CN201477087U - Fully degassing system of chromatographic high-performance overall analysis online monitoring device - Google Patents

Fully degassing system of chromatographic high-performance overall analysis online monitoring device Download PDF

Info

Publication number
CN201477087U
CN201477087U CN2009201827463U CN200920182746U CN201477087U CN 201477087 U CN201477087 U CN 201477087U CN 2009201827463 U CN2009201827463 U CN 2009201827463U CN 200920182746 U CN200920182746 U CN 200920182746U CN 201477087 U CN201477087 U CN 201477087U
Authority
CN
China
Prior art keywords
oil
degassing tank
cylinder
line pipe
tank
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN2009201827463U
Other languages
Chinese (zh)
Inventor
王远远
诸建华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fuzhou Power Supply Co of State Grid Fujian Electric Power Co Ltd
Original Assignee
Fuzhou Power Supply Co of State Grid Fujian Electric Power Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fuzhou Power Supply Co of State Grid Fujian Electric Power Co Ltd filed Critical Fuzhou Power Supply Co of State Grid Fujian Electric Power Co Ltd
Priority to CN2009201827463U priority Critical patent/CN201477087U/en
Application granted granted Critical
Publication of CN201477087U publication Critical patent/CN201477087U/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Landscapes

  • Sampling And Sample Adjustment (AREA)

Abstract

The utility model relates to a fully degassing system of a chromatographic high-performance overall analysis online monitoring device, which comprises an oil filtering and back-streaming system and an online gas content detection system. The oil filtering and back-streaming system comprises an oil channel circulation system, a degassing tank, a mixer and an oil storage tank, the mixing component of the mixer extends into the degassing tank, the oil channel circulation system comprises a cylinder and a vacuum pump, the oil inlet of the cylinder is communicated with the upper oil outlet and the lower oil outlet of a transformer through oil channel pipelines, the vacuum pump is communicated with the oil inlet end of the cylinder through an oil channel pipeline, the oil inlet end of the cylinder is also communicated with a carrier gas channel system through an oil channel pipeline, the oil inlet of the cylinder is also communicated with the degassing tank and the oil storage tank through oil channel pipelines, the outlet of the degassing tank is communicated with the vacuum pump through an oil channel pipeline and is also communicated with the carrier gas channel system through an oil channel pipeline, and each oil channel pipeline is provided with a solenoid valve. The online gas content detection system comprises the mixer and the degassing tank in the oil filtering and back-streaming system, the outlet of the degassing tank is respectively connected with a pressure sensor and a gas collecting device through oil channel pipelines, and each oil channel pipeline is provided with a solenoid valve.

Description

The full degas system of chromatogram high-performance total analysis on-Line Monitor Device
Technical field
The present invention relates to a kind of novel chromatogram monitoring device, particularly a kind of full degas system that is applicable to the insulating oil chromatogram monitoring device of transformer.
Background technology
The stratographic analysis of insulation oil dissolved gas is to detect the effective ways that oil-filled inside electric appliance has the latency fault, and along with carrying out of electrical equipment repair based on condition of component work, the stratographic analysis of insulating oil seems more important, and testing will be heavier.Because laboratory off-line chromatogram sense cycle is longer, therefore national in recent years each province and city power department has all been carried out on-line monitoring, for active and effective effect has been played in the safe operation of electrical network main equipment.Existing degas system in use, exists complex structure, oil line pipe exists dead oil, detects the shortcomings such as difference of effect.
Summary of the invention
The objective of the invention is to overcome weak point of the prior art and a kind of novel improved detection quality is provided, simple in structure, the full degas system of easy to operate chromatogram high-performance total analysis on-Line Monitor Device.
The full degas system of a kind of chromatogram high-performance total analysis on-Line Monitor Device of the present invention, its structural feature is; It comprises that oil strain returns oil system, online air content detection system, described oil strain returns oil system and comprises the oil circulation system, degassing tank, stirrer, storage tank, the stirring parts of described stirrer stretches in the degassing tank, described oil circulation system comprises cylinder, vacuum pump, the logical hydraulic fluid port of cylinder is connected with the end of oil-out up and down of transformer by oil line pipe, described vacuum pump is connected with the blow vent end of cylinder by oil line pipe, the blow vent end of cylinder also is connected with the carrier gas air-channel system by oil line pipe, the logical hydraulic fluid port of described cylinder also by oil line pipe respectively with degassing tank, storage tank is connected, the outlet of degassing tank is connected by oil line pipe with vacuum pump, the outlet of degassing tank is also by oil line pipe communication with carrier gas air-channel system, each oil line pipe is provided with solenoid valve, described online air content detection system is to comprise that oil strain returns the stirrer in the oil system, degassing tank, the outlet of degassing tank also is connected with pressure transducer and gas extractor by oil line pipe respectively, and each oil line pipe is provided with solenoid valve.
The full degas system of this structure, in use, two pipelines are connected to the end of oil-out up and down of transformer, utilize the cylinder in the full degasser, stainless-steel tube by connecting V2 and transformer is among the transformer oil suction cylinder space A, by the stainless-steel tube that connects V4 and transformer the transformer oil among the cylinder space A is returned in the transformer again, carried out this operation and once be the circulation primary oil sample, can be according to the number of times that how much comes Control Circulation that calculates dead volume.It is quantitative just to carry out oil sample after circulation is good, again fixed measured oil sample is sent into the degas chamber processing that outgases, differential pressure pick-up detects air content in the oil according to the pressure differential before and after the oil-feed, the gas of deviating from enters gas extractor, and the gas collection ball is again operating in the subsequent handling of the gas introducing monitoring device of deviating from.
Described gas extractor is a kind of gas collection ball, and the gas collection ball is connected with six-way valve.
Behind gas extractor, set up six-way valve, the gas of deviating from can be changed over to earlier and carry out in the six-way valve quantitatively, reach a certain amount of after, it is changed in the follow-up post piece-rate system again and separates.
At the storage tank top oil level switch is set.
At the storage tank top oil level detecting switch is set, when for several times or oil several times when being drained in the storage tank, oil level reach a certain height, and oil level switch will detect signal, then oil is sent back among the cylinder space A again, carries out follow-up operation.
Be provided with grease proofing device between degassing tank and the pressure transducer
Grease proofing device is set, can prevents that a small amount of oil that carries in the gas from damaging pressure transducer.
The objective of the invention is to realize by following approach.
In sum, the present invention has following advantage compared to existing technology:
1. per minute of the present invention is once capable of circulation, according to in-line volume calculation clean cycle number of times, the dead oil that just can finish pipeline in several minutes cleans, simpler compared with the external ebullator loop structure of traditional usefulness, circulation is with effective and rapid, simultaneously more saved ebullator, not only saved cost, and avoided because of the caused various faults of ebullator.Whole monitoring device compact conformation, the characteristics that price is low.
2. the oil strain of chromatogram high-performance total analysis on-Line Monitor Device of the present invention returns oil system, adopted and directly returned the method that oil combines with oil extraction, after returning oil earlier, again remaining oil sample is entered in the storage tank, after running up to some Deng the oil in the storage tank, it is sent back among the cylinder space A again, carry out follow-up operation.Therefore the present invention can avoid remaining oil sample to stay the ill effect that causes in the degassing tank, can improve to detect quality, prolong chromatographic column serviceable life, prolong transformer oil and use the time.
3. air content degasser of the present invention owing to set up pressure sensing gas, therefore can be measured the air content in fuel-displaced.
Description of drawings
Fig. 1 is the structural representation of most preferred embodiment of the present invention
Embodiment
Below in conjunction with embodiment the present invention is described in more detail.
Most preferred embodiment:
A kind of full degas system of the chromatogram high-performance total analysis on-Line Monitor Device that is used for transformer as shown in Figure 1.Comprise that oil strain returns oil system 1, online air content detection system 2.Described oil strain returns oil system and comprises oil circulation system 11, degassing tank 12, stirrer 13, storage tank 14, the stirring parts 131 of described stirrer stretches in the degassing tank, described oil circulation system comprises cylinder 111, vacuum pump 112, the logical hydraulic fluid port of cylinder is connected with the end of oil-out up and down of transformer by oil line pipe, described vacuum pump is connected with the blow vent end of cylinder by oil line pipe, the blow vent end of cylinder also is connected with the carrier gas air-channel system by oil line pipe, the logical hydraulic fluid port of described cylinder also by oil line pipe respectively with degassing tank, storage tank is connected, the outlet of degassing tank is connected by oil line pipe with vacuum pump, the outlet of degassing tank is also by oil line pipe communication with carrier gas air-channel system, each oil line pipe is provided with solenoid valve V, described online air content detection system is to comprise that oil strain returns the stirrer in the oil system, degassing tank, the outlet of degassing tank also is connected with pressure transducer 3 and gas extractor 4 by oil line pipe respectively, and each oil line pipe is provided with solenoid valve.Described gas extractor is the gas collection valve, and described gas collection ball is connected with six-way valve 5, at the storage tank top oil level switch is set.Between degassing tank and pressure transducer, be provided with grease proofing device 6.
V2 and V4 are connected to the end of oil-out up and down of transformer with Φ 3 stainless-steel tubes,, at first open V5, V3, and vacuum pump, cylinder space A is carried out vacuum cleaned, close V3, V5 then in order to clean the dead oil in this stainless-steel tube.Open V2, V10.Allow transformer oil enter among the space A of cylinder by stainless-steel tube 1, closing V2, V10, open V16, V4, cylinder piston rod is moved downward, make the oil among the A of space come back in the transformer, for playing the abundant circulation of oil circuit, can estimate the volume of V2 to transformer coupling part stainless-steel tube, thereby calculate the dead oil in the complete pipe blow-through of the ability that to circulate several times, after cleaning is finished, at first open vacuum pump, V1, V3, V5, V9, V12, V13 vacuumizes cleaning to degas system inside, closes V3 then, V5, open V2, V10 allows oil sample enter to carry out among the cylinder space A oil sample quantitative, close V1 again, V2, V10, V12 opens the V3 stirring motor, allows measured surely oil enter the degassing tank degassing.Under vacuum state and beating action, gas sample in the oil can comparatively fast overflow, be filled in the space of not having oil and also can reach balance, this moment the pressure before pressure that pressure transducer produces and oil-feed the time, a pressure differential is arranged, can calculate air content in fuel-displaced according to this pressure differential, after gassiness measures, close V13, open V1, V6.Allow gas collection ball ball film move downward, make gas collect the top of gas collection ball, close V1, V6 then and open V9 the collection membrane of gas collection ball is moved upward, the gas of collecting is delivered in the quantity tube of six-way valve, then close V9 again, open V1, V6.The gas collection ball is moved downward, make the gas of deviating from collect gas collection ball top.When at this moment collecting gas owing to the first time major part being deviate from gas has collected and has transferred in the six-way valve quantity tube, can open V7, V11 respectively successively each 1 second, mending some gases enters and carries out wash-out in the oil, make the degassing reach comparatively ideal effect, repeat above step, can carry out the degassing more than 4 times altogether, degassing efficiency is reached more than 90%, by the time after the gas of deviating from is all sent into the six-way valve quantity tube, open six-way valve, by carrier gas the sample gas in the quantity tube is brought into chromatographic detector and enter qualitative and quantitative full constituent analysis.
The oil sample that has taken off gas returns in the transformer: at first open vacuum pump and V5, stirring motor, residual gas in the oil is taken out to the greatest extent, again V5 is closed V3, V10 opens, being extracted among the cylinder space A through vacuum treated oil sample, close V3 again, V10, open V4, V16 sends into transformer inside to the oil sample among the cylinder A, according to the actual tests situation, can operate through the oil that returns more than three times, just can all send in the transformer oil sample of test, in order to accomplish not remain the effect that a small amount of oil sample is stayed influence degassing next time in the deaeration pipe, there is not sump tank in the device, closing under the prerequisite of all valves, open V8, V14, with air pressure the irreducible oil in the deaeration pipe is pressed onto that the sump tank top does not have an oil level detecting switch in the sump tank, when for several times or tens times oil be drained in the sump tank, oil level reach a certain height, oil level switch will detect signal, drive vacuum pump then, V10, V14 is the oil in the sump tank again among the suction cylinder space A, again V14, V10 opens V3, V16, oil among the cylinder space A is sent into deaeration pipe carry out oil strain, the good back of filter is being returned oily method the oil sample in the deaeration pipe is being sent in the transformer according to above-mentioned.
1. 2. all joining in the diagram with the carrier gas air-channel system.
It is same as the prior art that present embodiment is not stated part.

Claims (4)

1. the full degas system of a chromatogram high-performance total analysis on-Line Monitor Device is characterized in that; It comprises that oil strain returns oil system, online air content detection system, described oil strain returns oil system and comprises the oil circulation system, degassing tank, stirrer, storage tank, the stirring parts of described stirrer stretches in the degassing tank, described oil circulation system comprises cylinder, vacuum pump, the logical hydraulic fluid port of cylinder is connected with the end of oil-out up and down of transformer by oil line pipe, described vacuum pump is connected with the blow vent end of cylinder by oil line pipe, the blow vent end of cylinder also is connected with the carrier gas air-channel system by oil line pipe, the logical hydraulic fluid port of described cylinder also by oil line pipe respectively with degassing tank, storage tank is connected, the outlet of degassing tank is connected by oil line pipe with vacuum pump, the outlet of degassing tank is also by oil line pipe communication with carrier gas air-channel system, each oil line pipe is provided with solenoid valve, described online air content detection system is to comprise that oil strain returns the stirrer in the oil system, degassing tank, the outlet of degassing tank also is connected with pressure transducer and gas extractor by oil line pipe respectively, and each oil line pipe is provided with solenoid valve.
2. the full degas system of chromatogram high-performance total analysis on-Line Monitor Device according to claim 1 is characterized in that; Described gas extractor is a kind of gas collection ball, and the gas collection ball is connected with six-way valve.
3. the full degas system of chromatogram high-performance total analysis on-Line Monitor Device according to claim 2 is characterized in that; At the storage tank top oil level switch is set.
4. the full degas system of chromatogram high-performance total analysis on-Line Monitor Device according to claim 3 is characterized in that; Be provided with grease proofing device between degassing tank and the pressure transducer.
CN2009201827463U 2009-09-01 2009-09-01 Fully degassing system of chromatographic high-performance overall analysis online monitoring device Expired - Lifetime CN201477087U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2009201827463U CN201477087U (en) 2009-09-01 2009-09-01 Fully degassing system of chromatographic high-performance overall analysis online monitoring device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2009201827463U CN201477087U (en) 2009-09-01 2009-09-01 Fully degassing system of chromatographic high-performance overall analysis online monitoring device

Publications (1)

Publication Number Publication Date
CN201477087U true CN201477087U (en) 2010-05-19

Family

ID=42413339

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2009201827463U Expired - Lifetime CN201477087U (en) 2009-09-01 2009-09-01 Fully degassing system of chromatographic high-performance overall analysis online monitoring device

Country Status (1)

Country Link
CN (1) CN201477087U (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101650353B (en) * 2009-09-01 2011-10-05 福建省电力有限公司福州电业局 Desaeration process of full desaeration system of chromatogram high-performance total analysis on-line monitoring device and desaeration system
CN104330286A (en) * 2014-10-22 2015-02-04 中国石油化工股份有限公司 Oil-gas concentration sampling detection device for external floating roof storage tank and sampling detection method of oil-gas concentration sampling detection device
CN104807681A (en) * 2014-01-24 2015-07-29 重庆地质矿产研究院 Automatic vacuum degassing instrument for coal bed gas or shale gas and corresponding vacuum degassing method
CN107008033A (en) * 2017-06-06 2017-08-04 利穗科技(苏州)有限公司 A kind of chromatographic column exhaust apparatus
CN112082828A (en) * 2020-08-04 2020-12-15 山东五岳电器有限公司 Online gas taking detection device and method for transformer gas relay

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101650353B (en) * 2009-09-01 2011-10-05 福建省电力有限公司福州电业局 Desaeration process of full desaeration system of chromatogram high-performance total analysis on-line monitoring device and desaeration system
CN104807681A (en) * 2014-01-24 2015-07-29 重庆地质矿产研究院 Automatic vacuum degassing instrument for coal bed gas or shale gas and corresponding vacuum degassing method
CN104807681B (en) * 2014-01-24 2019-07-16 重庆地质矿产研究院 Automatic vacuum degassing instrument for coal bed gas or shale gas and corresponding vacuum degassing method
CN104330286A (en) * 2014-10-22 2015-02-04 中国石油化工股份有限公司 Oil-gas concentration sampling detection device for external floating roof storage tank and sampling detection method of oil-gas concentration sampling detection device
CN107008033A (en) * 2017-06-06 2017-08-04 利穗科技(苏州)有限公司 A kind of chromatographic column exhaust apparatus
CN107008033B (en) * 2017-06-06 2022-04-22 利穗科技(苏州)有限公司 Chromatographic column exhaust device
CN112082828A (en) * 2020-08-04 2020-12-15 山东五岳电器有限公司 Online gas taking detection device and method for transformer gas relay

Similar Documents

Publication Publication Date Title
CN101650353B (en) Desaeration process of full desaeration system of chromatogram high-performance total analysis on-line monitoring device and desaeration system
CN201454165U (en) Gas online separating device in dielectric oil
CN201477087U (en) Fully degassing system of chromatographic high-performance overall analysis online monitoring device
CN102353724B (en) On-line detection system and method of trace dissolved gas in organic oil
CN107247108B (en) Transformer oil on-line monitoring high-concentration vacuum oil-gas separation device and method
CN101706482B (en) Full-automatic vacuum degasser and degassing method thereof
CN2859527Y (en) Automatic degassing sampling device for insulating oil chromatographic analysis
CN103252113A (en) On-line degasser for transformer oil gas
CN111220759A (en) Portable insulating oil gas content detection device and sealing defect diagnosis method based on gas content
CN103364461B (en) Online water heavy metal analyzer
CN104236985A (en) Oil-gas separator for monitoring gas dissolved in transformer oil on line
CN104880538B (en) Device and method for on-site inspection of online monitor for dissolved gas in transformer oil
CN109239229A (en) A kind of for transformer oil chromatography on-Line Monitor Device
CN2814408Y (en) Transformer oil chromatographic on-line monitoring system
CN103383296A (en) Leakage detecting system for condensers
CN201477086U (en) Full-automatic vacuum degasser
CN201477084U (en) Oil filtering and back-streaming system of chromatographic high-performance overall analysis online monitoring device
CN109521121A (en) A kind of method of vapor in the VOC monitoring device and separation sample gas of separable vapor
CN103323287B (en) Automatic sampling device for sampling furfural in transformer oil and sampling method
CN106053719B (en) Trace gas measuring device for electrical apparatus
CN210674325U (en) High-efficient degasser based on vacuum
CN213780031U (en) Online monitoring device for dissolved gas in transformer oil
CN109765275B (en) Method and device for rapidly detecting hydrogen sulfide content of crude oil on line outdoors
CN207318428U (en) Transformer oil monitors highly enriched vacuum gas and oil separating plant on-line
CN105259260A (en) Novel transformer oil chromatography online monitoring device with three-way valve

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee

Owner name: FUZHOU ELECTRIC POWER BUREAU, FUJIAN ELECTRIC POWE

Free format text: FORMER NAME: FUZHOU ELECTRIC POWER BUREAU OF FUJIAN PROVINCE

CP03 Change of name, title or address

Address after: 350009 Taijiang Fuzhou District, Fujian province Xingang Road No. 4 strip type frame, 12 storey building

Patentee after: Fuzhou Electric Power Bureau, Fujian Electric Power Co., Ltd.

Address before: 350009 No. 4, Xingang Road, Taijiang District, Fujian, Fuzhou

Patentee before: Fuzhou Electric Power Bureau of Fujian Province

AV01 Patent right actively abandoned

Granted publication date: 20100519

Effective date of abandoning: 20090901