CN202870010U - Portable magnesium sulfate detection instrument - Google Patents

Portable magnesium sulfate detection instrument Download PDF

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Publication number
CN202870010U
CN202870010U CN 201220573804 CN201220573804U CN202870010U CN 202870010 U CN202870010 U CN 202870010U CN 201220573804 CN201220573804 CN 201220573804 CN 201220573804 U CN201220573804 U CN 201220573804U CN 202870010 U CN202870010 U CN 202870010U
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CN
China
Prior art keywords
micro
wave oven
microwave oven
magnesium sulfate
monosodium glutamate
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 201220573804
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Chinese (zh)
Inventor
张丽华
刘玉静
马春影
毕海燕
刘岩
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Bohai University
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Bohai University
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Publication date
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Priority to CN 201220573804 priority Critical patent/CN202870010U/en
Application granted granted Critical
Publication of CN202870010U publication Critical patent/CN202870010U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model relates to a portable magnesium sulfate detection instrument. The portable magnesium sulfate detection instrument comprises a microwave oven and is characterized in that glass ware is placed in the microwave oven, wherein the diameter of the glass ware is 90-150 mm, the height of the glass ware is 18-22 mm, a handle is arranged at the top face of the microwave oven, hinge frames are hinged at the side face of the microwave oven, a telescopic pull rod is arranged on the hinge frames, idler wheels are arranged at the bottom of the microwave oven, and a power indicator, a start switch and a timer with a warning function are arranged on a face plate of the microwave oven. According to the magnesium sulfate detection instrument, the qualitative authentication can be carried out on doping of magnesium sulfate in monosodium glutamate, the detection is convenient, the operation is simple, the carrying and the moving are convenient, the detection cost is low, and the detection speed is quick.

Description

Portable magnesium sulphate detector
Technical field
The utility model relates to a kind of portable magnesium sulphate detector.
Background technology
Monosodium glutamate is people's daily life flavouring commonly used, is a kind of column crystal of white granular.Magnesium sulphate is the crystallization of colourless quadrangular prism shape or granular crystal, and from the appearance, to monosodium glutamate and similar, naked eyes are difficult the resolution extremely.Higher economic interests are pursued in order to reduce cost by illegal businessman in recent years, add excessive magnesium sulphate in monosodium glutamate, and sodium glutamate is seriously not up to standard.
The magnesium sulphate bitter, soluble in water, it is a kind of bulk cathartic, if people take concentration excessive Adlerika, can cause the eater to dewater, poison, Symptoms is stomach severe pain, vomiting, diarrhoea, expiratory dyspnea mydriasis, bladder and kidney is unable, shock, severe person's bradycardia, blood pressure drops, lethargic sleep, stupor; Suck for a long time low dose of magnesium sulphate, can cause constipation and paralytic ileus.Therefore, for ensureing the healthy of the people, check in the monosodium glutamate content of magnesium sulphate severely most important.
Stipulate among the GB/T8967-2000 that State Bureau of Technical Supervision implemented on September 1st, 2000 that sulfate is (with SO in the monosodium glutamate 4 2-Meter) content is not more than 0.05%.The mensuration of sulfate is to use the barium chloride precipitation method in the GB, and the method also needs number of chemical reagent and various glass apparatus except the exact instrument such as needs electronic balance.When the barium chloride precipitation method detect, when colorimetric, need carry out visually than turbid, if the sample hose turbidity is not higher than the standard pipe turbidity, be equal to or less than 0.05% with regard to sulphates content in the interpret sample.The mensuration of sulfate is to use the barium chloride precipitation method in the GB, and the method can not accurately detect the content of magnesium ion.When more accurately detecting the content of magnesium sulphate such as need, usually adopt the atomic absorption spectrophotometer (AAS) method to detect the accurate content of magnesium ion, the method also will have atomic absorption spectrophotometer (AAS) and support equipment (such as acetylene cylinder, acetylene gas etc.) except using number of chemical reagent and glass apparatus.Metalization of skin is expensive, and domestic about 120,000.
Whether barium chloride precipitation method detecting the contet of sulphate content exceeds standard, and error is large, wastes time and energy.The atomic absorption spectrophotometer (AAS) method is higher to equipment requirement, complicated operation.No matter be the barium chloride precipitation method or detect magnesium sulphate content with the atomic absorption spectrophotometer (AAS) method, all need to prepare number of chemical reagent, increase testing cost, detect the result and need at least three hours from sampling during detection, length consuming time, also need simultaneously the operator to have certain professional knowledge and stronger operative skill, the discrimination method that sulfate is commonly used is the method with the barium chloride precipitation, this large time of method error grows up to this height, needs number of chemical reagent and glass apparatus, and the atomic absorption spectrophotometer (AAS) method detects the content of magnesium ion, the result is accurate, but complicated operation, the time is long, and cost is high.
Summary of the invention
The technical problems to be solved in the utility model provides a kind of portable magnesium sulphate detector that carries out qualitative discriminating to mixing magnesium sulphate in the monosodium glutamate, and this detector is easy to detect, simple to operate, be easy to carry and move, and testing cost is low, detection speed is fast.
Technical solution of the present utility model is:
A kind of portable magnesium sulphate detector, comprise micro-wave oven, its special character is: be placed with glassware in micro-wave oven, the diameter of described glassware is 90mm-150mm, highly is 18mm-22mm, is provided with handle at the micro-wave oven end face, in the micro-wave oven side hinged hinged, be provided with telescopic lever at the hinge frame, be provided with roller in the micro-wave oven bottom, be provided with the timer of power light, starting switch and band warning at the panel of micro-wave oven.
The beneficial effects of the utility model are: by microwave heating, make the magnesium sulphate in the monosodium glutamate that contains magnesium sulphate lose water of crystallization, after magnesium sulphate loses water of crystallization, become white particles, this granule and monosodium glutamate particle have obvious difference; Magnesium sulphate is dissolved in self water of crystallization, and makes most of magnesium sulphate and small part monosodium glutamate be gathered in container bottom when losing water of crystallization in addition, with the monosodium glutamate particle of dispersing significant difference is arranged also, thereby is judged whether have magnesium sulphate to exist in the monosodium glutamate.In glassware, add 20-50 gram monosodium glutamate sample to be detected during each the detection, carry out 2-6 minute thermal treatment after starting micro-wave oven, if glassware bottom and edge have the cohesion adsorbate to exist, or the white powder that exists between the monosodium glutamate particle, then mixed magnesium sulphate in the monosodium glutamate; If glassware bottom and edge be without the existence of cohesion adsorbate, and between the monosodium glutamate particle without white powder, then do not mix magnesium sulphate in the monosodium glutamate.Owing to being provided with roller in micro-wave oven bottom and being provided with telescopic lever in the micro-wave oven side and being provided with handle at the micro-wave oven end face, being convenient to mobile and carrying; Volume is little, is easy to carry; Easy to detect, simple to operate, testing cost is low, detection speed is fast.
Description of drawings
Fig. 1 is structural representation of the present utility model;
Among the figure: micro-wave oven 1, handle 2, telescopic lever 3, hinge frame 4, roller 5, glassware 6, starting switch 7, the timer 8 that band is reported to the police, power light 9.
Embodiment
As shown in the figure, this portable magnesium sulphate detector, comprise micro-wave oven 1, in micro-wave oven 1, be placed with glassware 6, the diameter of described glassware 6 is 90mm-150mm, highly be 18mm-22mm, the diameter of glassware 6 is 120 mm in the present embodiment, height is 20 mm, be provided with handle 2 at micro-wave oven 1 end face, in micro-wave oven 1 side hinged hinged 4, be hinged with telescopic lever 3 at hinge frame 4, be provided with four rolling 5 in micro-wave oven 1 bottom, be provided with power light 9 at the panel of micro-wave oven 1, the timer 8 that is used for the band warning of control microwave heating time, be used for starting the starting switch 7 of microwave heating.
During detection, accurately take by weighing the 20g monosodium glutamate, put into glassware 6, again glassware 6 is put into micro-wave oven 1, set microwave power 800W, be 3min heat time heating time, press starting switch 7 after, micro-wave oven begin the heating, behind setting-up time, be with timer 8 disconnecting circuits and the warning of reporting to the police, take out glassware 6, jiggle glassware 6, observations, if there are different big or small condensation products glassware 6 bottoms with the edge, also visible adularescent powder exists between the monosodium glutamate particle, and this white powder and monosodium glutamate particle have obvious difference, show to have mixed magnesium sulphate in the monosodium glutamate.If glassware 6 bottoms all do not have different big or small condensation products with the edge, show that monosodium glutamate does not mix magnesium sulphate.

Claims (1)

1. portable magnesium sulphate detector, comprise micro-wave oven, it is characterized in that: in micro-wave oven, be placed with glassware, the diameter of described glassware is 90mm-150mm, highly is 18mm-22mm, is provided with handle at the micro-wave oven end face, in the micro-wave oven side hinged hinged, be provided with telescopic lever at the hinge frame, be provided with roller in the micro-wave oven bottom, be provided with the timer of power light, starting switch and band warning at the panel of micro-wave oven.
CN 201220573804 2012-11-04 2012-11-04 Portable magnesium sulfate detection instrument Expired - Fee Related CN202870010U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220573804 CN202870010U (en) 2012-11-04 2012-11-04 Portable magnesium sulfate detection instrument

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201220573804 CN202870010U (en) 2012-11-04 2012-11-04 Portable magnesium sulfate detection instrument

Publications (1)

Publication Number Publication Date
CN202870010U true CN202870010U (en) 2013-04-10

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CN 201220573804 Expired - Fee Related CN202870010U (en) 2012-11-04 2012-11-04 Portable magnesium sulfate detection instrument

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CN (1) CN202870010U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102680510A (en) * 2012-05-30 2012-09-19 渤海大学 Method for qualitatively identifying magnesium sulfate mixing in monosodium glutamate
CN108918517A (en) * 2018-05-15 2018-11-30 汕尾市食品药品检验所 A method of the magnesium sulfate illegally added in detection Chinese medicine and medicine materical crude slice

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102680510A (en) * 2012-05-30 2012-09-19 渤海大学 Method for qualitatively identifying magnesium sulfate mixing in monosodium glutamate
CN102680510B (en) * 2012-05-30 2013-10-23 渤海大学 Method for qualitatively identifying magnesium sulfate mixing in monosodium glutamate
CN108918517A (en) * 2018-05-15 2018-11-30 汕尾市食品药品检验所 A method of the magnesium sulfate illegally added in detection Chinese medicine and medicine materical crude slice

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C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130410

Termination date: 20131104