CN201464413U - Microscopical electro chemical analysis device - Google Patents
Microscopical electro chemical analysis device Download PDFInfo
- Publication number
- CN201464413U CN201464413U CN2009201075315U CN200920107531U CN201464413U CN 201464413 U CN201464413 U CN 201464413U CN 2009201075315 U CN2009201075315 U CN 2009201075315U CN 200920107531 U CN200920107531 U CN 200920107531U CN 201464413 U CN201464413 U CN 201464413U
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- organic glass
- glass cover
- cover plate
- side organic
- analysis device
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Abstract
A microscopical electro chemical analysis device mainly consists of an organic glass plate (1), a left-side organic glass cover plate (2), a right-side organic glass cover pate (3), a copper plate electrode (4), wiring bolts (5) and insulators (6), wherein the left-side organic glass cover plate (2), the right-side organic glass cover pate (3), the organic glass plate (1) and the copper plate electrode (4) are mutually adhered to form the mainbody of the analysis device, and form a sample reservoir (23); and two sides of the analysis device are provided with dual-nut wiring bolts (5) provided with the insulators (6). The microscopical electro chemical analysis device has simple structure and low manufacturing cost, can be widely applied to determination and improvement and the like of scientific research, analysis, detection and production process in various industrial fields such as petrochemical technology, bioengineering and the like, and has extremely simple use and maintenance.
Description
Technical field
The utility model relates to a kind of microscopic analysis device that water-oil emulsion is carried out the electric demulsification analysis, belongs to microscopic analysis equipment.
Background technology
The electric demulsification of crude oil emulsion is that present oil field is to the defeated outside preceding treatment process a kind of commonly used of extraction crude oil, because the character of the different oil well produced crude oil in different oil fields even same oil field all has very big-difference, adopting which type of current field condition just can reach efficient breakdown of emulsion when carrying out electric demulsification is the problem that each elephant is concerned about.To determine that at the scene the best electric pulse field parameter of electric demulsification often will test many times, and need the cost long time.
Based on above-mentioned situation, Many researchers has all proposed a kind of microscopic analysis experimental technique that carries out in the laboratory, generally all adopt a cover microscopic analysis system to experimentize, the analytic system that is adopted generally comprises computer, video frequency collection card and Analysis of Matching software thereof, high-voltage power supply, microscopic analysis device, optical microscope, video camera and connecting line etc.As long as the software and hardware condition that is equipped with is suitable, in such system, all can test accordingly.Except the microscopic analysis device, other ingredients in the microscopic analysis system all have the product of moulding at present.
Summary of the invention
According to background technology, the purpose of this utility model is to provide a kind of electrochemical analysis device that is used for the microscopic analysis of emulsion fluid electric demulsification based on above-mentioned microscopic analysis system, mainly form by organic glass flat board, cover plate, copper coin electrode, connection bolt and sample cell, the copper coin electrode is connected with connection bolt, can connect high-voltage power supply, for safety is gone back the suit insulator on connection bolt.
To achieve these goals, the utility model is achieved through the following technical solutions:
A kind of micro-electrochemical analysis device, mainly by organic glass flat board (1), left side organic glass cover plate (2), right side organic glass cover plate (3), copper coin electrode (4), connection bolt (5) and insulator (6) are formed, wherein: by left side organic glass cover plate (2), right side organic glass cover plate (3), organic glass flat board (1) and copper coin electrode (4) by the mutual bonding composition analysis device main body of insulating gel, and constitute sample cell (23), go up the spool insulator (6) that suit has wire hole (61) at connection bolt (5).
The end lower surface of described left side organic glass cover plate (2) is provided with a rectangle groove (21), and be shaped on bolt hole (24) at the middle part of its rectangle groove (21), be provided with square three-way groove (22) at the edge, the other end of left side organic glass cover plate (2), copper coin electrode (4) is shaped on an end of bolt hole (41) and inserts in the rectangle groove (21) of left side organic glass cover plate (2), copper coin electrode (4) is bonding mutually with left side organic glass cover plate (2), the other end crimp (42) of its copper coin electrode (4) is bonding with the side (25) of square three-way groove (22), by the bolt hole (24) of left side organic glass cover plate (2) and copper coin electrode (4), (41) be provided with the connection bolt (5) of double nut (51); One rectangle groove (31) and bolt hole (32) are set on right side organic glass cover plate (3), copper coin electrode (4) is bonding mutually with right side organic glass cover plate (3), the other end crimp (42) of copper coin electrode (4) is bonding with an end margin of right side organic glass cover plate (3), and connection bolt (5) is set on right side organic glass cover plate (3).
Microscopic analysis device of the present utility model is placed on the objective table of optical microscope, microscope is connected with digital camera, digital camera mutually again be contained in computer on video frequency collection card link to each other, when the microscopic analysis device being linked to each other with high-voltage power supply and during energized, just can on computer screen, see the variation that is taken place in the microscopic analysis device by microscope and video camera and analysis software, as the distortion of water droplet in the water-oil emulsion and situation such as coalescent. as long as the enlargement factor of microscopical object lens and analysis software is suitable, just can see micron-sized water droplet motion conditions clearly, by changing the electric pulse field parameter of power supply output, just can observe of the influence of different current field conditions to emulsion breakdown, can find out suitable separately current field condition at different emulsion fluid, can be used for instructing execute-in-place.
Owing to adopted technique scheme, the utlity model has following advantage and effect:
1, the utility model insulativity is good, can be used for the experimental study under the high-voltage power supply.
2, the utility model compact conformation is simple, and is cheap, can be widely used in petrochemical complex, and the scientific research of multiple industrial circle such as bioengineering is analyzed, and detects aspects such as the formulation of production technology and typing.
Description of drawings
Fig. 1 is the utility model structure collectivity schematic perspective view
Fig. 2 is the utility model left side organic glass covering plate structure synoptic diagram
Fig. 3 is the utility model right side organic glass covering plate structure synoptic diagram
Fig. 4 is the utility model copper coin electrode structure synoptic diagram
Fig. 5 is the utility model and microscopic analysis system connection diagram
Embodiment
As shown in Figures 1 to 4, a kind of micro-electrochemical analysis device, mainly by organic glass flat board 1, left side organic glass cover plate 2, right side organic glass cover plate 3, copper coin electrode 4, connection bolt 5 and insulator 6 are formed, wherein: by the mutual bonding composition analysis device main body of insulating gel, and constitute sample cell 23 by left side organic glass cover plate 2, right side organic glass cover plate 3, organic glass dull and stereotyped 1 and copper coin electrode 4, suit has the spool insulator 6 of wire hole 61 on connection bolt 5.
The end lower surface of described left side organic glass cover plate 2 is provided with a rectangle groove 21, and be shaped on bolt hole 24 at the middle part of its rectangle groove 21, edge, the other end at left side organic glass cover plate 2 is provided with square three-way groove 22, copper coin electrode 4 is shaped on an end of bolt hole 41 and inserts in the rectangle groove 21 of left side organic glass cover plate 2, copper coin electrode 4 is bonding mutually with left side organic glass cover plate 2, the other end crimp 42 of its copper coin electrode 4 is bonding with the side 25 of square three-way groove 22, by the bolt hole 24 of left side organic glass cover plate 2 and copper coin electrode 4,41 are provided with the connection bolt 5 of double nut 51; One rectangle groove 31 and bolt hole 32 are set on right side organic glass cover plate 3, copper coin electrode 4 is bonding mutually with right side organic glass cover plate 3, the other end crimp 42 of copper coin electrode 4 is bonding with an end margin of right side organic glass cover plate 3, on right side organic glass cover plate 3 connection bolt 5 is set.
Other knows, by Fig. 5 the connection diagram of the utility model and microscopic analysis system is shown, among the figure: 7-high-voltage power supply control box, 8-microlens, 9-digital camera, 10-video frequency collection card, 11-computer, 12-display screen, 13-cable, 14-electric power connection line.
The utility model places on the objective table of optical microscope, microlens 8 links to each other with digital camera 9, and link to each other with video frequency collection card 10 on being contained in computer 11 mainboards by cable 13, the image analysis software supporting with digital camera 9 and video frequency collection card 10 is housed in the computer 11. analyzed sample is put into the sample cell 23 of microscopic analysis device, mix up microscope, after the energized, in the sample cell 23 of micro-electrochemical analysis device, regulate microscope and make the sample characteristic in the clear show sample of the energy pond on the computer monitor screen 12, open high-voltage power supply, regulate the electric field intensity and the frequency that apply on the sample cell 23, can on computer monitor screen 12, clearly observe the motion conditions of water droplet under different current field conditions in the emulsion fluid, may take place coalescent as water droplet, form the water droplet chain, vibration, distortion, break etc. at specific oil-water emulsion, carry out oil-moisture from the time, can be according to the best current field condition of analyzing needs by the observed phenomenon in microscopic analysis unit, to be used to instruct execute-in-place.
When the utility model is connected with high-voltage power supply control box 7, pick up insulator 6 earlier, electric power connection line 14 is passed through wires hole 61 on it, exposed tinsel with electric power connection line 14 is entangled between two nuts 51 of connection bolt 5 then, and fastening nut 51, cover is loaded onto the insulator of being made by polytetrafluoroethylmaterial material 6 then, and the other end of electric power connection line 14 is connected with high-voltage power supply control box 7, will apply the electric field of certain intensity when power connection in sample cell 23.
Claims (2)
1. micro-electrochemical analysis device, mainly by organic glass flat board (1), left side organic glass cover plate (2), right side organic glass cover plate (3), copper coin electrode (4), connection bolt (5) and insulator (6) are formed, it is characterized in that: left side organic glass cover plate (2), right side organic glass cover plate (3), organic glass flat board (1) and copper coin electrode (4) are by the mutual bonding composition analysis device main body of insulating gel, and constitute sample cell (23), go up the spool insulator (6) that suit has wire hole (61) at connection bolt (5).
2. micro-electrochemical analysis device according to claim 1, it is characterized in that: the end lower surface of left side organic glass cover plate (2) is provided with a rectangle groove (21), and be shaped on bolt hole (24) at the middle part of its rectangle groove (21), be provided with square three-way groove (22) at the edge, the other end of left side organic glass cover plate (2), copper coin electrode (4) is shaped on an end of bolt hole (41) and inserts in the rectangle groove (21) of left side organic glass cover plate (2), copper coin electrode (4) is bonding mutually with left side organic glass cover plate (2), the other end crimp (42) of its copper coin electrode (4) is bonding with the side (25) of square three-way groove (22), by the bolt hole (24 of left side organic glass cover plate (2) and copper coin electrode (4), 41) be provided with the connection bolt (5) of double nut (51); One rectangle groove (31) and bolt hole (32) are set on right side organic glass cover plate (3), copper coin electrode (4) is bonding mutually with right side organic glass cover plate (3), the other end crimp (42) of copper coin electrode (4) is bonding with an end margin of right side organic glass cover plate (3), and connection bolt (5) is set on right side organic glass cover plate (3).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009201075315U CN201464413U (en) | 2009-04-24 | 2009-04-24 | Microscopical electro chemical analysis device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009201075315U CN201464413U (en) | 2009-04-24 | 2009-04-24 | Microscopical electro chemical analysis device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201464413U true CN201464413U (en) | 2010-05-12 |
Family
ID=42391763
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009201075315U Expired - Fee Related CN201464413U (en) | 2009-04-24 | 2009-04-24 | Microscopical electro chemical analysis device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201464413U (en) |
-
2009
- 2009-04-24 CN CN2009201075315U patent/CN201464413U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20100512 Termination date: 20130424 |