CN202322668U - Continuous alkali wash system for isopropylbenzene - Google Patents
Continuous alkali wash system for isopropylbenzene Download PDFInfo
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- CN202322668U CN202322668U CN2011204377032U CN201120437703U CN202322668U CN 202322668 U CN202322668 U CN 202322668U CN 2011204377032 U CN2011204377032 U CN 2011204377032U CN 201120437703 U CN201120437703 U CN 201120437703U CN 202322668 U CN202322668 U CN 202322668U
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Abstract
The utility model discloses a continuous alkali wash system for isopropylbenzene. The system mainly comprises a sodium hydroxide tank, a material tank, a depositing tank, a primary alkali wash tank and a secondary alkali wash tank, the sodium hydroxide tank is respectively connected with the primary alkali wash tank and the secondary alkali wash tank, the material tank is connected with the primary alkali wash tank, the primary alkali wash tank is connected with the secondary alkali wash tank, and the secondary alkali wash tank is connected with the depositing tank. The continuous alkali wash system for isopropylbenzene has the following advantages: (1) the method of circulating reflux is adopted to sufficiently mix isopropylbenzene and sodium hydroxide, so that acidic impurities and volatile phenol in isopropylbenzene can be effectively removed; (2) isopropylbenzene and sodium hydroxide continuously get in and out, so that production is continuous, and thereby the productivity is increased; (3) when in contact, isopropylbenzene and sodium hydroxide are mixed by a mixer, so the effect is better.
Description
Technical field
The utility model relates to a kind of alkaline cleaner, specifically the continuous alkaline cleaner of isopropyl benzene.
Background technology
Existing isopropyl benzene alkali cleaning generally adds liquid caustic soda in storage tank, suitably bubbling perhaps uses pump to play the circulation mixing then, discharges salkali waste behind the redeposition.
Weak point has: 1. periodical operation, and duration of service is long, influences throughput; 2. in the alkaline cleaning procedure, liquid caustic soda contacts not enough with isopropyl benzene, cause alkali cleaning effect relatively poor.
The utility model content
The purpose of the utility model is the deficiency that exists to prior art, provides a kind of production efficiency height and alkali cleaning effect the good continuous alkaline cleaner of isopropyl benzene.
For realizing above-mentioned utility model purpose; The technical scheme that the utility model adopts is the continuous alkaline cleaner of a kind of isopropyl benzene; Mainly comprise liquid caustic soda groove, raw material tank, settling bath, one-level alkaline bath and secondary alkaline bath, said liquid caustic soda groove joins with one-level alkaline bath and secondary alkaline bath respectively, and said raw material tank and one-level alkaline bath join; Said one-level alkaline bath and secondary alkaline bath join, and said secondary alkaline bath and settling bath join.
Said liquid caustic soda groove joins with one-level alkaline bath and secondary alkaline bath respectively through the liquid caustic soda pump.
Said raw material tank joins through feedstock pump and one-level alkaline bath.
The outlet at bottom of said one-level alkaline bath is connected to one-level alkali cleaning pump, is connected to the one-level mixing tank on the said one-level alkali cleaning pump, and said one-level mixing tank joins with the import of one-level alkaline bath again.
The outlet at bottom of said secondary alkaline bath is connected to secondary alkali cleaning pump, is connected to the secondary mixing tank on the said secondary alkali cleaning pump, and said secondary mixing tank joins with the import of secondary alkaline bath again.
Beneficial effect: 1. adopt the method for pump around circuit, make isopropyl benzene and liquid caustic soda thorough mixing, effectively remove acidic impurities and volatile phenol in the isopropyl benzene; Isopropyl benzene and liquid caustic soda continuously into and out of, make to produce to be in continuous regime, enlarged production capacity; 3. isopropyl benzene and liquid caustic soda have mixing tank to mix, better effects if when contacting.
Description of drawings
Fig. 1 is the utility model structural representation.1. liquid caustic soda grooves among the figure, 2. raw material tank, 3. settling bath, 4. one-level alkaline bath, 5. secondary alkaline bath; 6. liquid caustic soda pump, 7. feedstock pump, 8. one-level alkali cleaning pump, 9. secondary alkali cleaning pump, 10. one-level mixing tank; 11. the secondary mixing tank, 12. baffle plates, the on-the-spot tensimeter of PG-, the on-the-spot liquidometer of LG-.
Embodiment
Below in conjunction with specific embodiment, further illustrate the utility model, present embodiment is being to implement under the prerequisite with the utility model technical scheme, should understand these embodiment only be used to the utility model is described and be not used in the restriction the utility model scope.
As shown in Figure 1, the continuous alkaline cleaner of a kind of isopropyl benzene mainly comprises liquid caustic soda groove 1, is provided with liquidometer and blow-down pipe; Raw material tank 2 is provided with liquidometer and blow-down pipe; Settling bath 3 is provided with liquidometer and blow-down pipe, and the opening for feed position is provided with baffle plate 12 and bottom groove; One-level alkaline bath 4 is provided with liquidometer and opening for feed inwardly projecting orifice, and hugging length reaches more than 6 meters; Secondary alkaline bath 5 is provided with liquidometer and opening for feed inwardly projecting orifice, and hugging length reaches more than 6 meters.
Wherein raw material tank 2, and outlet at bottom is connected with 7 imports of isopropyl benzene pump; 7 outlets of isopropyl benzene pump are connected with 8 imports of one-level alkali cleaning pump.Liquid caustic soda groove 1, outlet at bottom are connected with 8 imports of one-level alkali cleaning pump, 9 imports of secondary alkali cleaning pump respectively.One-level alkaline bath 4, bottom are provided with two outlets, and an outlet is connected with 8 imports of one-level alkali cleaning pump; Salkali waste is got rid of in another outlet.8 outlets of one-level alkali cleaning pump are connected with one-level mixing tank 10, are connected with 4 imports of one-level alkaline bath again.One-level alkaline bath 4 top exits are connected with 5 imports of secondary alkali cleaning pump.Secondary alkaline bath 5, bottom are provided with two outlets, and an outlet is connected with 9 imports of secondary alkali cleaning pump; Salkali waste is got rid of in another outlet.9 outlets of secondary alkali cleaning pump are connected with secondary mixing tank 11, are connected with 5 imports of secondary alkaline bath again.Secondary alkaline bath 5 top exits are connected with settling bath 3 imports.
Principle of work: raw material isopropyl benzene and liquid caustic soda get into one-level alkali cleaning pump simultaneously, through mixing tank, in the one-level alkaline bath, precipitate at last again.Post precipitation, lower floor is the liquid caustic soda layer, the upper strata is the isopropyl benzene oil reservoir.A liquid caustic soda layer part recycles through one-level alkali cleaning pump again, and an order part is discharged as salkali waste.The isopropyl benzene layer extrudes at the top, gets into the secondary caustic washing system.The secondary caustic washing system is identical with one-level caustic washing system principle, and the isopropyl benzene that the secondary alkali cleaning extrudes is suitable post precipitation in settling bath, discharges a small amount of salkali waste, and qualified isopropyl benzene is for use.
Working process: the raw material isopropyl benzene is delivered in the one-level alkali cleaning pump 8 through feedstock pump 2; Liquid caustic soda is delivered in the one-level alkali cleaning pump 8 through liquid caustic soda pump 1; The liquid caustic soda layer gets in the one-level alkali cleaning pump 8 in the one-level alkaline bath 4, and three kinds of materials are delivered in the mixing tank 10 by one-level alkali cleaning pump 8, are back to precipitated and separated in the one-level alkaline bath 4 again.Bottom liquid caustic soda layer segment refluxes and uses, and part is discharged; The top isopropyl benzene is laminated in the secondary alkali cleaning pump 9.
One-level alkaline bath 4 top isopropyl benzenes are laminated in the secondary alkali cleaning pump 9; Liquid caustic soda is delivered in the secondary alkali cleaning pump 9 through liquid caustic soda pump 1; The liquid caustic soda layer gets in the secondary alkali cleaning pump 9 in the secondary alkaline bath 5, and three kinds of materials are delivered in the mixing tank 11 by secondary alkali cleaning pump 9, are back to precipitated and separated in the secondary alkaline bath 5 again.Bottom liquid caustic soda layer segment refluxes and uses, and part is discharged; The top isopropyl benzene is laminated in the settling bath 3.
In the settling bath 3, the liquid caustic soda after the small amount of precipitate is discharged as salkali waste, and qualified isopropyl benzene is for use in storage tank.
Claims (5)
1. continuous alkaline cleaner of isopropyl benzene; It is characterized in that: comprise liquid caustic soda groove (1), raw material tank (2), settling bath (3), one-level alkaline bath (4) and secondary alkaline bath (5); Said liquid caustic soda groove (1) joins with one-level alkaline bath (4) and secondary alkaline bath (5) respectively; Said raw material tank (2) joins with one-level alkaline bath (4), and said one-level alkaline bath (4) and secondary alkaline bath (5) join, and said secondary alkaline bath (5) joins with settling bath (3).
2. according to the continuous alkaline cleaner of the said a kind of isopropyl benzene of claim 1, it is characterized in that: said liquid caustic soda groove (1) joins with one-level alkaline bath (4) and secondary alkaline bath (5) respectively through liquid caustic soda pump (6).
3. according to the continuous alkaline cleaner of the said a kind of isopropyl benzene of claim 1, it is characterized in that: said raw material tank (2) joins through feedstock pump (7) and one-level alkaline bath (4).
4. according to the continuous alkaline cleaner of the said a kind of isopropyl benzene of claim 1; It is characterized in that: the outlet at bottom of said one-level alkaline bath (4) is connected to one-level alkali cleaning pump (8); Be connected to one-level mixing tank (10) on the said one-level alkali cleaning pump (8), said one-level mixing tank (10) joins with the import of one-level alkaline bath (4) again.
5. according to the continuous alkaline cleaner of the said a kind of isopropyl benzene of claim 1; It is characterized in that: the outlet at bottom of said secondary alkaline bath (5) is connected to secondary alkali cleaning pump (9); Be connected to secondary mixing tank (11) on the said secondary alkali cleaning pump (9), said secondary mixing tank (11) joins with the import of secondary alkaline bath (5) again.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN2011204377032U CN202322668U (en) | 2011-11-08 | 2011-11-08 | Continuous alkali wash system for isopropylbenzene |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN2011204377032U CN202322668U (en) | 2011-11-08 | 2011-11-08 | Continuous alkali wash system for isopropylbenzene |
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CN202322668U true CN202322668U (en) | 2012-07-11 |
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CN2011204377032U Expired - Fee Related CN202322668U (en) | 2011-11-08 | 2011-11-08 | Continuous alkali wash system for isopropylbenzene |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111807920A (en) * | 2020-07-14 | 2020-10-23 | 中国石油化工股份有限公司 | Method and system for deacidifying cumene raw material of CHPPO (chlorinated Polypropylene oxide) device |
CN111848325A (en) * | 2020-07-14 | 2020-10-30 | 中国石油化工股份有限公司 | Method and system for washing cumene raw material with alkali by using CHPPO (chlorinated Polypropylene oxide) device |
CN111892474A (en) * | 2020-07-14 | 2020-11-06 | 中国石油化工股份有限公司 | System and method for pretreating cumene raw material of CHPPO (chlorinated Polypropylene oxide) device |
CN112010728A (en) * | 2019-05-29 | 2020-12-01 | 中国石油化工股份有限公司 | Alkali washing and water washing method |
CN113019338A (en) * | 2021-02-04 | 2021-06-25 | 合瑞康流体技术(北京)有限公司 | Method for removing organic acid from hydrocarbon oxidation liquid |
-
2011
- 2011-11-08 CN CN2011204377032U patent/CN202322668U/en not_active Expired - Fee Related
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112010728A (en) * | 2019-05-29 | 2020-12-01 | 中国石油化工股份有限公司 | Alkali washing and water washing method |
CN111807920A (en) * | 2020-07-14 | 2020-10-23 | 中国石油化工股份有限公司 | Method and system for deacidifying cumene raw material of CHPPO (chlorinated Polypropylene oxide) device |
CN111848325A (en) * | 2020-07-14 | 2020-10-30 | 中国石油化工股份有限公司 | Method and system for washing cumene raw material with alkali by using CHPPO (chlorinated Polypropylene oxide) device |
CN111892474A (en) * | 2020-07-14 | 2020-11-06 | 中国石油化工股份有限公司 | System and method for pretreating cumene raw material of CHPPO (chlorinated Polypropylene oxide) device |
CN111848325B (en) * | 2020-07-14 | 2023-05-09 | 中国石油化工股份有限公司 | Method and system for alkaline washing of cumene raw material by CHPPO device |
CN111892474B (en) * | 2020-07-14 | 2023-08-01 | 中国石油化工股份有限公司 | System and method for preprocessing cumene raw material of CHPPO device |
CN113019338A (en) * | 2021-02-04 | 2021-06-25 | 合瑞康流体技术(北京)有限公司 | Method for removing organic acid from hydrocarbon oxidation liquid |
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Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20120711 Termination date: 20201108 |