CN201859072U - Titanium tetrachloride sampling device for producing refined titanium tetrachloride - Google Patents
Titanium tetrachloride sampling device for producing refined titanium tetrachloride Download PDFInfo
- Publication number
- CN201859072U CN201859072U CN2010205814910U CN201020581491U CN201859072U CN 201859072 U CN201859072 U CN 201859072U CN 2010205814910 U CN2010205814910 U CN 2010205814910U CN 201020581491 U CN201020581491 U CN 201020581491U CN 201859072 U CN201859072 U CN 201859072U
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- CN
- China
- Prior art keywords
- titanium tetrachloride
- sampling
- fixed cover
- rubber stopper
- slip cap
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Abstract
The utility model relates to the production of refined titanium tetrachloride and provides a titanium tetrachloride sampling device for producing refined titanium tetrachloride. The titanium tetrachloride sampling device comprises a sampling bottle. A guiding pipe (1), a sampling valve (2) and a sampling elbow (3) are arranged along the flowing direction of a titanium tetrachloride sample in sequence; a pipe opening at the outlet end of the sampling elbow (3) faces downwardly; the outlet end of the sampling elbow (3) is provide with a sealing mechanism matched with the pipe opening; as the sealing mechanism is adopted, the outflow of residue liquid is avoided, so that the working environment is obviously improved, the air is prevented from entering the sampling pipe, and the precision of the sampling liquid is improved. The device is suitable for sampling the titanium tetrachloride in the production of the refined titanium tetrachloride.
Description
Technical field
The utility model relates to the production of smart titanium tetrachloride, especially a kind of titanium tetrachloride sampler that is used for smart titanium tetrachloride production.
Background technology
During smart titanium tetrachloride was produced, in order to analyze each operation production run, the CONTROL PROCESS parameter provided foundation for instructing to produce, and needs titanium tetrachloride is taken a sample.
At present, a general drainage tube, the sample valve of adopting of domestic smart titanium tetrachloride manufacturer taken a sample to titanium tetrachloride with the sampler that a sampling elbow is connected.During sampling, sampling liquid flows through drainage tube, sample valve and sampling elbow and enters in the sampling jar.This sampler has following shortcoming: after sampling finished, raffinate flowed out in the stopple coupon, caused the production scene appearance in a large number because of titanium tetrachloride contacts the hydrochloric acid smog that produces with air, and working environment is relatively poor, and it is healthy that long-term operation meeting influences operating personnel; Go out in the process at the sampling raffinate stream, the water in air branch enters stopple coupon, with raffinate reaction in the stopple coupon, can bring certain influence to sampling liquid accuracy, can cause stopple coupon to stop up after long-time; The sample valve damage taking place in emergency circumstances, can't in time block stopple coupon, cause a large amount of titanium tetrachlorides to reveal, produce a large amount of harmful smog; When sample valve damages, change difficulty, and have a large amount of harmful smog to produce when changing.
The utility model content
Technical problem to be solved in the utility model provides a kind of raffinate of avoiding and is used for the titanium tetrachloride sampler that smart titanium tetrachloride is produced to what environment and sample accuracy impacted.
The technical scheme that its technical matters that solves the utility model adopts is: be used for the titanium tetrachloride sampler that smart titanium tetrachloride is produced, comprise sampling jar, be disposed with drainage tube, sample valve and sampling elbow along titanium tetrachloride sample flow direction, the described sampling elbow endpiece mouth of pipe down, the endpiece of described sampling elbow is provided with the sealing mechanism that matches with its mouth of pipe.
As a kind of preferred, described sealing mechanism is a rubber stopper.
Further, described sealing mechanism also comprises slip cap, fixed cover, compression spring, support; Fixedly connected with the sampling elbow endpiece mouth of pipe in described fixed cover top, described rubber stopper is fixedlyed connected with fixed cover by support, and described rubber stopper bottom is below the fixed cover bottom and be provided with the gap between rubber stopper and the fixed cover; Described slip cap and compression spring are enclosed within on the fixed cover respectively, and described slip cap fixed cover is axial and fixed cover is slidingly matched, described compression spring is arranged between fixed cover and the slip cap, and described slip cap bottom cooperates with the rubber stopper hermetic seal under the compression spring effect; Described rubber stopper maximum gauge is less than the sampling jar internal diameter of the bottleneck, and described slip cap is provided with the jacking block that matches with the sampling jar bottleneck.
As a kind of preferred version, described rubber stopper is up-small and down-big taper.
Further, be provided with sealing gasket or sealing ring between described slip cap and the fixed cover.
Further, be provided with emergent stop valve between described sample valve and the drainage tube.
Further, be provided with connecting pipe between described sampling elbow and the sample valve.
The beneficial effects of the utility model are: by the setting of sealing mechanism, avoided the outflow of raffinate, can obviously improve operating environment; Can prevent that air from entering stopple coupon, increase the accuracy of sampling liquid.The setting of emergent stop valve under the situation that sample valve damages, has been avoided the leakage of titanium tetrachloride, avoids producing harmful smog, has improved operating environment, has made things convenient for the replacing operation of sample valve simultaneously.
Description of drawings
Fig. 1 is a layout synoptic diagram of the present utility model.
Embodiment
Below in conjunction with drawings and Examples the utility model is further specified.
As shown in Figure 1, the titanium tetrachloride sampler that is used for smart titanium tetrachloride production of the present utility model, comprise sampling jar, be disposed with drainage tube 1, sample valve 2 and sampling elbow 3 along titanium tetrachloride sample flow direction, the described sampling elbow 3 endpiece mouths of pipe down, the endpiece of described sampling elbow 3 is provided with the sealing mechanism that matches with its mouth of pipe.
Above-mentioned sealing mechanism can be mechanisms such as screw thread cock, and for simplified structure, handled easily, described sealing mechanism is a rubber stopper 4.
In order further to simplify the operation, avoid manually plugging rubber stopper 4, described sealing mechanism also comprises slip cap 7, fixed cover 9, compression spring 8, support 10; Fixedly connected with the sampling elbow 3 endpiece mouths of pipe in described fixed cover 9 tops, described rubber stopper 4 is fixedlyed connected with fixed cover 9 by support 10, and described rubber stopper 4 bottoms are being provided with the gap below fixed cover 9 bottoms and between rubber stopper 4 and the fixed cover 9; Described slip cap 7 and compression spring 8 are enclosed within respectively on the fixed cover 9, and described slip cap 7 fixed covers 9 axially and fixed cover 9 be slidingly matched, described compression spring 8 is arranged between fixed cover 9 and the slip cap 7, and described slip cap 7 bottoms cooperate with rubber stopper 4 hermetic seals under compression spring 8 effects; Described rubber stopper 4 maximum gauges are less than the sampling jar internal diameter of the bottleneck, and described slip cap 7 is provided with the jacking block that matches with the sampling jar bottleneck.
When carrying out sampling operation, open sample valve 2, by contacting of sampling jar bottleneck and slip cap 7 jacking blocks, with slip cap 7 jack-up, slip cap 7 breaks away from rubber stopper 4, sampling liquid is successively by drainage tube 1, sample valve 2, sampling elbow 3, and the gap of finally passing through between rubber stopper 4 and the fixed cover 9 flows in the sampling jar.
After sampling finishes, sampling jar and slip cap 7 break away from, slip cap 7 resets under compression spring 8 effects, form hermetic seal with rubber stopper 4 once more, the raffinate that can prevent to take a sample flows out in a large number, produce harmful smog, can prevent simultaneously the water in air branch stopple coupon of entering, influence is the accuracy of sub-sampling liquid down.
Above-mentioned rubber stopper 4 can diameter greater than the cylindricality of slip cap 7 internal diameters, but in order to guarantee being sealed and matched of slip cap 7 and rubber stopper, the setting of jacking block for convenience simultaneously is in example as shown in the figure, described rubber stopper 4 is up-small and down-big taper, and described jacking block itself is made of slip cap 7.Concrete, in order to guarantee the position stability of rubber stopper 4, described support 10 is the threaded rods of fixedlying connected with fixed cover 9, and described rubber stopper 4 strings are on the threaded rod and by being positioned at below the rubber stopper 4 spacers with the threaded rod threaded engagement.
In order further to prevent the water in air branch stopple coupon of entering, be provided with sealing gasket or sealing ring between described slip cap 7 and the fixed cover 9.Concrete, in example as shown in the figure, adopt seal ring structure, be arranged between slip cap 7 inwalls and fixed cover 9 outer walls.
Further, be provided with emergent stop valve 5 between described sample valve 2 and the drainage tube 1.Under the situation that sample valve 2 damages, close emergent stop valve 5 rapidly, can prevent a large amount of titanium tetrachlorides leakages.This moment, detachable sample valve 2 was changed.For convenience of sampling operation, emergent stop valve 5 is an open type.
Take a sample for convenience installation of elbow 3 makes things convenient for sampling operation, is provided with connecting pipe 6 between described sampling elbow 3 and the sample valve 2.The length of connecting pipe 6 is determined according to concrete needs.
Concrete, in example as shown in the figure, drainage tube 1 one ends and the equipment or the pipeline welding that need sampling, the other end and emergent stop valve 5 are connected by flange; Emergent stop valve 5 other ends and sample valve 2 are connected by flange; Sample valve 2 and connecting pipe 6 are connected by flange; Connecting pipe 6 other ends and 3 welding of sampling elbow.
Claims (7)
1. be used for the titanium tetrachloride sampler that smart titanium tetrachloride is produced, comprise sampling jar, be disposed with drainage tube (1), sample valve (2) and sampling elbow (3) along titanium tetrachloride sample flow direction, described sampling elbow (3) the endpiece mouth of pipe is characterized in that down: the endpiece of described sampling elbow (3) is provided with the sealing mechanism that matches with its mouth of pipe.
2. the titanium tetrachloride sampler that is used for smart titanium tetrachloride production as claimed in claim 1, it is characterized in that: described sealing mechanism comprises rubber stopper (4).
3. the titanium tetrachloride sampler that is used for smart titanium tetrachloride production as claimed in claim 2, it is characterized in that: described sealing mechanism also comprises slip cap (7), fixed cover (9), compression spring (8), support (10); Fixedly connected with sampling elbow (3) the endpiece mouth of pipe in described fixed cover (9) top, described rubber stopper (4) is fixedlyed connected with fixed cover (9) by support (10), and described rubber stopper (4) bottom is positioned between below, fixed cover (9) bottom and rubber stopper (4) and the fixed cover (9) and is provided with the gap; Described slip cap (7) and compression spring (8) are enclosed within respectively on the fixed cover (9), and described slip cap (7) fixed cover (9) is axial and fixed cover (9) is slidingly matched, described compression spring (8) is arranged between fixed cover (9) and the slip cap (7), and described slip cap (7) bottom cooperates with rubber stopper (4) hermetic seal under compression spring (8) effect; Described rubber stopper (4) maximum gauge is less than the sampling jar internal diameter of the bottleneck, and described slip cap (7) is provided with the jacking block that matches with the sampling jar bottleneck.
4. the titanium tetrachloride sampler that is used for smart titanium tetrachloride production as claimed in claim 3, it is characterized in that: described rubber stopper (4) is up-small and down-big taper.
5. the titanium tetrachloride sampler that is used for smart titanium tetrachloride production as claimed in claim 3 is characterized in that: be provided with sealing gasket or sealing ring between described slip cap (7) and the fixed cover (9).
6. as claim 1,2,3, the 4 or 5 described titanium tetrachloride samplers that are used for smart titanium tetrachloride production, it is characterized in that: be provided with emergent stop valve (5) between described sample valve (2) and the drainage tube (1).
7. as claim 1,2,3, the 4 or 5 described titanium tetrachloride samplers that are used for smart titanium tetrachloride production, it is characterized in that: be provided with connecting pipe (6) between described sampling elbow (3) and the sample valve (2).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010205814910U CN201859072U (en) | 2010-10-28 | 2010-10-28 | Titanium tetrachloride sampling device for producing refined titanium tetrachloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010205814910U CN201859072U (en) | 2010-10-28 | 2010-10-28 | Titanium tetrachloride sampling device for producing refined titanium tetrachloride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201859072U true CN201859072U (en) | 2011-06-08 |
Family
ID=44104876
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010205814910U Expired - Fee Related CN201859072U (en) | 2010-10-28 | 2010-10-28 | Titanium tetrachloride sampling device for producing refined titanium tetrachloride |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201859072U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102435464A (en) * | 2011-11-23 | 2012-05-02 | 攀钢集团钛业有限责任公司 | Method and device for sampling titanium tetrachloride |
| CN107607363A (en) * | 2016-07-11 | 2018-01-19 | 宁波创润新材料有限公司 | Sampler and sampling method |
| CN107703089A (en) * | 2017-09-28 | 2018-02-16 | 陈林梭 | A kind of titanium tetrachloride infrared spectrograph sample detection means |
| CN112284831A (en) * | 2020-11-13 | 2021-01-29 | 禄丰新立钛业有限公司 | Titanium tetrachloride sampling device and method |
-
2010
- 2010-10-28 CN CN2010205814910U patent/CN201859072U/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102435464A (en) * | 2011-11-23 | 2012-05-02 | 攀钢集团钛业有限责任公司 | Method and device for sampling titanium tetrachloride |
| CN102435464B (en) * | 2011-11-23 | 2016-08-10 | 攀钢集团钛业有限责任公司 | The method and apparatus that titanium tetrachloride is sampled |
| CN107607363A (en) * | 2016-07-11 | 2018-01-19 | 宁波创润新材料有限公司 | Sampler and sampling method |
| CN107607363B (en) * | 2016-07-11 | 2019-12-20 | 宁波创润新材料有限公司 | Sampling device and sampling method |
| CN107703089A (en) * | 2017-09-28 | 2018-02-16 | 陈林梭 | A kind of titanium tetrachloride infrared spectrograph sample detection means |
| CN112284831A (en) * | 2020-11-13 | 2021-01-29 | 禄丰新立钛业有限公司 | Titanium tetrachloride sampling device and method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20110608 Termination date: 20151028 |
|
| EXPY | Termination of patent right or utility model |