CN201760239U - Raw material ethanol proportioning device in process for preparing acetaldehyde by utilizing catalytic oxidation of ethanol - Google Patents

Raw material ethanol proportioning device in process for preparing acetaldehyde by utilizing catalytic oxidation of ethanol Download PDF

Info

Publication number
CN201760239U
CN201760239U CN2010202581035U CN201020258103U CN201760239U CN 201760239 U CN201760239 U CN 201760239U CN 2010202581035 U CN2010202581035 U CN 2010202581035U CN 201020258103 U CN201020258103 U CN 201020258103U CN 201760239 U CN201760239 U CN 201760239U
Authority
CN
China
Prior art keywords
ethanol
pipeline
acetaldehyde
raw material
oxidation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2010202581035U
Other languages
Chinese (zh)
Inventor
张超
张立省
王广荣
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN2010202581035U priority Critical patent/CN201760239U/en
Application granted granted Critical
Publication of CN201760239U publication Critical patent/CN201760239U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Landscapes

  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The utility model relates to a raw material ethanol proportioning device in the process for preparing acetaldehyde by utilizing the catalytic oxidation of ethanol, belonging to an improved device for preparing the acetaldehyde by utilizing oxidation. The raw material ethanol proportioning device comprises an industrial ethanol gauge tank (1), a recovered ethanol gauge tank (2), a proportioning pump (5), a mixed raw material ethanol storage tank (6), a raw material ethanol feeding pump (7), an industrial ethanol charging pipeline (9), a recovered ethanol charging pipeline (10), a primary water intake pipeline (12), an ethanol-removing preheater pipeline (13), a fermented ethanol distillation head fraction charging pipeline (11), a fermented ethanol distillation head fraction gauge tank (3), a fermented ethanol distillation head fraction filter (4), and a charging filter (8).The utility model provides the raw material ethanol proportioning device in the process for preparing the acetaldehyde by utilizing the oxidation, which can fully utilize precious ethanol resources in the firstcut, reduces the production cost of the ethanol, enhances the market competition capacity and can prolong the service life of a catalyst.

Description

The alcohol catalysis oxidation prepares feed ethanol proportioner in the acetaldehyde technology
Technical field
The utility model is the proportioner that a kind of oxidation of ethanol prepares feed ethanol in the acetaldehyde technology.Belong to the device improvement for preparing acetaldehyde by oxidation.
Background technology
In fermentative production of ethanol technology, the heads that distillation workshop section collects is called as the foreshot, and the ethanol content among the foreshot is up to more than 90%.But the cost of the technical standard that reaches industrial alcohol owing to its separation is purified is higher, the way processing foreshot that most producers sell outside adopting at a low price.Cause the ethanol among the foreshot not to be fully used, cause the wasting of resources.
Oxidation of ethanol method of the prior art is produced in the acetaldehyde technology, reaction is about 84% batching ethanol with feed ethanol, after adopting about 70% recovery ethanol of 95% industrial alcohol and native system recovery to mix by a certain percentage, enter preheater, enter oxidation furnace then and participate in oxidative dehydrogenation.Still there are the following problems:
1. the ethanol raw material cost awaits further reduction, to improve the acetaldehyde competition capability.
2. catalyst is shorter service life.
Summary of the invention
The purpose of this utility model is to avoid above-mentioned weak point of the prior art, and provide a kind of ethanol resource that can either make full use of the preciousness among the foreshot, can reduce the acetaldehyde production cost again, improve its market competitiveness, and the oxidation of ethanol that can prolong catalyst service life prepares the proportioner of feed ethanol in the acetaldehyde technology.
The purpose of this utility model can reach by following measure:
Oxidation of ethanol of the present utility model prepares the proportioner of feed ethanol in the acetaldehyde technology, comprise the industrial alcohol measuring tank 1 that is connected with pipe fitting by pipeline, reclaim alcohol meter measuring tank 2, dosing pump 5, mixed material ethanol storage tank 6, feed ethanol feeding engine 7, industrial alcohol feeding line 9, reclaim ethanol feeding line 10, a water enters pipeline 12, removes ethanol preheater pipeline 13, it is characterized in that also comprising:
A. distill heads filter 4 by pipeline and the interconnective successively fermenting alcohol distillation of pipe fitting heads feeding line 11, fermenting alcohol distillation heads measuring tank 3, fermenting alcohol;
B. enter pipeline 12 and the charging filter 8 that goes ethanol preheater pipeline 13 to be connected by pipeline and pipe fitting and feed ethanol feeding engine 7, a water.
Oxidation of ethanol of the present utility model prepares the proportioner of feed ethanol in the acetaldehyde technology, oxidation of ethanol in the prior art prepares in the commercial plant of acetaldehyde, has added a. and has distilled heads filter 4 by pipeline and the interconnective successively fermenting alcohol distillation of pipe fitting heads feeding line 11, fermenting alcohol distillation heads measuring tank 3, fermenting alcohol; B. enter pipeline 12 and the charging filter 8 that goes ethanol preheater pipeline 13 to be connected by pipeline and pipe fitting and feed ethanol feeding engine 7, a water.Successful solution the ethanol among the foreshot of the prior art can not be fully used, cause the wasting of resources; And the ethanol raw material cost in the acetaldehyde production awaits further reduction, to improve two technical problems of acetaldehyde competition capability.
The impurity that fermenting alcohol distillation heads and other raw materials are brought the oxidation reaction stove into has been removed in the dual setting of fermenting alcohol distillation heads filter 4 and charging filter 8, has prolonged the service life of catalyst, has further reduced the production cost of acetaldehyde.
The disclosed oxidation of ethanol of the utility model prepares the technical scheme of the proportioner of feed ethanol in the acetaldehyde technology, can produce following good effect compared to existing technology:
1. a kind of ethanol resource that can either make full use of the preciousness among the foreshot is provided, can have reduced the acetaldehyde production cost again, improved its market competitiveness, and the oxidation of ethanol that can prolong catalyst service life prepares the proportioner of feed ethanol in the acetaldehyde technology.
2. the ethanol that has successfully solved among the foreshot of the prior art can not be fully used, and causes the problem of the wasting of resources.
3. the ethanol raw material cost in the acetaldehyde production reduces, and has improved the acetaldehyde competition capability.
4. prolong the service life of catalyst, reduced the production cost of acetaldehyde.
Description of drawings
Fig. 1 is the proportioner schematic diagram that oxidation of ethanol of the present utility model prepares feed ethanol in the acetaldehyde technology
Fig. 2 is the proportioner schematic diagram that oxidation of ethanol of the prior art prepares feed ethanol in the acetaldehyde technology
Among the figure
1-industrial alcohol measuring tank
2-reclaims the alcohol meter measuring tank
3-fermenting alcohol distillation heads measuring tank
4-fermenting alcohol distillation heads filter
The 5-dosing pump
6-mixed material ethanol storage tank
7-feed ethanol feeding engine
8-charging filter
9-industrial alcohol feeding line
10-reclaims the ethanol feeding line
11-fermenting alcohol distillation heads feeding line
Water of 12-enters pipeline
13-removes ethanol preheater pipeline.
The specific embodiment
The utility model is described in further detail below in conjunction with embodiment:
Oxidation of ethanol of the present utility model prepares the proportioner of feed ethanol in the acetaldehyde technology, comprise the industrial alcohol measuring tank 1 that is connected with pipe fitting by pipeline, reclaim alcohol meter measuring tank 2, dosing pump 5, mixed material ethanol storage tank 6, feed ethanol feeding engine 7, industrial alcohol feeding line 9, reclaim ethanol feeding line 10, a water enters pipeline 12, removes ethanol preheater pipeline 13, it is characterized in that also comprising:
A. distill heads filter 4 by pipeline and the interconnective successively fermenting alcohol distillation of pipe fitting heads feeding line 11, fermenting alcohol distillation heads measuring tank 3, fermenting alcohol;
B. enter pipeline 12 and the charging filter 8 that goes ethanol preheater pipeline 13 to be connected by pipeline and pipe fitting and feed ethanol feeding engine 7, a water.

Claims (1)

1. an oxidation of ethanol prepares the proportioner of feed ethanol in the acetaldehyde technology, comprise that industrial alcohol measuring tank (1), recovery alcohol meter measuring tank (2), dosing pump (5), mixed material ethanol storage tank (6), feed ethanol feeding engine (7), industrial alcohol feeding line (9), recovery ethanol feeding line (10), a water of being connected with pipe fitting by pipeline enter pipeline (12), remove ethanol preheater pipeline (13), is characterized in that also comprising:
A. distill heads filter (4) by pipeline and the interconnective successively fermenting alcohol distillation of pipe fitting heads feeding line (11), fermenting alcohol distillation heads measuring tank (3), fermenting alcohol;
B. enter pipeline (12) and the charging filter (8) that go ethanol preheater pipeline (13) be connected with pipe fitting with feed ethanol feeding engine (7), a water by pipeline.
CN2010202581035U 2010-07-14 2010-07-14 Raw material ethanol proportioning device in process for preparing acetaldehyde by utilizing catalytic oxidation of ethanol Expired - Fee Related CN201760239U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2010202581035U CN201760239U (en) 2010-07-14 2010-07-14 Raw material ethanol proportioning device in process for preparing acetaldehyde by utilizing catalytic oxidation of ethanol

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2010202581035U CN201760239U (en) 2010-07-14 2010-07-14 Raw material ethanol proportioning device in process for preparing acetaldehyde by utilizing catalytic oxidation of ethanol

Publications (1)

Publication Number Publication Date
CN201760239U true CN201760239U (en) 2011-03-16

Family

ID=43712837

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2010202581035U Expired - Fee Related CN201760239U (en) 2010-07-14 2010-07-14 Raw material ethanol proportioning device in process for preparing acetaldehyde by utilizing catalytic oxidation of ethanol

Country Status (1)

Country Link
CN (1) CN201760239U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103113201A (en) * 2013-03-12 2013-05-22 江苏凯茂石化科技有限公司 Production process of acetaldehyde
CN109364787A (en) * 2018-11-19 2019-02-22 云南昆船环保技术有限公司 A kind of alcohol concentration auto-scheduling system and its concocting method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103113201A (en) * 2013-03-12 2013-05-22 江苏凯茂石化科技有限公司 Production process of acetaldehyde
CN109364787A (en) * 2018-11-19 2019-02-22 云南昆船环保技术有限公司 A kind of alcohol concentration auto-scheduling system and its concocting method

Similar Documents

Publication Publication Date Title
CN102229520B (en) Method for preparing alcohol by acetic acid gas phase hydrogenation
CN101928217A (en) Novel method for synthetizing vinyl acetate by calcium carbide acetylene method
CN102399130B (en) Method for simplifying rectification process for preparing ethanol through hydrogenation of acetic acid
CN104945262A (en) Method for preparing prepare methyl nitrite by catalyzing methanol to reduce dilute nitric acid
CN1970688A (en) Ethylene bottom oil complex processing technology
CN103710155A (en) Method for preparing biodiesel through high-temperature esterification reaction of high acid value oil
CN102924233A (en) Method for preparing propylene glycol by glycerin hydrogenolysis
CN101941887A (en) Method for indirectly synthesizing ethanol by using carbon monoxide and hydrogen
CN201760239U (en) Raw material ethanol proportioning device in process for preparing acetaldehyde by utilizing catalytic oxidation of ethanol
CN101591574A (en) A kind of method of preparing biodiesel by zirconia solid base catalyst
CN101786782B (en) Cattle manure anaerobic fermentation process
CN102580766B (en) Regeneration method of recycled Raney-Ni catalyst for EHA (2-ethylhexyl 4-(dimethylamino)benzoate)
CN101704733B (en) New hydrolysis coupling process of methyl acetate and special device thereof
CN102690170A (en) Method for preparing ethanol by acetic acid gas phase hydrogenation
CN103819447A (en) Method for preparing glycerinum ketal ester by using glycerinum
CN103222538A (en) Method for recycling low-threonine-content ceramic membrane dialysate
CN108707061B (en) Process for preparing ethanol from methyl acetate by using methanol
CN102285883B (en) Method for synthesizing tributyl citrate (TBC) by adopting composite ionic liquid catalyst
CN103570498A (en) Method of preparing dichloropropanol by glycerol chlorination
CN204385192U (en) A kind of biogas fermentation, gas storage, airing system
CN202415410U (en) Multi-tower continuous operation system device for synthesizing methyl 3,3-dimethyl pentenoate
CN102285882B (en) Method for synthesizing acetyl tributyl citrate (ATBC) by adopting composite ionic liquid catalyst
CN107540522A (en) A kind of production technology of sec-butyl alcohol
CN201538755U (en) Device for smelting diesel oil by wasted tyre and rubber
CN104560411A (en) Technique for preparing fatty acid methyl ester by biological process

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
EE01 Entry into force of recordation of patent licensing contract

Assignee: Zhang Chao

Assignor: Zhang Chao

Contract record no.: 2011370000272

Denomination of utility model: Raw material ethanol proportioning device in process for preparing acetaldehyde by utilizing catalytic oxidation of ethanol

Granted publication date: 20110316

License type: Exclusive License

Record date: 20110622

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20110316

Termination date: 20170714

CF01 Termination of patent right due to non-payment of annual fee