CN202778457U - High-negative-pressure-resistant teflon lining reaction tank - Google Patents

High-negative-pressure-resistant teflon lining reaction tank Download PDF

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Publication number
CN202778457U
CN202778457U CN 201220332450 CN201220332450U CN202778457U CN 202778457 U CN202778457 U CN 202778457U CN 201220332450 CN201220332450 CN 201220332450 CN 201220332450 U CN201220332450 U CN 201220332450U CN 202778457 U CN202778457 U CN 202778457U
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China
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tank
cover
tank body
negative pressure
tetrafluoro
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Expired - Fee Related
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CN 201220332450
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Chinese (zh)
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胡永庆
贾建新
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  • Pressure Vessels And Lids Thereof (AREA)

Abstract

The utility model relates to a high-negative-pressure-resistant teflon lining reaction tank which comprises a tank body, a tank bottom and a tank lid, wherein the outer sides of the tank body and the tank bottom are provided with a jacket body, and a cavity is formed among the jacket body, the tank body and the tank bottom; the bottom of the tank bottom is provided with a discharge outlet, and the tank lid is provided with a plurality of pipe orifices; the internal surfaces of the tank body, the tank lid, the tank bottom and the pipe orifices are provided with a plurality of round steel bars protruded out of the inner wall surfaces of the tank body, the tank lid and the tank bottom; and the tank is characterized in that a teflon lining layer is adhered to the internal surfaces of the tank body, the tank lid, the tank bottom and the pipe orifices through an adhering layer; the upper end of the tank body is connected with a first pressure vessel flange, the lower end of the tank lid is connected with a second pressure vessel flange, and the tank body and the tank lid are connected and fastened through the first pressure vessel flange, the second pressure vessel flange and a double-headed stud. The tank disclosed by the utility model can be running for a long time under high-temperature and high-negative-pressure working conditions and no shelling, swelling and tearing occur.

Description

Negative pressure resistant tetrafluoro lining retort
Technical field
The utility model relates to a kind of negative pressure resistant tetrafluoro lining retort, especially a kind of retort of finishing the processes such as the reaction of material, synthetic, polymerization, chlorination for chemical industry, pharmaceutical engineering, and the negative pressure of minimum ability is-0.09MPa.
Background technology
In existing technology, retort lining tetrafluoro is because of the technical barrier such as can't process the bulge of tetrafluoro plate lining, shell, tear, and causes tetrafluoro plate lining to lose efficacy under high temperature and high pressure condition.For the arts demand of empty set lining, usually adopt two flange arrangements, namely cover is with tank body, tank body and respectively be connected fastening with a pair of main flange at the bottom of the tank.Heating jacket has to be divided into up and down two parts, below a pair of main flange be exposed, reduced chuck length, reduce the heating surface (area) (HS of chuck, simultaneously, be connected to a pair of flange in lower end of retort and numerous double-screw bolt and nuts, be heated simultaneously, waste heat, wasted heat energy, limited the intensification of retort, the normal function of heating.
In existing technology, at the inwall of retort, match by its internal diameter size, make the tetrafluoro inner sleeve, empty set is in tank, and the space that exists 1~3mm not wait between tank skin and the lining has formed the natural air interlayer.The sealing surface of retort master's flange and each mouth of pipe is not made adhesion process with the flange flange of tetrafluoro lining yet.Can't form Sealed sandwich between cover and can body and the tetrafluoro lining, the interlayer Air is in free state forever.When retort under high temperature, lower negative pressure operating mode, the every intensity index of PTFE sharply descends.The air of interlayer is heated suddenly and expands, lining has been produced external pressure has been subjected to again lower negative pressure effect in the tank simultaneously, the tetrafluoro lining under the dual-pressure effect, unstability and produce shelling, tear or deformation of cylindrical.
In existing technology, also have on above-mentioned empty set basis, added adhesive, very smooth smooth on the surface, but producer offers some clarification on not ability negative pressure, and can not be high temperature resistant; Having added wire netting also can only anti-little negative pressure, 110~120 ℃ of operating temperatures, but still be two flange arrangements.
In order to solve the dual pressurized problem of lining, once the remedial measure that adopted aborning is, adopt vacuum line with tetrafluoro lining interlayer and the retort tank body tetrafluoro lining interlayer pipeline connection of retort cover, vavuum pump is communicated with vacuum line, vavuum pump and retort vacuum system start synchronously, close synchronously makes the interlayer place what vacuum state of tetrafluoro lining and tank skin, with the negative pressure in the tank that contends with.Although on reason, as if solved the vacuum equalization problem, but ignored the impact of the linear expansion stress of PTFE deadweight under the high temperature, boundary stress that the agitator rotation produces, PTFE, under these composite factor effects, tetrafluoro lining or deformation of cylindrical.Therefore, can't solve the at high temperature problem of anti-negative pressure of steel lining tetrafluoro retort.
Summary of the invention
The purpose of this utility model is to overcome the deficiencies in the prior art, and a kind of negative pressure resistant tetrafluoro lining retort is provided, can be under high temperature, high negative pressure long-term operation and do not shell, not bulge, the tetrafluoro lining retort product do not torn.
According to the technical scheme that the utility model provides, a kind of negative pressure resistant tetrafluoro lining retort comprises at the bottom of tank body, the tank and cover, and tank body and tank back welding connect and form, and in described tank body agitator are installed; The outside is provided with jacket body at the bottom of described tank body and tank, has cavity between at the bottom of jacket body and tank body and the tank; Bottom at the bottom of described tank is provided with drain hole, is provided with a plurality of mouths of pipe at described cover; Inner wall surface at described tank body, End Pieces is provided with some round steel that protrude from the inner wall surface of tank body, End Pieces, and the inner wall surface of the mouth of pipe on described cover is provided with the round steel that protrudes from the internal wall of pipe orifice surface; Feature is: at the bottom of described tank body, cover, tank and the inner wall surface of the mouth of pipe by the bonding tetrafluoro backing layer of adhesive layer, the tetrafluoro backing layer coats round steel; The inner wall surface close adhesion of described tetrafluoro backing layer and tank body, End Pieces; Connect the first pressure container flange in the upper end of described tank body, the lower end of cover connects the second pressure container flange, and tank body is connected the first pressure container flange, the second pressure container flange and studs and connects fastening with cover; The described mouth of pipe all arranges the effective flange of pressure vessel.
Described round steel is circular, is welded at the bottom of tank body, cover, the tank and the inner wall surface of the mouth of pipe.
The thickness of described tetrafluoro backing layer is 2~4mm.
Between described the first pressure container flange and the second pressure container flange, sealing gasket is set.
Be welded with T-Ring at described tank body, the lower end at the bottom of tank is welded with lower T-Ring, and upper T-Ring is connected with chuck, and lower T-Ring is connected with jacket head, and T-Ring is provided with gas vent on described.
Between the shaft of described agitator and cover, be provided with mechanical sealing member.
The shaft of described agitator stretches out the cover outside, and is connected with the output shaft of the reductor that is arranged on the cover top.Described reductor is installed in the top of cover by the reductor support.
Described jacket body comprises the chuck that is located at the tank body outside and is located at the basolateral jacket head of tank, is provided with condensate drain outlet at jacket head, is provided with heating agent entrance sleeve and the heating agent discharge connection that is communicated with the jacket body internal cavity at chuck.Be provided with journal stirrup at described chuck.
The utility model is following advantage compared with prior art:
(1) the utility model can be under high temperature, high negative pressure operating mode long-term operation and do not shell, not bulge, do not tear;
(2) the utility model is high pressure resistant: extreme design pressure≤2.5MPa;
(3) the utility model negative pressure resistant: minimum design pressure is-0.09MPa;
(4) the utility model is high temperature resistant: design temperature≤180 ℃;
(5) the utility model is low temperature resistant: minimum design temperature<-40 ℃;
(6) the utility model non-stick pan, non-scaling have been stablized manufacturing schedule, have guaranteed high-purity feed purity, are particularly useful for pharmaceutical industry, are better than glass-lined reactor;
(7) the utility model is under high temperature, high negative pressure operating mode, and the tetrafluoro lining can be resisted all chemical mediator corrosion of nature, is better than glass-lined reactor;
(8) the utility model low cost of manufacture, than ward off F40, roll F40, the product market price of spray F40 lining, cheap about 1/3rd;
(9) the utility model tetrafluoro lining is never aging, and long service life is that glass-lined reactor is more than ten times;
(10) the utility model has overcome glass-lined reactor easy burst porcelain, the easy weakness of fouling, and the trouble of avoiding the user often to stop production, change tank, scrap one pot of material has improved productivity ratio, has saved the energy;
(11) the utility model adopts a pair of pressure vessel special flange, allows working pressure to reach as high as 2.5MPa.
Description of drawings
Fig. 1 is structural representation of the present utility model.
Fig. 2 is the I enlarged drawing of Fig. 1.
Fig. 3 is tank body expanded view described in the utility model.
Fig. 4 is the A-A cutaway view of Fig. 3.
Fig. 5 is the top view of Fig. 1.
Fig. 6 is the structure chart in the mouth of pipe tetrafluoro material described in the utility model.
The specific embodiment
The utility model is described in further detail below in conjunction with concrete accompanying drawing.
Such as Fig. 1~shown in Figure 6: negative pressure resistant tetrafluoro lining retort comprises jacket head 1, at the bottom of the tank 2, tank body 3, chuck 4, journal stirrup 5, heating agent entrance sleeve 6, the first pressure container flange 7, sealing gasket 8, studs 9, the second pressure container flange 10, manhole 11, agitator 12, mechanical sealing member 13, reductor 14, reductor support 15, temperature-measuring port 16, cover 17, upper T-Ring 18, heating agent discharge connection 19, condensate drain outlet 20, drain hole 21, lower T-Ring 22, tetrafluoro backing layer 23, adhesive layer 24, round steel 25, the effective flange 26 of pressure vessel, visor hole 28, lamp hole 29, gas vent 30 etc.
As shown in Figure 1, the utility model comprise at the bottom of tank body 3, the tank 2 with cover 17,2 are welded at the bottom of tank body 3 and the tank, the first pressure container flange 7 is welded in the upper end of tank body 3, the second pressure container flange 10 is welded in the lower end of cover 17, and tank body 3 is connected by the first pressure container flange 7, the second pressure container flange 10 and studs 9 connections fastening with cover; At described tank body 3 interior installation agitators 12, the shaft of agitator 12 stretches out cover 17 outsides, and be connected with the output shaft of the reductor 14 that is arranged on cover 17 tops, the stirring reaction of various chemical materials in retort all is to rely on the rotation of agitator 12 to finish, and agitator 12 rotations are driven by reductor 14; 2 outsides are provided with to heat or cool off the jacket body of chemical substance in the retort at the bottom of described tank body 3 and tank, there is cavity between 2 at the bottom of jacket body and tank body 3 and the tank, the jacket head 1 in 2 outsides at the bottom of described jacket body comprises the chuck 4 that is located at tank body 3 outsides and is located at tank, be provided with condensate drain outlet 20 at jacket head 1, be provided with heating agent entrance sleeve 6 and the heating agent discharge connection 19 that is communicated with the jacket body internal cavity at chuck 4, be equipped with impingement baffle on the opposite of heating agent entrance sleeve 6 and heating agent discharge connection 19; 2 bottom is provided with drain hole 21 at the bottom of described tank, is provided with a plurality of mouths of pipe at described cover 17, and the mouth of pipe comprises manhole 11, charge door, temperature-measuring port 16, relief valve port, mouth for subsequent use, visor hole 28 and lamp hole 29; The described mouth of pipe all arranges the effective flange 26 of pressure vessel;
Such as Fig. 2, Fig. 3, shown in Figure 4,2 inner wall surface at the bottom of described tank body 3, cover 17 and the tank be provided with some protrude from tank body 3, cover 17 and tank at the bottom of the round steel 25 of 2 inner wall surface, this round steel 25 is circular, is welded at the bottom of tank body 3, cover 17 and the tank 2 inner wall surface; 2 inner wall surface is by adhesive layer 24 bonding tetrafluoro backing layers 23 at the bottom of described tank body 3, cover 17 and tank, and tetrafluoro backing layer 23 coats round steel 25; There is not vacuum layer in 2 inner wall surface close adhesion at the bottom of described tetrafluoro backing layer 23 and tank body 3, cover 17 and the tank; The thickness of described tetrafluoro backing layer 23 is 2~4mm;
As shown in Figure 6, the inner wall surface of the mouth of pipe on described cover 17 also is provided with the round steel 25 that protrudes from the internal wall of pipe orifice surface; Inner wall surface at the described mouth of pipe is passed through adhesive layer 24 bonding tetrafluoro backing layers 23, and tetrafluoro backing layer 23 coats round steel 25; There is not vacuum layer in the inner wall surface close adhesion of described tetrafluoro backing layer 23 and the mouth of pipe; The thickness of described tetrafluoro backing layer 23 is 2~4mm;
As shown in Figure 2, in order to prevent the leakage of material, between described the first pressure container flange 7 and the second pressure container flange 10 sealing gasket 8 is set and seals, sealing pad 8 adopts polytetrafluoroethylene (PTFE) to coat the asbestos rubber pad;
As shown in Figure 1, be welded with T-Ring 18 at described tank body 3,2 lower end is welded with lower T-Ring 22 at the bottom of tank, and upper T-Ring 8 is connected with chuck 4, and lower T-Ring 18 is connected with jacket head 1, and T-Ring 8 is provided with gas vent 30 on described; Described upper T-Ring 8 and lower T-Ring 18 are the arts demands for lining tetrafluoro backing layer, and before lining tetrafluoro backing layer, upper T-Ring 8 and lower T-Ring 18 are welded on first at the bottom of tank body 3 and the tank on 2, served as a contrast the cooling of tetrafluoro backing layer after, mounting clamp body again;
As shown in Figure 1, between the shaft of described agitator 12 and cover 17, be provided with mechanical sealing member 13;
As shown in Figure 1, described reductor 14 is installed in the top of cover 17 by reductor support 15;
As shown in Figure 1, be provided with four journal stirrups 5 at described chuck 4, journal stirrup 5 usefulness whats are fixed on floor or the support, to carry the weight of whole retort.
Retort described in the utility model mainly by at the bottom of cover 17, tank body 3, the tank 2, jacket body and agitator 12 form, cover 17 is provided with each mouth of pipe (manhole 11, charge door, temperature-measuring port 16, relief valve port, for subsequent use mouthful, visor hole 28 and lamp hole 29).Cover 17 and tank body 3 adopts the first pressure container flange 7 and is connected pressure container flange 10 and is connected fasteningly, and securing member is studs 9; Simultaneously, each mouth of pipe on the cover 17 all connects with pressure container flange, makes retort high pressure resistant, and extreme design pressure is 2.5MPa;
The whole manufacturing of the utility model all adopted the manufacturing of current stress container relevant criterion with parts.
The utility model is on product structure, for negative pressure resistant, tetrafluoro lining and tank skin close adhesion, there is not vacuum interlayer, through the bonding tensile strength of test tetrafluoro backing layer 23 and steel plate under 200 ℃ of test temperatures greater than 0.35MPa, the interior negative pressure of the tank that is enough to contend with has guaranteed long-term operation under the retort; And steady production technique has improved enterprise production.
The line swelling stress that at high temperature produces in order to solve PTFE, the utility model has been welded with several annulus unit steel 25 at the inner wall surface point of can body and cover, with tetrafluoro liner plate layer 23, the large-area swelling stress that at high temperature produces is decomposed and carrying by several roundlet ring element steel 25, large-area swelling stress dissolved be the small size swelling stress, avoided the tetrafluoro liner plate layer 23 on the can body with cover on tetrafluoro liner plate layer 23 produce the large tracts of land relative displacements; Avoid lining tetrafluoro flaggy at high temperature to produce bulge, shelled, torn phenomenon.The utility model is owing to be welded with several annulus unit steel 25 at tank inwall point, tetrafluoro backing layer 23 adopts special technique with the retort inwall, under high temperature, high pressure conditions, tetrafluoro liner plate layer 23 closely is bonded on the tank skin fully by adhesive layer 24, there is not vacuum interlayer.
The utility model has been cancelled a pair of main flange of conventional retort bottom on the market, only keeps a pair of main flange on a pair of cover and the can body, has kept original heating (cooling) space of chuck.

Claims (10)

1. negative pressure resistant tetrafluoro lining retort comprises (2) and cover (17) at the bottom of tank body (3), the tank, and (2) are welded at the bottom of tank body (3) and the tank, installation agitator (12) in described tank body (3); (2) outside is provided with jacket body at the bottom of described tank body (3) and tank, has cavity between (2) at the bottom of jacket body and tank body (3) and the tank; The bottom of (2) is provided with drain hole (21) at the bottom of described tank, is provided with a plurality of mouths of pipe at described cover (17); The inner wall surface of (2) at the bottom of described tank body (3), cover (17) and the tank be provided with some protrude from tank body (3), cover (17) and tank at the bottom of the round steel (25) of inner wall surface of (2), the inner wall surface of the mouth of pipe on described cover (17) is provided with the round steel (25) that protrudes from the internal wall of pipe orifice surface; It is characterized in that: the inner wall surface of (2) and the mouth of pipe is by the bonding tetrafluoro backing layer of adhesive layer (24) (23) at the bottom of described tank body (3), cover (17), tank, and tetrafluoro backing layer (23) coats round steel (25); The inner wall surface close adhesion of (2) at the bottom of described tetrafluoro backing layer (23) and tank body (3), cover (17) and the tank; Connect the first pressure container flange (7) in the upper end of described tank body (3), the lower end of cover (17) connects the second pressure container flange (10), and tank body (3) is connected 17 with cover) connect fastening by the first pressure container flange (7), the second pressure container flange (10) and studs (9); The described mouth of pipe all arranges the effective flange of pressure vessel (26).
2. negative pressure resistant tetrafluoro lining retort as claimed in claim 1 is characterized in that: described round steel (25) is for circular, is welded to the inner wall surface of (2) and the mouth of pipe at the bottom of tank body (3), cover (17), the tank.
3. negative pressure resistant tetrafluoro lining retort as claimed in claim 1, it is characterized in that: the thickness of described tetrafluoro backing layer (23) is 2~4mm.
4. negative pressure resistant tetrafluoro lining retort as claimed in claim 1 is characterized in that: between described the first pressure container flange (7) and the second pressure container flange (10) sealing gasket (8) is set.
5. negative pressure resistant tetrafluoro lining retort as claimed in claim 1, it is characterized in that: be welded with upper T-Ring (18) at described tank body (3), the lower end of (2) is welded with lower T-Ring (22) at the bottom of tank, upper T-Ring (8) is connected with chuck (4), lower T-Ring (18) is connected with jacket head (1), and T-Ring (8) is provided with gas vent (30) on described.
6. negative pressure resistant tetrafluoro lining retort as claimed in claim 1 is characterized in that: be provided with mechanical sealing member (13) between the shaft of described agitator (12) and cover (17).
7. negative pressure resistant tetrafluoro lining retort as claimed in claim 1 is characterized in that: the shaft of described agitator (12) stretches out cover (17) outside, and is connected with the output shaft of the reductor (14) that is arranged on cover (17) top.
8. negative pressure resistant tetrafluoro lining retort as claimed in claim 7, it is characterized in that: described reductor (14) is installed in the top of cover (17) by reductor support (15).
9. negative pressure resistant tetrafluoro lining retort as claimed in claim 1, it is characterized in that: the jacket head (1) in (2) outside at the bottom of described jacket body comprises the chuck (4) that is located at tank body (3) outside and is located at tank, be provided with condensate drain outlet (20) at jacket head (1), be provided with heating agent entrance sleeve (6) and the heating agent discharge connection (19) that is communicated with the jacket body internal cavity at chuck (4).
10. negative pressure resistant tetrafluoro lining retort as claimed in claim 9 is characterized in that: be provided with journal stirrup (5) at described chuck (4).
CN 201220332450 2012-07-10 2012-07-10 High-negative-pressure-resistant teflon lining reaction tank Expired - Fee Related CN202778457U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220332450 CN202778457U (en) 2012-07-10 2012-07-10 High-negative-pressure-resistant teflon lining reaction tank

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201220332450 CN202778457U (en) 2012-07-10 2012-07-10 High-negative-pressure-resistant teflon lining reaction tank

Publications (1)

Publication Number Publication Date
CN202778457U true CN202778457U (en) 2013-03-13

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113062980A (en) * 2021-05-11 2021-07-02 齐泽民 PTFE lining pressure container and manufacturing method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113062980A (en) * 2021-05-11 2021-07-02 齐泽民 PTFE lining pressure container and manufacturing method thereof
CN113062980B (en) * 2021-05-11 2022-04-22 齐泽民 PTFE lining pressure container and manufacturing method thereof

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
EE01 Entry into force of recordation of patent licensing contract

Assignee: Wuxi Huanyu Equipment Technology Co., Ltd.

Assignor: Zhang Yayu|Hu Yongqing

Contract record no.: 2014320010143

Denomination of utility model: High-negative-pressure-resistant teflon lining reaction tank

Granted publication date: 20130313

License type: Exclusive License

Record date: 20140716

LICC Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130313

Termination date: 20150710

EXPY Termination of patent right or utility model