CN202478646U - Device for extracting active ingredients in dried gingers by adopting subcritical water extraction method - Google Patents
Device for extracting active ingredients in dried gingers by adopting subcritical water extraction method Download PDFInfo
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- CN202478646U CN202478646U CN2012200333487U CN201220033348U CN202478646U CN 202478646 U CN202478646 U CN 202478646U CN 2012200333487 U CN2012200333487 U CN 2012200333487U CN 201220033348 U CN201220033348 U CN 201220033348U CN 202478646 U CN202478646 U CN 202478646U
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- extraction
- extractor
- subcritical water
- filter
- water extraction
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- 238000000034 method Methods 0.000 title claims abstract description 27
- 238000003809 water extraction Methods 0.000 title claims abstract description 8
- 239000004480 active ingredient Substances 0.000 title claims abstract description 7
- 241000234314 Zingiber Species 0.000 title abstract description 5
- 235000006886 Zingiber officinale Nutrition 0.000 title abstract description 5
- 235000008397 ginger Nutrition 0.000 title abstract description 5
- 238000000605 extraction Methods 0.000 claims abstract description 27
- 239000000284 extract Substances 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 12
- 230000007613 environmental effect Effects 0.000 abstract description 4
- 239000003960 organic solvent Substances 0.000 abstract description 4
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 235000020708 ginger extract Nutrition 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 5
- 239000007788 liquid Substances 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 239000003818 cinder Substances 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000003801 milling Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000001256 steam distillation Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
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- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The utility model provides a device for extracting active ingredients in dried gingers by adopting a subcritical water extraction method, and relates to the technical field of extraction devices. The device is characterized in that a grinder (1) is connected with a filter device (2); the filter device (2) and a high pressure pump (3) are connected with an extraction tank (4); steam cycle devices (5) are arranged on the outer walls of the extraction tank (4); the lower end of the extraction tank (4) is connected with an extracting solution container (9) by virtue of a discharge valve (8); and the extracting solution container (9) is connected with a water division device (10). The device has the following beneficial effects: the device breaks through the traditional extraction concepts and methods of dried ginger extraction, applies subcritical water extraction to dried ginger extracts for the first time, dispenses with organic solvents in the whole process, has the obvious advantages of advanced science, clean process, environmental friendliness, high extraction speed, high efficiency and simple process and can meet the requirement of large industrial production.
Description
Technical field:
The utility model relates to the extraction equipment technical field, is specifically related to a kind of device that adopts active ingredient among the subcritical water extraction method extraction Jiang Gan.
Background technology:
The main method of extracting Ginger P.E at present has steam distillation, solvent method, milling process and supercritical extraction.
The steam distillation leaching process time is long, temperature is high, open system, and its process causes destruction and the volatilization loss that is prone to cause thermally labile and is prone to oxidizing component, and the part component is had destruction.
The product that solvent method extracts has solvent residual amount easily, and causes the product taste impure.
The milling process complicated operation, oil yield is low, and product volume remaining in the squeezing material later is too much, is not suitable for industry and promotes.
Supercritical CO
2The extraction extraction process is relatively short, temperature is low, extraction system is airtight, oil-collecting ratio improves greatly; In extraction process, got rid of the possibility that some chemical compositions are met the oxygen oxidation and seen light reaction; Can extract lower boiling effumability composition; Avoid destroying having the qualities of plants flavor component, also can extract unstable components such as serial alkane, organic acid and long-chain fat hydrocarbon.But in large-scale production process, extraction time is still long relatively, and the CO that uses
2In removal process, cause recovery not thorough easily, discharge into the atmosphere, cause greenhouse effects.
The utility model content:
The purpose of the utility model provides a kind of device that adopts active ingredient among the subcritical water extraction method extraction Jiang Gan, and it has broken traditional extraction idea and method to the extraction of rhizoma zingiberis, subcritical water is extracted be applied to Rhizoma Zingiberis extract first; Whole process does not need organic solvent; Have that section emulates the advanced, process cleaning, environmental friendliness, extraction rate is fast, efficient is high; The simple remarkable advantage of technology, and can satisfy the needs of industrialized production.
In order to solve the existing problem of background technology; The utility model is to adopt following technical scheme: it comprises pulverizer 1, filter 2, high-pressure pump 3, extractor 4, vapor recycle device 5, dispensing valve 8, extract container 9 and division box 10; Pulverizer 1 is connected with filter 2; Filter 2 all is connected with extractor 4 with high-pressure pump 3; Extractor 4 outer walls are provided with vapor recycle device 5, and the lower end of extractor 4 is connected with extract container 9 through dispensing valve 8, and extract container 9 is connected with division box 10.
Described extractor 4 inside bottom are provided with filter 7, filter 7 tops be provided with external communications get cinder notch 6.
Described filter 2 inside are 20 mesh sieves.
The course of work of the utility model is: the washing dried ginger slice through pulverizer 1 is good with airing is pulverized, and crosses 20 mesh sieves.Crushing rear material is packed in the extractor 4, and solid-liquid ratio is 1: 1～1: 3, and is ready to preheating water; Through high-pressure pump 3 preheating water is pumped in the extractor 4, and pressure is risen to 20～25Mpa, open vapor recycle device 5, with the adjustment to 120 of extractor 4 ℃～150 ℃.This moment, extractor 4 interior water were in subcritical state, pressurize 10～15min.Steam off EGR 5 is opened extractor 4 lower end dispensing valves 8, and the extract that contains Ginger P.E of the extractor 4 inner high voltages filter 7 through extractor 4 bottoms is expelled in the container rapidly.After highly pressurised liquid in the extractor 4 is disposed to normal pressure, draw off the rhizoma zingiberis residue.Extract in the container is cooled to room temperature, uses division box 10 to remove the water in the extract, surplus products are Ginger P.E.
The utility model has been broken traditional extraction idea and method to the extraction of rhizoma zingiberis; First subcritical water is extracted and be applied to Rhizoma Zingiberis extract, whole process does not need organic solvent, has that section emulates the advanced, a process cleaning, environmental friendliness; Extraction rate is fast; Efficient is high, the simple remarkable advantage of technology, and can satisfy the needs of industrialized production.
Description of drawings:
Fig. 1 is the structural representation of the utility model.
The specific embodiment:
With reference to Fig. 1; This specific embodiment adopts following technical scheme: it comprises pulverizer 1, filter 2, high-pressure pump 3, extractor 4, vapor recycle device 5, dispensing valve 8, extract container 9 and division box 10; Pulverizer 1 is connected with filter 2, and filter 2 all is connected with extractor 4 with high-pressure pump 3, and extractor 4 outer walls are provided with vapor recycle device 5; And the lower end of extractor 4 is connected with extract container 9 through dispensing valve 8, and extract container 9 is connected with division box 10.
Described extractor 4 inside bottom are provided with filter 7, filter 7 tops be provided with external communications get cinder notch 6.
Described filter 2 inside are 20 mesh sieves.
The course of work of this specific embodiment is: the washing dried ginger slice through pulverizer 1 is good with airing is pulverized, and crosses 20 mesh sieves.Crushing rear material is packed in the extractor 4, and solid-liquid ratio is 1: 1～1: 3, and is ready to preheating water; Through high-pressure pump 3 preheating water is pumped in the extractor 4, and pressure is risen to 20～25Mpa, open vapor recycle device 5, with the adjustment to 120 of extractor 4 ℃～150 ℃.This moment, extractor 4 interior water were in subcritical state, pressurize 10～15min.Steam off EGR 5 is opened extractor 4 lower end dispensing valves 8, and the extract that contains Ginger P.E of the extractor 4 inner high voltages filter 7 through extractor 4 bottoms is expelled in the container rapidly.After highly pressurised liquid in the extractor 4 is disposed to normal pressure, draw off the rhizoma zingiberis residue.Extract in the container is cooled to room temperature, uses division box 10 to remove the water in the extract, surplus products are Ginger P.E.
This specific embodiment has been broken traditional extraction idea and method to the extraction of rhizoma zingiberis; First subcritical water is extracted and be applied to Rhizoma Zingiberis extract, whole process does not need organic solvent, has that section emulates the advanced, a process cleaning, environmental friendliness; Extraction rate is fast; Efficient is high, the simple remarkable advantage of technology, and can satisfy the needs of industrialized production.
Claims (2)
1. adopt the device of active ingredient among the subcritical water extraction method extraction Jiang Gan; It is characterized in that it comprises pulverizer (1), filter (2), high-pressure pump (3), extractor (4), vapor recycle device (5), dispensing valve (8), extract container (9) and division box (10); Pulverizer (1) is connected with filter (2); Filter (2) all is connected with extractor (4) with high-pressure pump (3); Extractor (4) outer wall is provided with vapor recycle device (5), and the lower end of extractor (4) is connected with extract container (9) through dispensing valve (8), and extract container (9) is connected with division box (10).
2. the device of active ingredient is characterized in that described filter (2) inside is 20 mesh sieves among the employing subcritical water extraction method extraction Jiang Gan according to claim 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012200333487U CN202478646U (en) | 2012-01-17 | 2012-01-17 | Device for extracting active ingredients in dried gingers by adopting subcritical water extraction method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012200333487U CN202478646U (en) | 2012-01-17 | 2012-01-17 | Device for extracting active ingredients in dried gingers by adopting subcritical water extraction method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202478646U true CN202478646U (en) | 2012-10-10 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012200333487U Expired - Fee Related CN202478646U (en) | 2012-01-17 | 2012-01-17 | Device for extracting active ingredients in dried gingers by adopting subcritical water extraction method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN202478646U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107080970A (en) * | 2017-03-20 | 2017-08-22 | 河南雍华生态农业科技有限公司 | A kind of subcritical dialysis process of water soluble ingredient |
| CN112807726A (en) * | 2021-01-20 | 2021-05-18 | 福建蔓丝源生物科技有限公司 | Preparation device and use method of ginger extract |
-
2012
- 2012-01-17 CN CN2012200333487U patent/CN202478646U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107080970A (en) * | 2017-03-20 | 2017-08-22 | 河南雍华生态农业科技有限公司 | A kind of subcritical dialysis process of water soluble ingredient |
| CN112807726A (en) * | 2021-01-20 | 2021-05-18 | 福建蔓丝源生物科技有限公司 | Preparation device and use method of ginger extract |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee | ||
| CP03 | Change of name, title or address |
Address after: 266000, Qingdao District, Shandong City, Chengyang District, Hong Kong beach after the double lane road, 210 community Patentee after: QINGDAO H.EXTRACT CO., LTD. Address before: 266000, Houhai, Chengyang District, Qingdao Province, Shandong, 0774 Hong Kong Nishimura Patentee before: QINGDAO LIHE EXTRACT SCIENCE & TECHNOLOGY CO., LTD. |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Device for extracting active ingredients in dried gingers by adopting subcritical water extraction method Effective date of registration: 20161011 Granted publication date: 20121010 Pledgee: Qingdao high technology financing Company limited by guarantee Pledgor: QINGDAO H.EXTRACT CO., LTD. Registration number: 2016990000862 |
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| PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20170731 Granted publication date: 20121010 Pledgee: Qingdao high technology financing Company limited by guarantee Pledgor: QINGDAO H.EXTRACT CO., LTD. Registration number: 2016990000862 |
|
| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Device for extracting active ingredients in dried gingers by adopting subcritical water extraction method Effective date of registration: 20170822 Granted publication date: 20121010 Pledgee: Qingdao high technology financing Company limited by guarantee Pledgor: QINGDAO H.EXTRACT CO., LTD. Registration number: 2017370010048 |
|
| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20180814 Granted publication date: 20121010 Pledgee: Qingdao high technology financing Company limited by guarantee Pledgor: QINGDAO H.EXTRACT CO., LTD. Registration number: 2017370010048 |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20121010 Termination date: 20180117 |