all links to each other with blender joint 1.
Described hybrid chamber unit is a plurality of, equidistantly is axially disposed within on loam cake 3 and the lower cover 4.
Described sealing bolt 2 is a plurality of, and axially is arranged on symmetrically on loam cake 3 and the lower cover 4.
Described sealing gasket 5 is provided with positioning pin column 11, and loam cake 3 is provided with the locating hole that matches with positioning pin column 11.
The utility model is compared with prior art, has following advantage:
The chromatograph of this kind of version high pressure static mixer adopts two-piece type, multi-cavity body structure, and under the precondition that does not influence mixed effect, mixed structure is simple relatively, thereby has reduced processing and assembling difficulty; The characteristics on its little cavity, tubule road have guaranteed minimizing of internal volume; The employing of sealing bolt, sealing gasket guarantees that blender can tolerate high pressure; The connected mode of multi-cavity external body polyphone can be switched mixed volume at the most at one grade between the shelves.Therefore we can say that it has possessed multiple advantage, be particularly suitable for applying in the art that its market prospects are very wide.
Description of drawings
Fig. 1 is the vertical view of the utility model embodiment.
Fig. 2 is the front view of the utility model embodiment.
Fig. 3 is that the A-A of Fig. 1 is to postrotational cutaway view.
Fig. 4 is the structural representation of the utility model embodiment stereoscopic-state.
The specific embodiment
Below in conjunction with the description of drawings specific embodiment of the present utility model.As Fig. 1, Fig. 2, Fig. 3, shown in Figure 4: a kind of chromatograph high pressure static mixer, it comprises blender joint 1, be fixedly connected with loam cake 3 and the lower cover 4 of mutual snapping in a side of blender joint 1, fix by a plurality of sealing bolts symmetrically arranged, that axially evenly divide between loam cake 3 and the lower cover 4, and between loam cake 3 and lower cover 4, also be folded with sealing gasket 5; For accurate location, the side towards loam cake 3 on sealing gasket 5 also is provided with two positioning pin columns 11, and loam cake 3 corresponding faces are provided with the locating hole that matches with this positioning pin column 11; After loam cake 3, lower cover 4 closures, form column mixing chamber 6 jointly, in loam cake 3, be provided with hollow on connecting bolt 7, cross-under has upper pipeline 8 in it, this upper pipeline 8 is connected with the upper end of column mixing chamber 6; And the lower end of column mixing chamber 6 is connected with the lower pipeline 10 that is fixed in the lower cover 4 by following connecting bolt 9, and the initial end of above-mentioned upper pipeline 8, the end of lower pipeline 10 all link to each other with blender joint 1; Above-mentioned column mixing chamber 6, last connecting bolt 7, upper pipeline 8, following connecting bolt 9 and the lower pipeline 10 common hybrid chamber unit of forming, in order to obtain the better mixing effect, described hybrid chamber unit can be for a plurality of, and equidistantly are axially disposed within on loam cake 3 and the lower cover 4.
The chromatograph of the utility model embodiment is as follows with the course of work of high pressure static mixer: two or more liquid that need mix, enter upper pipeline 8 by blender joint 1, and enter the column mixing chamber 6 from the upper end away from first column mixing chamber 6 of blender joint 1 direction, mix, lower end from this column mixing chamber 6 enters lower pipeline 10 then, and enter the lower end of second column mixing chamber 6 by lower pipeline 10, after carrying out therein mixing the second time, upper pipeline 8 from its upper end enters the upper end of the 3rd column mixing chamber 6, and by that analogy, in all column mixing chambers 6, finish hybrid working until mixed liquor, discharge by the pipeline on the blender joint 1 at last.

Claims (4)

1. chromatograph high pressure static mixer, it is characterized in that: described blender comprises blender joint (1), side at blender joint (1) is provided with loam cake (3) and the lower cover (4) that connects as one structure by sealing bolt (2), between loam cake (3) and lower cover (4), be folded with sealing gasket (5), between loam cake (3) and lower cover (4), be provided with the hybrid chamber unit, described hybrid chamber unit is by column mixing chamber (6), the last connecting bolt (7) that matches, upper pipeline (8), the following connecting bolt (9) that matches, lower pipeline (10) is formed, column mixing chamber (6) is arranged between loam cake (3) and the lower cover (4), be provided with hollow last connecting bolt (7) in the loam cake (3), the interior cross-under of last connecting bolt (7) has upper pipeline (8), upper pipeline (8) is connected with the upper end of column mixing chamber (6), the lower end of column mixing chamber (6) is communicated with the initial end of upper pipeline (8) with the lower pipeline (10) that is connected in the lower cover (4) by following connecting bolt (9), the terminal of lower pipeline (10) all links to each other with blender joint (1).
2. chromatograph according to claim 1 high pressure static mixer, it is characterized in that: described hybrid chamber unit is a plurality of, equidistantly is axially disposed within on loam cake (3) and the lower cover (4).
3. chromatograph according to claim 2 high pressure static mixer is characterized in that: described sealing bolt (2) is for a plurality of, and axially is arranged on symmetrically on loam cake (3) and the lower cover (4).
4. chromatograph according to claim 3 high pressure static mixer, it is characterized in that: described sealing gasket (5) is provided with positioning pin column (11), and loam cake (3) is provided with the locating hole that matches with positioning pin column (11).
CN2012207052111U 2012-12-19 2012-12-19 High-pressure static mixer for chromatographic instrument Expired - Fee Related CN203061073U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012207052111U CN203061073U (en) 2012-12-19 2012-12-19 High-pressure static mixer for chromatographic instrument

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2012207052111U CN203061073U (en) 2012-12-19 2012-12-19 High-pressure static mixer for chromatographic instrument

Publications (1)

Publication Number Publication Date
CN203061073U true CN203061073U (en) 2013-07-17

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106501428A (en) * 2016-10-24 2017-03-15 南方医科大学 A kind of substep focuses on the method for combined use of axial mixed high-efficient liquid chromatographic separation system
US11185830B2 (en) 2017-09-06 2021-11-30 Waters Technologies Corporation Fluid mixer
US11555805B2 (en) 2019-08-12 2023-01-17 Waters Technologies Corporation Mixer for chromatography system
US11821882B2 (en) 2020-09-22 2023-11-21 Waters Technologies Corporation Continuous flow mixer
US11898999B2 (en) 2020-07-07 2024-02-13 Waters Technologies Corporation Mixer for liquid chromatography

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106501428A (en) * 2016-10-24 2017-03-15 南方医科大学 A kind of substep focuses on the method for combined use of axial mixed high-efficient liquid chromatographic separation system
CN106501428B (en) * 2016-10-24 2018-02-23 南方医科大学 A kind of substep focuses on the method for combined use of axial mixed high-efficient liquid chromatographic separation system
US11185830B2 (en) 2017-09-06 2021-11-30 Waters Technologies Corporation Fluid mixer
US11555805B2 (en) 2019-08-12 2023-01-17 Waters Technologies Corporation Mixer for chromatography system
US11898999B2 (en) 2020-07-07 2024-02-13 Waters Technologies Corporation Mixer for liquid chromatography
US11821882B2 (en) 2020-09-22 2023-11-21 Waters Technologies Corporation Continuous flow mixer

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130717

Termination date: 20191219

CF01 Termination of patent right due to non-payment of annual fee