CN201859340U - 一种竹醋液提取提纯监控系统 - Google Patents

一种竹醋液提取提纯监控系统 Download PDF

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CN201859340U
CN201859340U CN2010205257207U CN201020525720U CN201859340U CN 201859340 U CN201859340 U CN 201859340U CN 2010205257207 U CN2010205257207 U CN 2010205257207U CN 201020525720 U CN201020525720 U CN 201020525720U CN 201859340 U CN201859340 U CN 201859340U
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bamboo vinegar
bamboo
monitoring system
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王志勇
崔宇
周玉清
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JIANGYIN CHINA GRAND BIOTECHNOLOGY Co.,Ltd.
Jiangyin Zhong Lin Technology Co.,Ltd.
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    • Y02P90/02—Total factory control, e.g. smart factories, flexible manufacturing systems [FMS] or integrated manufacturing systems [IMS]

Abstract

本实用新型涉及一种竹醋液提取提纯的监控系统。竹醋液具有很好的增效、催化功能和抗菌力。在竹子进行干馏炭化的过程中和在竹醋液的多级提纯的过程中，将温控系统和压力监控系统布控在生产设备中，其中将温控系统和压力监控系统分别布控在炭化炉、第一提取器、第二提取器、焦油归集器、尾气归集器及第一提纯器、第二提纯器、压滤装置的进入、输出的位置。

Description

一种竹醋液提取提纯监控系统 
技术领域
本发明涉及竹醋液提取提纯生产系统。特别涉及竹醋液提取提纯监控系统。 
背景技术
王志勇的“竹醋液的应用与其工业化生产概论”(《森林工程》2008年7月第24卷第4期)中公开了竹醋液是一种从毛竹炭化过程中提取的液体，具有消毒、除臭、促进植物生长、改良土壤等功效，可用作土壤杀菌剂、植物生长促进剂、异味清除剂，并可用于开发美容、美肤用品，以至用于治疗糖尿病等。目前该产品仍是土窑烧竹炭时产生的挥发物加以收集产生，是作为烧制竹炭的副产品加以利用，因此不仅产量低，且因一炉窑的烧制时间长达23天，生产时间长，又由于烧制竹炭过程中的燃料是木材，不仅破坏生态环境，而且会产生一定数量的木醋液，木醋液与竹醋液混合后很难分离，直接影响竹醋液的组分和性质，从而影响竹醋液的有效成分。 
CN1237180C中公开了一种竹醋液的制备方法，其利用竹材下脚料为原料经热解制取竹醋液。CN101020832A中公开了一种木或竹醋液的精制方法，其通过对木或竹醋液中通入臭氧，利用臭氧的强氧化性和在水溶液中的微凝聚作用对木醋原液进行处理，同时配合过滤和/或精馏等纯化方法，有效地去除了多环芳香类物质及部分溶解焦油，使木醋液纯度显著提高，获得无色透明的木(竹)醋液。公开号为特许公开平9-249886的日本专利申请中公开了一种“竹醋、木醋液的处理方法”，采用的是壳聚糖快速精制法，在该方法中采用水溶性壳聚糖配合少量碳酸钙以100份醋原液加入7份碳酸钙和0.5-5份水溶性壳聚糖混合处理，以便达到快速精制醋液的效果，使原本需要一年时间沉降的焦油和苯并芘等成分快速除去。但是，由于该方法的精制过程中需要使用水溶性壳聚糖，因此生产成本较高。CN1404974A中公开了一种从竹材中获取高温竹炭和精制竹醋的方法，其将竹材或者竹制品加工过程中产生的边角余料经过800℃-1200℃以上的电热干馏炭化、气相冷凝、液相冷凝分离和液相气化冷凝精制四道工序，获取高温竹炭和精制竹醋等有用资源。CN1687311A公开了一种竹醋的制备方法，其利用竹材下脚料为原料通过发酵、干馏等工艺过程得到竹醋液。CN100497525C中公开了一种精制竹醋液的制备工艺，其经过加入活性炭或竹炭吸附后经过离子交换树脂的纯化分离得到淡黄色的精制竹醋液。CN101049176A公开了一种竹醋液提取物及其制备与应用，其将竹醋液调节pH至5.5-7.5，于60-85℃、真空度0.09Mpa以上的条件下蒸馏，至馏出体积为原液体积25％-40％后，再调节余下的竹醋液至蒸馏前的pH值，于60-85℃、真空度0.09Mpa以上的条 件下蒸馏，至馏出体积为原液体积50％，所得的馏出液即为所述的竹醋液提取物，产品色泽微黄色。CN100358976C中公开了一种木、竹酸液高度精制的方法，其通过在木、竹酸原液中加入适量的过氧化氢水溶液，然后进行蒸馏得到无色透明高度精制的木、竹酸液。 
如上所述，目前国内竹醋液生产公司大都采用以生产竹炭为主、生产竹醋液为辅的设备。竹醋液产量偏低，甚至还含有有害物质。 
工艺水平仍停留在土窑的原始水平上，产品的技术指标偏低、品质不稳定，不适合做工业化加工的原料，尤其是不适合用于食品加工中。 
竹醋液生产工艺消耗资源、污染环境。在生产竹炭、竹醋时需投放与竹炭等量的燃材作为外加能源进行燃烧，消耗森林资源资源。 
没有回收竹醋液，尾气直接排放，造成了环境污染。 
所以，用先进的工艺技术对竹醋液的提取提纯进行全程监控，然后将各点监测到的数据汇总到控制箱，然后通过控制箱整体调节生产各环节的各项生产参数，便于以达到获得的竹醋液例如食品级竹醋液是十分必要。 
发明内容
竹子进行干馏炭化的过程中和在竹醋液的多级提纯的过程中，将温控系统(80℃-500℃)和压力监控系统(-0.08Mpa-0.09Mpa)进行布控，围绕预定的技术参数以随时监控、调整生产诸多因子，使生产设备能保质保量地生产出竹醋液和竹醋蒸馏液即食品级竹醋液。 
将温控系统和压力监控系统分别布控在炭化炉、第一提取装置、第二提取装置、焦油归集装置、尾气归集装置及第一提纯装置、第二提纯装置、第三提纯装置、压滤装置的进入、输出的位置。 
用本系统生产的竹醋液可以达到以下指标： 
1、生物得率(％)≥40、总酸含量(％)≥6、折光率(％)≥7.0、PH值2.5-2.8、密度g/mL≥1.01。 
2、不含3-4苯并芘、二恶英等有害物质； 
用本系统生产的蒸馏竹醋液即食品级竹醋液可以达到以下指标： 
1、得率(％)≥80、总酸含量(％)≥6、折光率(％)≤2.5、PH值2.2-2.6、密度g/mL≤1.009；溶解焦油≤0.08。 
2、砷≥0.00mg/L；镉≥0.01mg/L；铬≥0.02mg/L；铅≥0.10mg/L；汞≥0.002mg/L；硒≥0.002mg/L；银≥0.02mg/L；钡≥0.10mg/L。 
3、不含3-4苯并芘、二恶英等有害物质。 
  参数   检测限度   备注
  a-BHC a-六氯苯   0.50ug/L
  r-BHC  r-六氯苯   0.50ug/L
  b-BHC b-六氯苯   0.50ug/L
  Heptachlor七氯   0.50ug/L
  d-BHC d-六氯苯   0.50ug/L
  Aldrin  氯甲桥萘   0.50ug/L
  Heptaclor Epoxide七氯环氧化物   0.50ug/L
  Endosulfan I硫丹I   1.00ug/L
  DDE滴滴衣   1.00ug/L
  Dieldrin氧桥氯甲桥萘   1.00ug/L
  Endrin异狄氏剂   1.00ug/L
  DDD滴滴衣   3.00ug/L
  Endosulfan II硫丹II   3.00ug/L
  DDT滴滴涕   3.00ug/L
  Endrin Aldehyde异狄氏剂醛   3.00ug/L
  Endosulfan Sulfate硫酸硫丹   3.00ug/L
  Methoxychlor甲氧氯   0.50ug/L
  Chlordane.氯丹   45.2ug/L
  Doxaphene盐酸右丙氧芬   45.2ug/L
  Aroclor 1016氯化二苯1016   45.2ug/L
  Aroclor 1221氯化二苯1221   45.2ug/L
  Aroclor 1232氯化二苯1232   45.2ug/L
  Aroclor 1242氯化二苯1242   45.2ug/L
  Aroclor 1248氯化二苯1248   45.2ug/L
  Aroclor 1254氯化二苯1254   45.2ug/L
  Aroclor 1260氯化二苯1260   45.2ug/L
4、不含黄曲霉素肉毒杆菌金黄色葡萄球菌、链球菌等；而且具有生产周期短，效率高，成本低的特点。 
5、产品纯净、无色、无焦烟味； 
6、保质期18个月。 
通过本系统制得的的食品级竹醋有益效果主要体现在：(1)所述食品级竹醋与竹醋精制液或其他竹醋提纯液相比，无焦烟味，于国内外所生产的竹醋液及其它衍生产品相比较，具 有较强的杀菌、抑菌效果；产品纯净、无色，可广泛应用于食品、日化、医药等领域；与植物源的药剂配伍效果尤佳，使其应用范围扩大，经济附加值提高；(2)应用所述的食品级竹醋作为食品防腐剂，抑菌效果突出，其抑菌效果与化学合成的防腐剂相当甚至更优，作为天然产物原料的价格在食品防腐剂中为较低廉，可广泛的应用于各种食品加工领域；(3)因为食品级竹醋中的有机酸具有强烈的渗透力，可以做高渗透剂使用，具有很好的增效、催化功能，还可以作为解酒饮料的防腐保鲜剂。 
附图说明
图1：竹醋液制造工序图 
图2：食品级竹醋液提纯工艺流程图 
★为监控点 
具体实施方式
在如工序图或工艺流程图所示的监控点上布控温控系统和压力监控系统，可以围绕预定的技术参数以随时监控，使生产设备能保质保量地生产出竹醋液和食品级竹醋液。 

Claims (1)

1.一种竹醋液提取提纯的监控系统，竹子进行干馏炭化的过程中和在竹醋液的多级提纯的过程中，将温控系统和压力监控系统布控在生产设备中，其特征在于将温控系统和压力监控系统分别布控在炭化炉、第一提取器、第二提取器、焦油归集器、尾气归集器及第一提纯器、第二提纯器、压滤装置的进入、输出的位置。 
CN2010205257207U 2010-09-13 2010-09-13 一种竹醋液提取提纯监控系统 Expired - Lifetime CN201859340U (zh)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104366029A (zh) * 2014-06-09 2015-02-25 江阴中炬生物科技有限公司 一种肉鸡饲料添加用竹醋液及其应用
CN105087348A (zh) * 2015-09-28 2015-11-25 淄博大创自动化科技有限公司 高纯竹醋的生产收集系统

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104366029A (zh) * 2014-06-09 2015-02-25 江阴中炬生物科技有限公司 一种肉鸡饲料添加用竹醋液及其应用
CN105087348A (zh) * 2015-09-28 2015-11-25 淄博大创自动化科技有限公司 高纯竹醋的生产收集系统

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