CN202337689U - Molecular sieve variable-pressure adsorption nitrogen making device - Google Patents

Molecular sieve variable-pressure adsorption nitrogen making device Download PDF

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Publication number
CN202337689U
CN202337689U CN2011204852248U CN201120485224U CN202337689U CN 202337689 U CN202337689 U CN 202337689U CN 2011204852248 U CN2011204852248 U CN 2011204852248U CN 201120485224 U CN201120485224 U CN 201120485224U CN 202337689 U CN202337689 U CN 202337689U
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China
Prior art keywords
molecular sieve
nitrogen
nitrogen making
cabinet
valve
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Expired - Lifetime
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CN2011204852248U
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Chinese (zh)
Inventor
倪治忠
倪建峰
金星
黄红梅
黄国卫
张定海
张百祁
刘燕
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JIANGSU NANJI MACHINERY CO Ltd
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JIANGSU NANJI MACHINERY CO Ltd
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Abstract

The utility model relates to a molecular sieve variable-pressure adsorption nitrogen making device which consists of an electric cabinet, an air compressor, a dryer, a filter, an air storage cabinet, a nitrogen generator and a nitrogen storage cabinet sequentially connected, wherein the nitrogen generator comprises a check valve, a throttle valve, a first carbon molecular sieve nitrogen making cabinet and a second carbon molecular sieve nitrogen making cabinet; one end of the check valve is connected with the air storage cabinet; the other end is communicated with the inlets of the first and second carbon molecular sieve nitrogen making cabinets through first and second changeover valves respectively; the inlets of the first and second carbon molecular sieve nitrogen making cabinets are communicated with an exhaust device through first and second exhaust valves respectively; the outlets of the first and second carbon molecular sieve nitrogen making cabinets are communicated with one end of the throttle valve through first and second air supply valves respectively; and the other end of the throttle valve is communicated with the nitrogen storage cabinet. In the nitrogen making device, two carbon molecular sieve nitrogen making cabinets alternately perform circular nitrogen making, air supply and exhaust, and finish variable-pressure adsorption nitrogen making under uniform pressure; and the nitrogen making device has simple and compact structure, good nitrogen making effect and stable nitrogen making, is safe to use and realizes that the nitrogen making purity reaches over 99.5%.

Description

But molecular sieve transformation absorption nitrogen-making device
Technical field
The utility model relates to a kind of nitrogen-making device, but is a kind of molecular sieve transformation absorption nitrogen-making device specifically.
Background technology
Existing system nitrogen mode has three kinds, i.e. cryogenic air separation method, the empty point-score of molecular sieve and the empty point-score of film.Wherein deep cooling nitrogen production by air separation device is suitable for large-scale industry system nitrogen; Deep cooling nitrogen production by air separation complex equipments, floor space are big, and capital cost is higher, and the equipment one-time investment is more; Running cost is higher; Aerogenesis is slow, and (12~24h), installation requirement is high, the cycle is longer, and the scale of investment of the empty point-score PSA of the molecular sieve of same size device is than deep cooling air separation facility low 20%~50%; The empty point-score of film is suitable for the medium and small nitrogen user of nitrogen gas purity≤98%, and best-of-breed functionality price ratio is arranged, and nitrogen gas purity is 98% when above, and it is compared price with the PSA equipment of making nitrogen of same size and will exceed more than 15%; And the empty point-score technical process of molecular sieve is simple, level of automation is high, aerogenesis is fast, energy consumption is low; Product purity can be regulated according to user's needs in a big way; Characteristics such as convenient operating maintenance, running cost is lower, device flexibility is stronger; So in the following equipment of making nitrogen of 1000Nm3/h, have much competitive power; More and more obtain medium and small nitrogen user's welcome, the empty branch legal system of molecular sieve nitrogen has become medium and small nitrogen user's prefered method, and the raising of its system nitrogen performance becomes current research emphasis gradually.
Summary of the invention
It is a kind of simple in structure, compact that the utility model provides, and system nitrogen is effective, and system nitrogen is stable, but molecular sieve transformation safe in utilization absorption nitrogen-making device.
The technical scheme that the utility model adopts is: but a kind of molecular sieve transformation absorption nitrogen-making device; Connect to form successively by electric control box, air, moisture eliminator, strainer, gas storage holder, nitrogenous generator and storage nitrogen cabinet; It is characterized in that said nitrogenous generator comprises vacuum breaker, throttling valve and first and second carbonaceous molecular sieve system nitrogen cabinet; Vacuum breaker one termination gas storage holder; The other end is communicated with the import of first and second carbonaceous molecular sieve system nitrogen cabinet respectively through first and second switching valve, the import of first and second carbonaceous molecular sieve system nitrogen cabinet is communicated with a gas barrier through first and second vent valve respectively; The outlet of first and second carbonaceous molecular sieve system nitrogen cabinet is communicated with throttling valve one end through first and second steam supply valve respectively, and the throttling valve the other end is communicated with storage nitrogen cabinet; Be serially connected with first equilibrium valve between the import of first and second carbonaceous molecular sieve system nitrogen cabinet, be serially connected with second equilibrium valve between the outlet of first and second carbonaceous molecular sieve system nitrogen cabinet.
Further, be serially connected with nitrogen between the outlet of said first and second carbonaceous molecular sieve system nitrogen cabinet and detect valve.
Again further, said strainer comprises coarse filter and fine filtrator.
Air is by dry, thick through moisture eliminator successively, the dedusting of fine filtrator two-stage filtration after the air compression, and pressurized air is sent into gas storage holder, by gas storage holder through vacuum breaker to the nitrogenous generator air feed; System nitrogen process is made up of first and second carbonaceous molecular sieve system nitrogen cabinet work two portions circulation.
First circulation: system nitrogen; First switching valve is opened; To the first carbonaceous molecular sieve system nitrogen cabinet air feed, the oxygen in the first carbonaceous molecular sieve system nitrogen cabinet absorbed air, non-adsorbable nitrogen pass through first steam supply valve and supply nitrogen by throttling valve to storage nitrogen cabinet pressurized air through vacuum breaker, first switching valve.Exhaust, second vent valve is opened simultaneously, and the oxygen of the second carbonaceous molecular sieve system nitrogen cabinet internal adsorption discharges warp second vent valve to the gas barrier exhaust, and the second carbonaceous molecular sieve system nitrogen cabinet internal pressure becomes normal pressure.All press, behind the exhaust setting-up time, first and second equilibrium valve is opened, and first and second carbonaceous molecular sieve system nitrogen cabinet is realized all pressing, and the oxygen of the first carbonaceous molecular sieve system nitrogen cabinet internal adsorption is divided equally to first and second carbonaceous molecular sieve system nitrogen cabinet.
Second circulation: system nitrogen; After first loop ends; Second switching valve is opened; To the second carbonaceous molecular sieve system nitrogen cabinet air feed, the oxygen in the second carbonaceous molecular sieve system nitrogen cabinet absorbed air, non-adsorbable nitrogen pass through second steam supply valve and supply nitrogen by throttling valve to storage nitrogen cabinet pressurized air through vacuum breaker, second switching valve.Exhaust, first vent valve is opened simultaneously, and the oxygen of the first carbonaceous molecular sieve system nitrogen cabinet internal adsorption discharges warp first vent valve to the gas barrier exhaust, and the first carbonaceous molecular sieve system nitrogen cabinet internal pressure becomes normal pressure.All press, behind the exhaust setting-up time, first and second equilibrium valve is opened, and first and second carbonaceous molecular sieve system nitrogen cabinet is realized all pressing, and the oxygen of the second carbonaceous molecular sieve system nitrogen cabinet internal adsorption is divided equally to first and second carbonaceous molecular sieve system nitrogen cabinet.
Above-mentioned two portions circulation goes round and begins again, and realizes the alternation absorption discharging of nitrogen-making device.
But the utility model nitrogen-making device adopts two carbonaceous molecular sieve system nitrogen cabinet alternate cycles system nitrogen, air feed, exhaust, all presses completion transformation absorption system nitrogen, and it is simple in structure, compact, and system nitrogen is effective, and system nitrogen is stablized, and is safe in utilization, and system nitrogen purity reaches more than 99.5%.
Description of drawings
Fig. 1 is the utility model structural representation.
Among the figure: air 1, moisture eliminator 2, coarse filter 3, fine filtrator 4, gas storage holder 5, vacuum breaker 6; First switching valve, 7, the second switching valves, 8, the first equilibrium valves, 9, the first vent valves, 10, the second vent valves 11; Gas barrier 12, the first carbonaceous molecular sieve system nitrogen cabinets 13, the second carbonaceous molecular sieve system nitrogen cabinets 14, the second equilibrium valves 15, nitrogen detects valve 16; First steam supply valve, 17, the second steam supply valves 18, throttling valve 19, storage nitrogen cabinet 20, electric control box 21.
Embodiment
Below in conjunction with accompanying drawing the utility model is described further.
Shown in Figure 1, but a kind of molecular sieve transformation absorption nitrogen-making device comprises air 1, moisture eliminator 2, coarse filter 3, fine filtrator 4, gas storage holder 5, vacuum breaker 6, first switching valve 7, second switching valve 8, first equilibrium valve 9, first vent valve 10, second vent valve 11, gas barrier 12, the first carbonaceous molecular sieve system nitrogen cabinet 13, the second carbonaceous molecular sieve system nitrogen cabinet 14, second equilibrium valve 15, nitrogen detection valve 16, first steam supply valve 17, second steam supply valve 18, throttling valve 19, stores up nitrogen cabinet 20 and electric control box 21.Air 1 is connected to gas storage holder 5 through moisture eliminator 2, coarse filter 3, fine filtrator 4 successively; Gas storage holder 5 connects vacuum breaker 6 one ends; Vacuum breaker 6 the other ends are communicated with the import of first and second carbonaceous molecular sieve system nitrogen cabinet 13,14 respectively through first and second switching valve 7,8, the import of first and second carbonaceous molecular sieve system nitrogen cabinet 13,14 is communicated with a gas barrier 12 through first and second vent valve 10,11 respectively; Be serially connected with nitrogen between the outlet of first and second carbonaceous molecular sieve system nitrogen cabinet 13,14 and detect valve 16; The outlet of first and second carbonaceous molecular sieve system nitrogen cabinet 13,14 is communicated with throttling valve 19 1 ends through first and second steam supply valve 17,18 respectively, and throttling valve 19 the other ends are communicated with storage nitrogen cabinet 20; Be serially connected with first equilibrium valve 9 between the import of first and second carbonaceous molecular sieve system nitrogen cabinet 13,14, be serially connected with second equilibrium valve 15 between the outlet of first and second carbonaceous molecular sieve system nitrogen cabinet 13,14.The keying of all electrical parts is by electric control box 21 controls in this nitrogen-making device.

Claims (3)

1. but a molecular sieve transformation is adsorbed nitrogen-making device; Connect to form successively by electric control box, air, moisture eliminator, strainer, gas storage holder, nitrogenous generator and storage nitrogen cabinet; It is characterized in that: said nitrogenous generator comprises vacuum breaker, throttling valve and first and second carbonaceous molecular sieve system nitrogen cabinet; Vacuum breaker one termination gas storage holder; The other end is communicated with the import of first and second carbonaceous molecular sieve system nitrogen cabinet respectively through first and second switching valve, the import of first and second carbonaceous molecular sieve system nitrogen cabinet is communicated with a gas barrier through first and second vent valve respectively; The outlet of first and second carbonaceous molecular sieve system nitrogen cabinet is communicated with throttling valve one end through first and second steam supply valve respectively, and the throttling valve the other end is communicated with storage nitrogen cabinet; Be serially connected with first equilibrium valve between the import of first and second carbonaceous molecular sieve system nitrogen cabinet, be serially connected with second equilibrium valve between the outlet of first and second carbonaceous molecular sieve system nitrogen cabinet.
2. but molecular sieve transformation absorption nitrogen-making device according to claim 1 is characterized in that: be serially connected with nitrogen between the outlet of said first and second carbonaceous molecular sieve system nitrogen cabinet and detect valve.
3. but molecular sieve transformation absorption nitrogen-making device according to claim 1, it is characterized in that: said strainer comprises coarse filter and fine filtrator.
CN2011204852248U 2011-11-30 2011-11-30 Molecular sieve variable-pressure adsorption nitrogen making device Expired - Lifetime CN202337689U (en)

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102936005A (en) * 2012-11-27 2013-02-20 凯迈(洛阳)气源有限公司 Nitrogen making machine and method
CN103011097A (en) * 2012-12-18 2013-04-03 江苏泰达机电设备有限责任公司 Nitrogen generating and filling device
CN107512696A (en) * 2017-08-17 2017-12-26 四川五月花精密机械有限公司 A kind of red wine goes out the fresh system and method for bartender
CN111439731A (en) * 2020-04-30 2020-07-24 重庆卡贝乐化工有限责任公司 Fault self-checking online switching operation system of PSA nitrogen making device
US10730006B2 (en) 2018-08-14 2020-08-04 Air Products And Chemicals, Inc. Port separation for rotary bed PSA
US10744450B2 (en) 2018-08-14 2020-08-18 Air Products And Chemicals, Inc. Multi-bed rapid cycle kinetic PSA
US10835856B2 (en) 2018-08-14 2020-11-17 Air Products And Chemicals, Inc. Carbon molecular sieve adsorbent
CN113340019A (en) * 2021-05-27 2021-09-03 五邑大学 Molecular sieve based refrigerator
CN113375397A (en) * 2021-05-27 2021-09-10 五邑大学 Refrigerator based on molecular sieve

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102936005A (en) * 2012-11-27 2013-02-20 凯迈(洛阳)气源有限公司 Nitrogen making machine and method
CN102936005B (en) * 2012-11-27 2015-04-08 凯迈(洛阳)气源有限公司 Nitrogen making machine and method
CN103011097A (en) * 2012-12-18 2013-04-03 江苏泰达机电设备有限责任公司 Nitrogen generating and filling device
CN107512696A (en) * 2017-08-17 2017-12-26 四川五月花精密机械有限公司 A kind of red wine goes out the fresh system and method for bartender
US10730006B2 (en) 2018-08-14 2020-08-04 Air Products And Chemicals, Inc. Port separation for rotary bed PSA
US10744450B2 (en) 2018-08-14 2020-08-18 Air Products And Chemicals, Inc. Multi-bed rapid cycle kinetic PSA
US10835856B2 (en) 2018-08-14 2020-11-17 Air Products And Chemicals, Inc. Carbon molecular sieve adsorbent
CN111439731A (en) * 2020-04-30 2020-07-24 重庆卡贝乐化工有限责任公司 Fault self-checking online switching operation system of PSA nitrogen making device
CN113340019A (en) * 2021-05-27 2021-09-03 五邑大学 Molecular sieve based refrigerator
CN113375397A (en) * 2021-05-27 2021-09-10 五邑大学 Refrigerator based on molecular sieve
CN113340019B (en) * 2021-05-27 2024-05-28 五邑大学 Refrigerator based on molecular sieve

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C14 Grant of patent or utility model
GR01 Patent grant
C53 Correction of patent for invention or patent application
CB03 Change of inventor or designer information

Inventor after: Zhang Baiqi

Inventor after: Jin Xing

Inventor after: Zhang Dinghai

Inventor after: Wang Liqing

Inventor after: Ni Jilin

Inventor after: Huang Hongmei

Inventor after: Liu Yan

Inventor before: Ni Zhizhong

Inventor before: Ni Jianfeng

Inventor before: Jin Xing

Inventor before: Huang Hongmei

Inventor before: Huang Guowei

Inventor before: Zhang Dinghai

Inventor before: Zhang Baiqi

Inventor before: Liu Yan

COR Change of bibliographic data

Free format text: CORRECT: INVENTOR; FROM: NI ZHIZHONG NI JIANFENG JIN XING HUANG HONGMEI HUANG GUOWEI ZHANG DINGHAI ZHANG BAIQI LIU YAN TO: ZHANG BAIQI JIN XING ZHANG DINGHAI WANG LIQING NI JILIN HUANG HONGMEI LIU YAN

C53 Correction of patent for invention or patent application
CB03 Change of inventor or designer information

Inventor after: Zhang Baiqi

Inventor after: Jin Xing

Inventor after: Zhang Dinghai

Inventor after: Wang Liqing

Inventor after: Ni Jilin

Inventor after: Huang Hongmei

Inventor after: Liu Yan

Inventor before: Ni Zhizhong

Inventor before: Ni Jianfeng

Inventor before: Jin Xing

Inventor before: Huang Hongmei

Inventor before: Huang Guowei

Inventor before: Zhang Dinghai

Inventor before: Zhang Baiqi

Inventor before: Liu Yan

COR Change of bibliographic data

Free format text: CORRECT: INVENTOR; FROM: NI ZHIZHONG NI JIANFENG JIN XING HUANG HONGMEI HUANG GUOWEI ZHANG DINGHAI ZHANG BAIQI LIU YAN TO: ZHANG BAIQI JIN XING ZHANG DINGHAI WANG LIQING NI JILIN HUANG HONGMEI LIU YAN

CX01 Expiry of patent term
CX01 Expiry of patent term

Granted publication date: 20120718