CN202778458U - Low-negative-pressure-resistant teflon lining reaction tank - Google Patents

Low-negative-pressure-resistant teflon lining reaction tank Download PDF

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Publication number
CN202778458U
CN202778458U CN 201220334031 CN201220334031U CN202778458U CN 202778458 U CN202778458 U CN 202778458U CN 201220334031 CN201220334031 CN 201220334031 CN 201220334031 U CN201220334031 U CN 201220334031U CN 202778458 U CN202778458 U CN 202778458U
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tank
tetrafluoro
tank body
cover
negative pressure
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Expired - Fee Related
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CN 201220334031
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Chinese (zh)
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胡永庆
贾建新
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Individual
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Abstract

The utility model relates to a low-negative-pressure-resistant teflon lining reaction tank which comprises a tank body, a tank bottom and a tank lid, wherein the tank body and the tank bottom are welded together; the outer sides of the tank body and the tank bottom are provided with a jacket body, and a cavity is formed among the jacket body, the tank body and the tank bottom; the bottom of the tank bottom is provided with a discharge outlet, and the tank lid is provided with pipe orifices; and the tank is characterized in that a teflon lining layer is adhered to the internal surfaces of the tank body, the tank lid and the tank bottom through an adhering layer, and the teflon lining layer is closely adhered to the inner wall surfaces of the tank body, the tank lid and the tank bottom; a first pressure vessel flange is welded at the upper end of the tank body, a second pressure vessel flange is welded at the lower end of the tank lid, and the tank body and the tank lid are connected and fastened through the first pressure vessel flange, the second pressure vessel flange and a double-headed stud; and the pipe orifices are respectively provided with a flange for pressure vessel tubes. The tank disclosed by the utility model can run for a long time under high-temperature and low-negative-pressure working conditions and no shelling, swelling and tearing occur.

Description

The tetrafluoro of anti-lower negative pressure lining retort
Technical field
The utility model relates to a kind of tetrafluoro of anti-lower negative pressure lining retort, especially a kind of retort of finishing the processes such as the reaction of material, synthetic, polymerization, chlorination for chemical industry, pharmaceutical engineering, and the negative pressure of minimum ability is-0.03MPa.
Background technology
In existing technology, retort lining tetrafluoro is because of the technical barrier such as can't process the bulge of tetrafluoro plate lining, shell, tear, and causes tetrafluoro plate lining to lose efficacy under high temperature and high pressure condition.For the arts demand of empty set lining, usually adopt two flange arrangements, namely cover is with tank body, tank body and respectively be connected fastening with a pair of main flange at the bottom of the tank.Heating jacket has to be divided into up and down two parts, has reduced the heating surface (area) (HS of chuck,, simultaneously, be connected to a pair of flange in retort lower end and numerous double-screw bolt and nuts, wasted heat, wasted heat energy, limited the intensification of retort, the normal function of heating.
In existing technology, the inwall in empty set tetrafluoro plate retort matches by its internal diameter size, makes the tetrafluoro inner sleeve, and empty set is in tank, and the space that exists 1~3mm not wait between tank skin and the lining has formed the natural air interlayer.The sealing surface of retort master's flange and each mouth of pipe is not made adhesion process with the flange flange of tetrafluoro lining yet.Can't form Sealed sandwich between cover and can body and the tetrafluoro plate lining, the interlayer Air is in free state forever.When retort under high temperature, lower negative pressure operating mode, the every intensity index of PTFE sharply descends.The air of interlayer is heated suddenly and expands, lining has been produced external pressure has been subjected to again lower negative pressure effect in the tank simultaneously, tetrafluoro plate lining under the dual-pressure effect, unstability and produce shelling, tear or deformation of cylindrical.
In existing technology, also have on above-mentioned empty set tetrafluoro plate base, added adhesive, very smooth smooth on the surface, but producer offers some clarification on not ability negative pressure, and can not be high temperature resistant; Having added wire netting also can only anti-little negative pressure, 110~120 ℃ of operating temperatures, but still be two flange arrangements.
In order to solve the dual pressurized problem of lining, manufactory once adopted remedial measure to be, adopt vacuum line with the tetrafluoro lining interlayer of retort cover and retort tank body tetrafluoro plate lining interlayer at retort outside pipeline connection, vavuum pump is communicated with vacuum line, consist of vacuum system, vavuum pump and retort vacuum system start close synchronously synchronously, make the interlayer place what vacuum state of tetrafluoro plate lining and tank skin, with the negative pressure in the tank that contends with.Although on principle, as if solved the vacuum equalization problem, but ignored the impact of the linear expansion stress of PTFE deadweight under the high temperature, boundary stress that the agitator rotation produces, PTFE, under these composite factor effects, tetrafluoro plate lining or deformation of cylindrical.Therefore, empty set tetrafluoro plate retort can't solve the tetrafluoro plate that the serves as a contrast problem of anti-negative pressure at high temperature.
Summary of the invention
The purpose of this utility model is to overcome the deficiencies in the prior art, and a kind of tetrafluoro of anti-lower negative pressure lining retort is provided, can be under high temperature, lower negative pressure long-term operation and do not shell, not bulge, the tetrafluoro lining retort product do not torn.
According to the technical scheme that the utility model provides, a kind of tetrafluoro of anti-lower negative pressure lining retort comprises at the bottom of tank body, the tank and cover, and tank body and tank back welding connect and form, and agitator is installed in tank body; The outside is provided with jacket body at the bottom of described tank body and tank, has cavity between at the bottom of jacket body and tank body and the tank; Bottom at the bottom of described tank is provided with drain hole, is provided with a plurality of mouths of pipe at described cover; Feature is: the inner wall surface at described tank body, End Pieces is passed through the bonding tetrafluoro backing layer of adhesive layer, the inner wall surface close adhesion of tetrafluoro backing layer and tank body, End Pieces; Weld the first pressure container flange in the upper end of described tank body, the second pressure container flange is welded in the lower end of cover, and tank body is connected the first pressure container flange, the second pressure container flange and studs and connects fastening with cover; The described mouth of pipe all arranges the effective flange of the effective pressure vessel of pressure vessel.
Described jacket body comprises the chuck that is located at the tank body outside and is located at the basolateral jacket head of tank, is provided with condensate drain outlet at jacket head, is provided with heating agent entrance sleeve and the heating agent discharge connection that is communicated with the jacket body internal cavity at chuck.
The mouth of pipe on the described cover comprises manhole, charge door, temperature-measuring port, relief valve port, mouth for subsequent use, visor hole and lamp hole.
The shaft of described agitator stretches out the cover outside, and is connected with the output shaft of the reductor that is arranged on the cover top.
Described reductor is installed in the top of cover by the reductor support.
The thickness of described tetrafluoro backing layer is 2~4mm.
Between described the first pressure container flange and the second pressure container flange, sealing gasket is set.
Be connected with T-Ring at described tank body, the lower end at the bottom of tank is connected with lower T-Ring, and upper T-Ring is connected with chuck, and lower T-Ring is connected with jacket head; T-Ring is provided with gas vent on described.
Between the shaft of described agitator and cover, be provided with mechanical sealing member.
Be provided with journal stirrup at described chuck.
The utility model is following advantage compared with prior art:
(1) the utility model can be under high temperature, lower negative pressure operating mode long-term operation and do not shell, not bulge, do not tear;
(2) the utility model is high pressure resistant: extreme design pressure≤2.5MPa;
(3) the anti-lower negative pressure of the utility model: minimum design pressure is-0.03MPa;
(4) the utility model is high temperature resistant: design temperature≤150 ℃;
(5) the utility model is low temperature resistant: minimum design temperature<-40 ℃;
(6) the utility model non-stick pan, non-scaling have been stablized manufacturing schedule, have guaranteed high-purity feed purity, are particularly useful for pharmaceutical industry, are better than glass-lined reactor;
(7) the utility model is under high temperature, lower negative pressure operating mode, and tetrafluoro plate lining can be resisted all chemical mediator corrosion of nature, is better than glass-lined reactor;
(8) the utility model low cost of manufacture, than ward off F40, roll F40, the product market price of spray F40 lining, cheap about 1/2nd;
(9) tetrafluoro plate lining of the present utility model is never aging, and long service life is that ten times of glass-lined reactors are more than the life-span;
(10) the utility model has overcome glass-lined reactor easy burst porcelain, the easy weakness of fouling, and the trouble of avoiding the user often to stop production, change tank, scrap one pot of material has improved productivity ratio, has saved the energy;
(11) this negative pressure resistant tetrafluoro plate lining retort as claimed in claim 1 is characterized in that: described utility model in addition parts all adopts the manufacturing of current stress container relevant criterion.
Description of drawings
Fig. 1 is structural representation of the present utility model.
Fig. 2 is the I enlarged drawing of Fig. 1.
Fig. 3 is the top view of Fig. 1.
Fig. 4 is the structural representation in the mouth of pipe tetrafluoro material of the present utility model.
The specific embodiment
The utility model is described in further detail below in conjunction with concrete accompanying drawing.
Such as Fig. 1~shown in Figure 4: the tetrafluoro of anti-lower negative pressure lining retort comprises jacket head 1, at the bottom of the tank 2, tank body 3, chuck 4, journal stirrup 5, heating agent entrance sleeve 6, the first pressure container flange 7, sealing gasket 8, studs 9, the second pressure container flange 10, manhole 11, agitator 12, mechanical sealing member 13, reductor 14, reductor support 15, temperature-measuring port 16, cover 17, upper T-Ring 18, heating agent discharge connection 19, condensate drain outlet 20, drain hole 21, lower T-Ring 22, tetrafluoro backing layer 23, adhesive layer 24, visor hole 25, lamp hole 26, gas vent 27, the effective flange 28 of pressure vessel etc.
As shown in Figure 1, the utility model comprise at the bottom of tank body 3, the tank 2 with cover 17,2 are welded at the bottom of tank body 3 and the tank, the first pressure container flange 7 is welded in the upper end of tank body 3, the second pressure container flange 10 is welded in the lower end of cover 17, and tank body 3 is connected by the first pressure container flange 7, the second pressure container flange 10 and studs 9 connections fastening with cover; At described tank body 3 interior installation agitators 12, the shaft of agitator 12 stretches out cover 17 outsides by mechanical seal, and be connected with the output shaft of the reductor 14 that is arranged on cover 17 tops, the stirring reaction of various chemical materials in retort all is to rely on the rotation of agitator 12 to finish, and agitator 12 rotations are driven by reductor 14; 2 outsides are provided with to heat or cool off the jacket body of chemical substance in the retort at the bottom of described tank body 3 and tank, exist between 2 at the bottom of jacket body and tank body 3 and the tank and add cold or the cooling cavity, the jacket head 1 in 2 outsides at the bottom of described jacket body comprises the chuck 4 that is located at tank body 3 outsides and is located at tank, be provided with condensate drain outlet 20 at jacket head 1, be provided with heating agent entrance sleeve 6 and the heating agent discharge connection 19 that is communicated with the jacket body internal cavity at chuck 4, be equipped with impingement baffle on the opposite of heating agent entrance sleeve 6 and heating agent discharge connection 19; 2 bottom is provided with drain hole 21 at the bottom of described tank, is provided with a plurality of mouths of pipe at described cover 17, and the mouth of pipe comprises manhole 11, axis hole, charge door, temperature-measuring port 16, relief valve port, mouth for subsequent use, visor hole 25 and lamp hole 26; The described mouth of pipe all arranges the effective flange 28 of pressure vessel;
Such as Fig. 2, shown in Figure 4,2 inner wall surface is by adhesive layer 24 bonding tetrafluoro backing layers 23 at the bottom of described tank body 3, cover 17 and tank, 2 inner wall surface close adhesion at the bottom of tetrafluoro backing layer 23 and tank body 3, cover 17 and the tank, there is not vacuum layer, through test adhesive under 200 ℃ of high temperature, peel strength>0.35MPa; The thickness of described tetrafluoro backing layer 23 is 2~4mm;
As shown in Figure 2, in order to prevent the leakage of material, between described the first pressure container flange 7 and the second pressure container flange 10 sealing gasket 8 is set and seals, sealing pad 8 adopts polytetrafluoroethylene (PTFE) to coat asbestos pad;
As shown in Figure 1, be welded with T-Ring 18 at described tank body 3,2 lower end is welded with lower T-Ring 22 at the bottom of tank, upper T-Ring 18 and chuck 4 welding, and lower T-Ring 22 and jacket head 1 welding, T-Ring 18 is provided with gas vent 27 on described; Described upper T-Ring 18 and lower T-Ring 22 are the arts demands for lining tetrafluoro backing layer, and before lining tetrafluoro backing layer, upper T-Ring 18 and lower T-Ring 22 are welded on first at the bottom of tank body 3 and the tank on 2, served as a contrast the cooling of tetrafluoro backing layer after, the assembly welding jacket body is installed again;
As shown in Figure 1, between the shaft of described agitator 12 and cover 17, be provided with mechanical sealing member 13;
As shown in Figure 1, described reductor 14 is installed in the top of cover 17 by reductor support 15;
As shown in Figure 1, be provided with four journal stirrups 5 at described chuck 4, journal stirrup 5 usefulness whats are fixed on floor or the support, to carry the weight of whole retort.
Retort described in the utility model mainly by at the bottom of cover 17, tank body 3, the tank 2, jacket body and agitator 12 form, cover 17 is provided with each mouth of pipe (manhole 11, charge door, temperature-measuring port 16, relief valve port, for subsequent use mouthful, visor hole 25 and lamp hole 26).Cover 17 and tank body 3 adopts the first pressure container flange 7 and is connected pressure container flange 10 and is connected fasteningly, and securing member is studs 9; Simultaneously, each mouth of pipe on the cover 17 all connects with the effective flange of pressure vessel, makes retort high pressure resistant, and extreme design pressure is 2.5MPa;
The utility model parts made in one piece all adopt current stress container relevant criterion.
The utility model is on product structure, for anti-lower negative pressure, tetrafluoro backing layer and retort inwall close adhesion, there is not vacuum interlayer, be bonded under 200 ℃ of test temperatures tensile strength greater than 0.35MPa through test tetrafluoro backing layer 23 and steel plate, the interior negative pressure of the tank that is enough to contend with has guaranteed long-term operation under the retort.Steady production technique has improved enterprise production.The utility model under high temperature, high pressure conditions, makes tetrafluoro backing layer 23 closely be bonded in fully on the tank skin by adhesive layer 24 because the tetrafluoro backing layer 23 on the retort inwall adopts special technique with the retort inwall, does not have vacuum interlayer.
The utility model has been cancelled a pair of main flange of conventional retort bottom on the market, only keeps a pair of main flange on a pair of cover and the can body, has kept original heating (cooling) space of chuck.

Claims (10)

1. the tetrafluoro of anti-lower negative pressure lining retort comprises (2) and cover (17) at the bottom of tank body (3), the tank, and (2) are welded at the bottom of tank body (3) and the tank, installation agitator (12) in tank body (3); (2) outside is provided with jacket body at the bottom of described tank body (3) and tank, has cavity between (2) at the bottom of jacket body and tank body (3) and the tank; The bottom of (2) is provided with drain hole (21) at the bottom of described tank, is provided with a plurality of mouths of pipe at described cover (17); It is characterized in that: the inner wall surface of (2) is passed through the bonding tetrafluoro backing layer of adhesive layer (24) (23) at the bottom of described tank body (3), cover (17) and tank, the inner wall surface close adhesion of (2) at the bottom of tetrafluoro backing layer (23) and tank body (3), cover (17) and the tank; Weld the first pressure container flange (7) in the upper end of described tank body (3), the second pressure container flange (10) is welded in the lower end of cover (17), and tank body (3) is connected 17 with cover) connect fastening by the first pressure container flange (7), the second pressure container flange (10) and studs (9); The described mouth of pipe all arranges the effective flange of the effective pressure vessel of pressure vessel (28).
2. the tetrafluoro of anti-lower negative pressure lining retort as claimed in claim 1, it is characterized in that: the jacket head (1) in (2) outside at the bottom of described jacket body comprises the chuck (4) that is located at tank body (3) outside and is located at tank, be provided with condensate drain outlet (20) at jacket head (1), be provided with heating agent entrance sleeve (6) and the heating agent discharge connection (19) that is communicated with the jacket body internal cavity at chuck (4).
3. the tetrafluoro of anti-lower negative pressure lining retort as claimed in claim 1 is characterized in that: the mouth of pipe on the described cover (17) comprises manhole (11), charge door, temperature-measuring port (16), relief valve port, for subsequent use mouthful, visor hole (25) and lamp hole (26).
4. the tetrafluoro of anti-lower negative pressure lining retort as claimed in claim 1 is characterized in that: the shaft of described agitator (12) stretches out cover (17) outside, and is connected with the output shaft of the reductor (14) that is arranged on cover (17) top.
5. the tetrafluoro of anti-lower negative pressure lining retort as claimed in claim 4 is characterized in that: described reductor (14) is installed in the top of cover (17) by reductor support (15).
6. the tetrafluoro of anti-lower negative pressure lining retort as claimed in claim 1 is characterized in that: the thickness of described tetrafluoro backing layer (23) is 2~4mm.
7. the tetrafluoro of anti-lower negative pressure lining retort as claimed in claim 1 is characterized in that: between described the first pressure container flange (7) and the second pressure container flange (10) sealing gasket (8) is set.
8. the tetrafluoro of anti-lower negative pressure lining retort as claimed in claim 2, it is characterized in that: be connected with upper T-Ring (18) at described tank body (3), the lower end of (2) is connected with lower T-Ring (22) at the bottom of tank, upper T-Ring (18) is connected with chuck (4), and lower T-Ring (22) is connected with jacket head (1); T-Ring (18) is provided with gas vent (27) on described.
9. the tetrafluoro of anti-lower negative pressure lining retort as claimed in claim 1 is characterized in that: be provided with mechanical sealing member (13) between the shaft of described agitator (12) and cover (17).
10. the tetrafluoro of anti-lower negative pressure lining retort as claimed in claim 2 is characterized in that: be provided with journal stirrup (5) at described chuck (4).
CN 201220334031 2012-07-10 2012-07-10 Low-negative-pressure-resistant teflon lining reaction tank Expired - Fee Related CN202778458U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220334031 CN202778458U (en) 2012-07-10 2012-07-10 Low-negative-pressure-resistant teflon lining reaction tank

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201220334031 CN202778458U (en) 2012-07-10 2012-07-10 Low-negative-pressure-resistant teflon lining reaction tank

Publications (1)

Publication Number Publication Date
CN202778458U true CN202778458U (en) 2013-03-13

Family

ID=47805803

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201220334031 Expired - Fee Related CN202778458U (en) 2012-07-10 2012-07-10 Low-negative-pressure-resistant teflon lining reaction tank

Country Status (1)

Country Link
CN (1) CN202778458U (en)

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
EE01 Entry into force of recordation of patent licensing contract

Assignee: Wuxi Huanyu Equipment Technology Co., Ltd.

Assignor: Zhang Yayu|Hu Yongqing

Contract record no.: 2014320010143

Denomination of utility model: Low-negative-pressure-resistant teflon lining reaction tank

Granted publication date: 20130313

License type: Exclusive License

Record date: 20140716

LICC Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130313

Termination date: 20150710

EXPY Termination of patent right or utility model