CN203048606U - Spraying and rotational flow washing device for expansible graphite - Google Patents

Spraying and rotational flow washing device for expansible graphite Download PDF

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Publication number
CN203048606U
CN203048606U CN2012206498873U CN201220649887U CN203048606U CN 203048606 U CN203048606 U CN 203048606U CN 2012206498873 U CN2012206498873 U CN 2012206498873U CN 201220649887 U CN201220649887 U CN 201220649887U CN 203048606 U CN203048606 U CN 203048606U
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China
Prior art keywords
washing
rotational flow
spraying
water
still
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Expired - Fee Related
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CN2012206498873U
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Chinese (zh)
Inventor
罗成旺
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Jixi Universal Graphite Co ltd
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YICHANG XINCHENG GRAPHITE CO Ltd
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Abstract

The utility model provides a spraying and rotational flow washing device for expansible graphite. The spraying and rotational flow washing device comprises a washing kettle, wherein a spraying pipe is arranged on the upper part of the washing kettle, a stirring mechanism and a water filtration inner wall are arranged in the washing kettle, a drain pipe is arranged at the bottom of the washing kettle, and a blow-off pipe penetrates through the bottom of the kettle and is communicated with a water filtration concave bottom of the water filtration inner wall. The spraying and rotational flow washing device is uniform in washing, and has little influence on the quality and expansion multiplying power of raw materials in the washing process and does not reduce the expansion times of the raw materials. Water consumption is substantially reduced, more than 160 tons of water is consumed for washing one ton of raw materials by the conventional method, 60-80 tons of water is consumed by the spraying and rotational flow washing manner, the water consumption is reduced by more than 50%, and the reduction of production cost is facilitated. The spraying and rotational flow washing device is simple in operation, and as long as a spraying water source is opened, the stirring mechanism is started, and a drain valve is adjusted, washing can be carried out. After washing is ended, a blow-off valve is opened, and bagging and dehydration are not needed, thus environmental protection is facilitated. The spraying and rotational flow washing device has high washing efficiency. Only one tone of raw materials can be washed per shift by the conventional method, and more than five tones of raw materials can be washed per shift by the spraying and rotational flow washing device, so that the production capacity is facilitated to be expanded.

Description

Expansible black lead rotational flow and spray washing device
Technical field
The utility model relates to a kind of graphite production unit, particularly a kind of expansible black lead rotational flow and spray washing device.
Background technology
Natural flake graphite, likeness in form fish scale shape belongs to hexagonal system, is laminate structure.Expansible black lead is produced, and is to utilize acid ion that the graphite interbed is carried out intercalation to separate, and sends into High Temperature Furnaces Heating Apparatus after washing drying, can make its volume moment that the expansion of tens of times and even hundreds of times takes place.Its production process is: use the vitriol oil and crystalline flake graphite to fill a prescription in proportion to drop into special reactor and carry out intercalation.Reacted graphite whisker washs through clear water, makes its pH=5 ~ 6, reaches neutral, gets final product through dehydrating again.
Traditional washing methods is as shown in Figure 3: make wooden square drainage trap, the base plate drainage aperture that gathers by oneself, the pad upper filter screen is contained reacted graphite raw material, manually holds diameter and be 60 ~ 80 water pipe, wash repeatedly with a large amount of clear water, qualified just now after detection reaches neutrality.Perhaps make square or bulge by oneself, the drainage lattice are put at the end, and built-in filter screen is put into reacted graphite raw material, and a water tap is established on top, open the water source flushing of flowing automatically for a long time, and sewage is discharged from the bottom, (seeing synoptic diagram two).These purging methods have been felt deficiency and the shortcoming of its existence deeply in long term production: the one, and the original backwardness of these methods, production efficiency is extremely low; The 2nd, production environment is very abominable, pollutes wayward; The 3rd, the workman operates heavy, and flush time is long, and is very tired; The 4th, water loss is big, causes water resource waste, increases production cost; The 5th, rinsing quality is difficult for grasping, and loses expansion multiplying power easily; The 6th, the raw material after the flushing need manually dig out pack and dewater, and labour intensity is big; The 7th, excessive because of water pipe hydraulic pressure in the flushing process, splash fly out spray and material and cause wastage of material.Therefore, flushing in the expansible black lead production process, dehydration, drying all are the important steps of restriction production efficiency and material quality.
Summary of the invention
At the deficiencies in the prior art, the purpose of this utility model provides a kind of expansible black lead rotational flow and spray washing device, can improve detersive efficiency and the washing effect of expansible black lead, improves the taste of raw material.
The purpose of this utility model is achieved in that a kind of expansible black lead rotational flow and spray washing device, comprise the washing still, washing still top is provided with shower, be provided with stirring mechanism in the washing still, in the washing still, also be provided with the drainage inwall, the still bottom of washing still is provided with water shoot, and drainage conduit is communicated with at the bottom of passing at the bottom of the still drainage spill with the drainage inwall.
Also be provided with the heating tube that is connected with hot water or steam between the inwall of described drainage inwall and washing still.
Described stirring mechanism is fixedly mounted on the top of washing still, and agitating vane extend into the washing still near the position at the bottom of the drainage spill.
Described drainage inwall is formed at the bottom of by sidewall filter screen and drainage spill.
In the arc-shaped or conical at the bottom of the described drainage spill, drainage conduit is positioned at the position of axis.
Described shower circularizes the position that is positioned near washing still inwall.
Described shower is along being distributed with 2-3 spray apertures on the circumference in its cross section.
Described spray apertures by inwardly, inwardly under the skew back and direction down arrange.
Described washing still top is provided with feeding trough.
A kind of expansible black lead rotational flow and spray washing device that the utility model provides, reacted raw material water lowered the temperature and enter in the washing still, opening the water intaking valve that is connected with shower evenly sprays water by washing still upper spray pipe, start stirring mechanism, when needing heating at built-in coil pipe, be to feed hot water in the heating tube or steam heats, utilize the clear water principle different with sour water proportion, top spray clear water, heavy sour water utilize to be stirred in the eddy flow that forms in the container toward the bottom sedimentation, make material in water, be the swirling flow state, both can avoid material to stop up filter screen, and can make sour water accelerate again, to accelerate washing speed.Detersive efficiency of the present utility model and washing effect are all very good.
The utility model is compared the conventional washing method, its advantage: the one, and changing artificial flushing is the rotational flow and spray washing, and washing is even, and washing process is very little to material quality and expansion multiplying power influence, can significantly not reduce the raw material expansion multiple.
The 2nd, water consumption significantly reduces, and one ton of raw material of traditional method flushing needs water consumption more than 160 tons, and existing rotational flow and spray washing water consumption is 60 ~ 80 tons, and water loss reduces more than 50%, is conducive to reduce production costs.
The 3rd, production environment is greatly improved, and material concentrates on washing in the still, not impacted by hydraulic pressure and spill.
The 4th, simple to operate, only need open the spray water source, start stirring mechanism, regulate water discharge valve and get final product.Washing is finished, and opens blow-off valve, need not the pack dehydration, is conducive to environment protection again.
The 6th, the detersive efficiency height, order of classes or grades at school of traditional method only washes one ton of raw material, and existing order of classes or grades at school can wash more than five tons, is conducive to expand production capacity.
The 7th, behind this washing methods of employing, the filter screen hole is reduced, reduced the washed away ratio of particulate starting material, reduced waste.Traditional method leaches in order to accelerate wash-down water, selects for use the filter screen mesh bigger, and during flushing, a large amount of particulate starting materials are flushed away, the place that is flushed to by water tap not, and under the pressure of raw material and water, opening of sieve is blocked easily, and wash-down water is difficult for discharging.The washing of employing rotational flow and spray, whole filtering net is in flow state when contacting with water with raw material, be difficult for stopping up filter screen, has reduced wastage of material; Sour water sedimentation in eddy flow is easily discharged, and has improved detersive efficiency.
The 8th, this equipment not only can be used for washing, also can be used for raw material reacting by heating in the still, improves the raw material grade.
Description of drawings
The utility model is described in further detail below in conjunction with drawings and Examples.
Fig. 1 is one-piece construction synoptic diagram of the present utility model.
Fig. 2 is the partial enlarged drawing at A place among Fig. 1.
Fig. 3 is the structural representation of rinse bath in the prior art.
Among the figure: water intaking valve 1, washing still 2, shower 3, spray apertures 31, stirring mechanism 4, heating tube 5, drainage inwall 6, sidewall filter screen 7, at the bottom of the drainage spill 8, at the bottom of the still 9, water shoot 10, water discharge valve 11, blow-off valve 12, drainage conduit 13, feeding trough 14.
Embodiment
In Fig. 1, a kind of expansible black lead rotational flow and spray washing device comprises washing still 2, and described washing still 2 tops are provided with feeding trough 14.Washing still 2 tops are provided with shower 3, and shower 3 is by water intaking valve 1 and clear water pipe coupling.Washing is provided with stirring mechanism 4 in the still 2, and the scheme of optimizing in this example is, described stirring mechanism 4 is fixedly mounted on the top of washing still 2, and agitating vane extend into washing still 2 near 8 position at the bottom of the drainage spills.
Also be provided with drainage inwall 6 in washing in the still 2, in the scheme of optimization, described drainage inwall 68 is formed at the bottom of by sidewall filter screen 7 and drainage spill.8 is in the arc-shaped or conical at the bottom of the described drainage spill, and drainage conduit 13 is positioned at the position of axis, is beneficial to discharge.
9 places are provided with water shoot 10 at the bottom of the still of washing still 2, drainage conduit 13 pass at the bottom of the still 9 with 8 be communicated with at the bottom of the drainage spill of drainage inwall 6.
Also be provided with the heating tube 5 that is connected with hot water or steam between the inwall of described drainage inwall 6 and washing still 2.
Described shower 3 circularizes the position that is positioned near washing still 2 inwalls.
In Fig. 2, described shower 3 when being distributed with 31,3 spray apertures 31 of 2-3 spray apertures on the circumference in its cross section, by inwardly, inwardly under the skew back and direction down arrange; During 2 spray apertures 31, by by arranging under the skew back inwardly and inwardly.Between spray apertures 31 of each row at a distance of 80-120mm.Structure is guaranteed that the clear water that sprays covers the material in the washing still 2, thereby can be saved the water purification of spray usefulness thus.
Embodiment:
In Fig. 1, washing still 2 is for to make bulge with corrosion resistant material, and the upper edge arranges a circle coil pipe, and namely shower 3, along shower 3 offer level inwards, inwards 45 °, the even staggered water spray aperture of square triplex row vertically downward, can evenly spray weep on bulge top after the water flowing.Container bottom arranges one pot of shape round bottom, arranges even water vent, and the bottom arranges at the bottom of the still 9 again, collects the sewage that leaches, and enters special-purpose treatment tank by a water shoot 10 pipes.Container inner wall is arranged a few coil pipes from top to bottom as heating tube 5, can feed hot water or steam heats.Drainage inwall 6 and sidewall filter screen 7 are set in the container, and the centre arranges agitating vane.
During washing, reacted material is entered in the washing still 2 by tremie pipe or feeding trough 14, open clear water water intaking valve 1,3 of showers evenly spray clear water in still, start stirring mechanism 4, material and water then form whirlpool eddy flow shape in the still under the whipping force effect, constantly replenish down at the spray clear water, sour water sinks with eddy flow than conference because of proportion, enter at the bottom of the still through the densely covered aperture on 8 at the bottom of drainage inwall 6 and sidewall filter screen 7 and the drainage spill, enter special-purpose neutralizing treatment pond through water shoot 10, water discharge valve 11 again.When needing heating, can feed steam or hot water by heating tube 5.Washing is finished, reach neutrality after testing after, close water discharge valve 11, open blow-off valve 12, material can enter the pond that gathers materials by drainage conduit 13 with clear water and enter the dehydration link.
In the washing process, close blow-off valve 12, liquid level height in the washing still can be regulated control by water discharge valve 11.

Claims (9)

1. expansible black lead rotational flow and spray washing device, comprise washing still (2), it is characterized in that: washing still (2) top is provided with shower (3), be provided with stirring mechanism (4) in the washing still (2), in washing still (2), also be provided with drainage inwall (6), (9) locate to be provided with water shoot (10) at the bottom of the still of washing still (2), and (8) were communicated with at the bottom of drainage conduit (13) was passed the drainage spill of (9) and drainage inwall (6) at the bottom of the still.
2. a kind of expansible black lead rotational flow and spray washing device according to claim 1 is characterized in that: also be provided with the heating tube (5) that is connected with hot water or steam between the inwall of described drainage inwall (6) and washing still (2).
3. a kind of expansible black lead rotational flow and spray washing device according to claim 1, it is characterized in that: described stirring mechanism (4) is fixedly mounted on the top of washing still (2), and agitating vane extend into washing still (2) near the position of (8) at the bottom of the drainage spill.
4. a kind of expansible black lead rotational flow and spray washing device according to claim 1 is characterized in that: described drainage inwall (6) by sidewall filter screen (7) and drainage spill at the bottom of (8) form.
5. a kind of expansible black lead rotational flow and spray washing device according to claim 4, it is characterized in that: (8) are in the arc-shaped or conical at the bottom of the described drainage spill, and drainage conduit (13) is positioned at the position of axis.
6. a kind of expansible black lead rotational flow and spray washing device according to claim 1 is characterized in that: described shower (3) circularizes the position that is positioned near washing still (2) inwall.
7. a kind of expansible black lead rotational flow and spray washing device according to claim 6, it is characterized in that: described shower (3) is along being distributed with 2-3 spray apertures (31) on the circumference in its cross section.
8. a kind of expansible black lead rotational flow and spray washing device according to claim 7 is characterized in that: described spray apertures (31) by inwardly, inwardly under the skew back and direction down arrange.
9. a kind of expansible black lead rotational flow and spray washing device according to claim 1 is characterized in that: be provided with feeding trough (14) above the described washing still (2).
CN2012206498873U 2012-12-02 2012-12-02 Spraying and rotational flow washing device for expansible graphite Expired - Fee Related CN203048606U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012206498873U CN203048606U (en) 2012-12-02 2012-12-02 Spraying and rotational flow washing device for expansible graphite

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2012206498873U CN203048606U (en) 2012-12-02 2012-12-02 Spraying and rotational flow washing device for expansible graphite

Publications (1)

Publication Number Publication Date
CN203048606U true CN203048606U (en) 2013-07-10

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109772570A (en) * 2017-11-13 2019-05-21 刘贤铨 A kind of novel washing methods
CN109850897A (en) * 2018-12-21 2019-06-07 滑县大潮林物产有限责任公司 A kind of super capacitor carbon production rinse-system

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109772570A (en) * 2017-11-13 2019-05-21 刘贤铨 A kind of novel washing methods
CN109850897A (en) * 2018-12-21 2019-06-07 滑县大潮林物产有限责任公司 A kind of super capacitor carbon production rinse-system

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20180716

Address after: 158130 Liumao Village, Liumao Township, Hengshan District, Jixi City, Heilongjiang Province

Patentee after: Jixi universal graphite Co.,Ltd.

Address before: 444100 30 east section of Jinping Avenue, baling development area, Dangyang city, Yichang, Hubei

Patentee before: YICHANG XINCHENG GRAPHITE Co.,Ltd.

TR01 Transfer of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130710

Termination date: 20211202

CF01 Termination of patent right due to non-payment of annual fee