CN101786782B - Cattle manure anaerobic fermentation process - Google Patents

Cattle manure anaerobic fermentation process Download PDF

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Publication number
CN101786782B
CN101786782B CN2010101306317A CN201010130631A CN101786782B CN 101786782 B CN101786782 B CN 101786782B CN 2010101306317 A CN2010101306317 A CN 2010101306317A CN 201010130631 A CN201010130631 A CN 201010130631A CN 101786782 B CN101786782 B CN 101786782B
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liquid
methane
solid
fermentation
cow dung
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CN101786782A (en
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关正军
李文哲
张鸿琼
毕兰平
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Northeast Agricultural University
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Northeast Agricultural University
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/30Fuel from waste, e.g. synthetic alcohol or diesel

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  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Processing Of Solid Wastes (AREA)
  • Treatment Of Sludge (AREA)

Abstract

The invention relates to a cattle manure anaerobic fermentation process which belongs to the technical field of anaerobic fermentation; the process comprises the following steps that: (1) a fluid spiral squeezing solid-liquid separator separates the fiber in cattle manure from raw materials which can be quickly fermented, and the separation process parameters are as follows: the mass ratio of cattle manure to water is 2:1, the spiral rotating speed is 68r/min, the separation gap is 1.5mm, and solid and liquid are prepared after solid-liquid separation; and (2) two-phase anaerobic digestion iscarried out to the liquid prepared in step (1), the fermentation temperature is 35DEG C, the inoculum is 30 percent when the methanogenic phase is started, the liquid is acidified for 3 days and enters a methane reactor, the daily feeding and discharge are one seventh of the effective volume of the methane reactor, the liquid discharged by the methane reactor is fermented for 1 day, the total hydraulic retention time is 11 days, and marsh gas is prepared; and the process makes full use of the crude fiber in the cattle manure, reduces the C/N of the fermentation raw materials, and has the advantages of short hydraulic retention time, high equipment utilization rate, water saving, and high methane yield in the marsh gas.

Description

一种牛粪厌氧发酵工艺 A kind of cow dung anaerobic fermentation process

技术领域technical field

本发明属于厌氧发酵技术,主要涉及牛粪便厌氧发酵处理工艺方法。The invention belongs to anaerobic fermentation technology, and mainly relates to an anaerobic fermentation treatment process of cow manure.

背景技术Background technique

目前,利用厌氧发酵处理畜禽养殖场粪便多采用简单的预处理和全混合发酵的方法。与猪粪和鸡粪相比,牛粪中粗纤维含量多,碳氮比大,在中温厌氧发酵过程中,粗纤维难于被厌氧微生物利用,影响牛粪发酵的产气效率;同时,简单的全混合发酵,水力停留时间长,设备利用率低,影响了利用牛粪厌氧发酵生产甲烷的经济效果。At present, simple pretreatment and full mixed fermentation methods are mostly used in the treatment of manure from livestock and poultry farms by anaerobic fermentation. Compared with pig manure and chicken manure, cow manure has more crude fiber content and higher carbon-to-nitrogen ratio. During the mesophilic anaerobic fermentation process, the crude fiber is difficult to be utilized by anaerobic microorganisms, which affects the gas production efficiency of cow manure fermentation; at the same time, Simple full mixed fermentation, long hydraulic retention time and low utilization rate of equipment affect the economic effect of anaerobic fermentation of cow dung to produce methane.

发明内容Contents of the invention

本发明的目的就是针对上述已有技术存在的问题,设计提供一种牛粪厌氧发酵工艺,达到使牛粪中粗纤维得到充分的综合利用、发酵水力停留时间短、产甲烷效率高的目的。The purpose of the present invention is to solve the problems existing in the above-mentioned prior art, and to design and provide a cow dung anaerobic fermentation process, so as to achieve the purpose of fully utilizing the crude fiber in cow dung, shortening the hydraulic retention time of fermentation and high methane production efficiency .

本发明的目的是这样实现的:一种牛粪厌氧发酵工艺,①、利用流状物螺旋压榨固液分离装置将牛粪中的纤维与可以快速发酵的原料分离开,分离工艺参数为:牛粪与水的质量比为2∶1,螺旋转速68转/分,分离间隙1.5毫米;固液分离后分别得到固形物和液体:其中固形物经干燥、压块后成为密度达到1.2克/厘米3的燃料块,为沼气工程加热保温提供燃料;②、利用上述①中分离后得到的TS值为6%、C/N小于20的液体进行两相厌氧发酵,发酵温度35℃,产甲烷相启动时,接种量为30%,料液酸化3天后进入产甲烷反应装置,每天进料量为产甲烷反应装置有效容积的1/7,对从产甲烷反应装置排出的料液后发酵1天,使料液中可产甲烷成份充分发酵,总水力停留时间11天,得甲烷沼气,完成牛粪厌氧发酵过程。The object of the present invention is achieved like this: a kind of cow dung anaerobic fermentation process, 1., utilize the solid-liquid separation device of streamline screw press to separate the fiber in the cow dung and the raw material that can ferment quickly, and separation process parameter is: The mass ratio of cow dung to water is 2:1, the screw speed is 68 rpm, and the separation gap is 1.5mm; after solid-liquid separation, solids and liquids are obtained respectively: the solids are dried and briquetted to become a density of 1.2 g/min. The fuel block of cm 3 provides fuel for the heating and heat preservation of the biogas project; ②, using the liquid with a TS value of 6% and a C/N less than 20 obtained after the separation in the above ① for two-phase anaerobic fermentation, the fermentation temperature is 35 ° C, and the product When the methane phase is started, the inoculation amount is 30%, and the feed liquid is acidified for 3 days and then enters the methanogenic reaction device. The daily feeding amount is 1/7 of the effective volume of the methanogenic reaction device. 1 day to fully ferment the methane-producing components in the feed liquid, and the total hydraulic retention time is 11 days to obtain methane biogas and complete the anaerobic fermentation process of cow dung.

该工艺可以充分利用牛粪中的有机废弃物,在提供沼气工程加热保温燃料的同时,又降低了发酵原料的C/N,采用两相厌氧发酵工艺,缩短了水力停留时间,提高设备利用率,节约用水,提高了沼气中甲烷产率,具有非常显著的应用前景。This process can make full use of the organic waste in cow dung. While providing heating and heat preservation fuel for biogas projects, it also reduces the C/N of fermentation raw materials. The two-phase anaerobic fermentation process shortens the hydraulic retention time and improves equipment utilization. efficiency, save water, and increase the methane yield in biogas, which has a very significant application prospect.

附图说明Description of drawings

附图是一种牛粪厌氧发酵工艺流程示意图。The accompanying drawing is a schematic flow chart of anaerobic fermentation of cow dung.

具体实施方式Detailed ways

下面举实例对本发明进行详细描述。一种牛粪厌氧发酵工艺,①、利用流状物螺旋压榨固液分离装置将牛粪中的纤维与可以快速发酵的原料分离开,分离工艺参数为:牛粪与水的质量比为2∶1,螺旋转速68转/分,分离间隙1.5毫米;固液分离后分别得到固形物和液体:其中固形物经干燥、压块后成为密度达到1.2克/厘米3的燃料块,为沼气工程加热保温提供燃料;②、利用上述①中分离后得到的TS值为6%、C/N小于20的液体进行两相厌氧发酵,发酵温度35℃,产甲烷相启动时,接种量为30%,料液酸化3天后进入产甲烷反应装置,每天进料量为产甲烷反应装置有效容积的1/7,对从产甲烷反应装置排出的料液后发酵1天,使料液中可产甲烷成份充分发酵,总水力停留时间11天,得甲烷沼气,完成牛粪厌氧发酵过程。The present invention is described in detail with examples below. An anaerobic fermentation process for cow dung, ①, using a fluid screw press solid-liquid separation device to separate the fiber in the cow dung from the raw materials that can be fermented quickly, the separation process parameters are: the mass ratio of cow dung to water is 2 : 1, the spiral speed is 68 rev/min, and the separation gap is 1.5 mm; after the solid-liquid separation, solids and liquids are obtained respectively: the solids become fuel blocks with a density of 1.2 g/ cm3 after drying and briquetting, which is a biogas project Heat and keep warm to provide fuel; ②, use the TS value obtained after separation in the above ① to be 6%, and the liquid with C/N less than 20 to carry out two-phase anaerobic fermentation, the fermentation temperature is 35 ° C, and when the methanogenic phase is started, the inoculum size is 30 %, the feed liquid enters into the methane reaction device after being acidified for 3 days, and the daily feeding amount is 1/7 of the effective volume of the methane reaction device. The methane component is fully fermented, the total hydraulic retention time is 11 days, methane biogas is obtained, and the anaerobic fermentation process of cow dung is completed.

本工艺中,固液分离后得到的固形物部份总固体含量TS不小于40%,牛粪厌氧发酵后,沼气容积产气率达到1.3m3/(m3·d),沼气中甲烷得率达到70%。In this process, the total solid content TS of the solid part obtained after solid-liquid separation is not less than 40%. After anaerobic fermentation of cow dung, the volumetric gas production rate of biogas reaches 1.3m 3 /(m 3 ·d), and methane in biogas Yield reaches 70%.

Claims (1)

1. cow dung anaerobic ferment process, 1., utilize stream shape thing screw press equipment for separating liquid from solid that fiber in the cow dung and raw material that can quick fermentation are separated it is characterized in that:, separation process parameters is: the mass ratio of cow dung and water is 2: 1,68 rev/mins of revolutions speed of screw, 1.5 millimeters of Separations; Obtain solid substance and liquid after the solid-liquid separation respectively: wherein become density behind solid substance drying, the briquetting and reach 1.2 gram per centimeters 3Fuel brick, for the biogas engineering heat tracing provides fuel; 2., utilize that the above-mentioned TS value that obtains after separating in 1. is 6%, C/N carries out diphasic anaerobic less than 20 liquid and ferments, 35 ℃ of leavening temperatures, when product methane starts mutually, inoculum size is 30%, the feed liquid acidifying entered after 3 days produces the methane reaction device, every day, inlet amount was for producing 1/7 of methane reaction device useful volume, to from producing the feed liquid secondary fermentation 1 day that the methane reaction device discharges, make and to produce the methane composition in the feed liquid and fully ferment, total hrt 11 days, get methane biogas, finish the cow dung anaerobic fermentation process.
CN2010101306317A 2010-03-24 2010-03-24 Cattle manure anaerobic fermentation process Expired - Fee Related CN101786782B (en)

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Publication number Priority date Publication date Assignee Title
CN101973684B (en) * 2010-11-03 2012-10-31 魏世锋 Separation and anaerobic fermentation technology after cow dung acidification
CN102786197A (en) * 2012-08-15 2012-11-21 东北农业大学 Cow dung and pig manure mixed anaerobic fermentation method
CN104512985A (en) * 2014-12-13 2015-04-15 佛山市高明区合朝农业发展有限公司 Piggery wastewater anaerobic digestion method for production of biogas
CN104846019A (en) * 2015-03-25 2015-08-19 东北农业大学 Gas making method by mixing and fermenting cow dung separating medium and kitchen garbage
CN108484232A (en) * 2018-05-30 2018-09-04 甘肃前进牧业科技有限责任公司 A kind of the treatment for cow manure system and processing method of dairy cow farm
CN114368889A (en) * 2020-10-15 2022-04-19 徐州生物工程职业技术学院 Biogas fermentation method using cow dung as raw material

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CN1060279A (en) * 1990-09-29 1992-04-15 上海东海水产科技服务部 Pig farm wastewater treatment and utilize technology
CN1054268C (en) * 1995-12-09 2000-07-12 杨兴容 Food conversion method by cow dung anaerobic fermentation
US6464875B1 (en) * 1999-04-23 2002-10-15 Gold Kist, Inc. Food, animal, vegetable and food preparation byproduct treatment apparatus and process
KR101003482B1 (en) * 2008-09-04 2010-12-28 이정규 Treatment method of high concentration organic wastewater

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