CN201454525U - Self-adjusting quick reaction kettle - Google Patents
Self-adjusting quick reaction kettle Download PDFInfo
- Publication number
- CN201454525U CN201454525U CN2009200243949U CN200920024394U CN201454525U CN 201454525 U CN201454525 U CN 201454525U CN 2009200243949 U CN2009200243949 U CN 2009200243949U CN 200920024394 U CN200920024394 U CN 200920024394U CN 201454525 U CN201454525 U CN 201454525U
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- pipe
- guide rail
- fixed disk
- outer guide
- kettle
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Abstract
The utility model relates to a self-adjusting quick reaction kettle for the mixing and reaction of different chemical raw materials, which is additionally provided with a liquid level adjusting part in a kettle body on the basis of the traditional reaction kettle. The liquid level adjusting part mainly comprises a gas communicated pipe, a groove-shaped float body, a movable pipe of the float body, an upper fixed plate of an inner guide rail, a lower fixed plate of the inner guide rail, a lower fixed plate of an outer guide rail, an upper fixed plate of the outer guide rail, the inner guide rail, the outer guide rail, an annular float body, a connecting rod and a liquid retaining pipe. The utility model achieves the aim of quickly and evenly mixing non mutually-soluble liquid and solid, ensures automatic process of evenly-mixing by one-time setting, and is widely suitable for reactions between organic matters and between the organic matters and inorganic matters. Since the mixing is quick and even, the reaction time is shorter and the degree of side reaction is reduced, the quality of produced products is high; in addition, the reaction time after evenly mixing is shortened so that energy sources are saved.
Description
Technical field
The utility model relates to the reactor (device) in chemical production equipment field, not only be fit to effectively mix and reaction needed between the general intersolubility liquid, especially can be to the self-adjusting quick reaction kettle of rapid mixing and reaction between non-mutually soluble liquids, between liquid and solid.
Background technology
Reactor is the mixing and the reaction unit commonly used of chemical production field.Present reactor (device) primary structure is that various feed inlet and outlets and drive motors, agitator etc. are set on kettle, utilizes agitator to rotate mixing and the reaction of quickening between the raw material, reaches the purpose of producing various chemical products with this.But the reason owing to the intersolubility difference often appears in the actual production between the liquid (or solid) of reaction raw materials (or non-reaction dissolvent), situations such as larger area contact appear after raw material adds reactor between the drop of layering intuitively and microcosmic, occur being difficult to effective mixing between the raw material (or non-reaction dissolvent), influence the even contact between reaction raw materials and the time of reaction, finally cause long, problems such as reaction is insufficient, side reaction increase and poor product quality of reaction time.Be the speed of the whole stirring of raising in reactor at present for the method one that reaches mixing between medium, the 2nd, adopt the feed liquor liquid distributor to strengthen the even of feed liquor.
The utility model content
The purpose of this utility model is exactly the defective that exists at prior art, provide a kind of can according between the liquid (or solid) of raw material (or non-reaction dissolvent) because situations such as larger area contact appear between the drop of layering intuitively and microcosmic in the intersolubility difference, automatically adjust the mixed proportion between the raw material, and then force quick mixing, improve the self-adjusting quick reaction kettle of raw material mixing and reaction speed.
Its technical scheme is: comprise kettle and the feed inlet and outlet, the drive motors that are arranged on the kettle, and be arranged on the agitator in the kettle, agitator is that V shape stirs 1.1 structures; Upwards be fixed with centre chamber's pipe 1.3 at kettle 1.2 inner bottom parts, the cross section formed "T"-shaped post chamber after 1.3 top hole enlargements were managed by centre chamber, the upper port of managing 1.3 hole enlargements part in centre chamber is fixed with fixed disk 2.6 on the outer guide, the inward flange of fixed disk 2.6 axially is provided with outer guide 2.8 on the outer guide, fixed disk 2.3 and outer guide lower fixed disk 2.5 on the guide rail in being fixed with respectively up and down of outer guide 2.8, fixed disk 2.3 inward flanges guide rail 2.7 and interior guide rail lower fixed disk 2.4 in having vertically on interior guide rail; Outer guide 2.8 outsides below fixed disk on the outer guide 2.6 are provided with ring type buoyancy aid 2.9.1, this ring type buoyancy aid 2.9.1 inboard upwards is fixed with retaining liquid pipe 2.9.3 by connecting rod 2.9.2, retaining liquid pipe 2.9.3 is on fixed disk on the inner orbit 2.3 and the outside track between the fixed disk 2.6, above fixed disk on the inner orbit 2.3, be provided with slot type buoyancy aid 2.2.1, this slot type buoyancy aid 2.2.1 bottom has to be run through lower fixed disk on the inner orbit and manages the mobile pipe 2.2.2 of 1.3 bottoms to centre chamber, and the top radial distribution several and the mozzle that moves pipe 2.2.2 conducting.
Such scheme also comprises:
Be fixed with the pipe (2.1) of collaborating upwards symmetrical and connection T-shape post chamber on fixed disk on the outer guide, the pipe top of collaborating is provided with pore.On the kettle wall, also be provided with heat exchange jacket, between kettle 1.2 tops and bottom and centre chamber's pipe 1.3, set up isocon and control valve.
Effect of the present utility model: 1. be meant two or more mutual undissolved liquid between the non-intersolubility liquid of present technique indication. present technique can make between the non-intersolubility liquid (or non-reaction dissolvent) that participates in reaction (perhaps in the course of reaction newly-generated liquid or solid) moment Forced Mixing even, and overcome during the whole service natural separation between them continually strengthen and deepen this mixing evenly; The reaction present technique that participates in for solid can be earlier transfers solid and certain specific liquid the slurry form of suspension to by stirring, present technique is equal to single liquid for the slurry adaptability that suspends. so present technique can reach the purpose of quick mixing equally to non-mutually soluble liquids and solid, overcomes natural separation between them simultaneously and continually strengthens during whole service and deepen the even of this mixing.
2. the self-adjustable of present technique indication is meant; when participating in the flow of a certain material (or mixture of different mixed styles) that mixes at the property settings of the material of wanting to mix; only need disposable setting and equipment that other adjusting is made by present technique is finished voluntarily, that just can guarantee to mix carries out voluntarily.
3. present technique has solved the problem of existing reactor purposes restriction, and the chemical reaction characteristics between the organic matter, between organic matter and the inorganic matter are: reactive species is numerous, there is side reaction in slow, a lot of reaction of reaction speed.Therefore exist during actual production because of the inhomogeneous of exposure concentration between the material and the long side reaction product that is caused of reaction time that causes therefrom too much, it is even unqualified to make that product quality descends.Although the producer who has is with accelerating whole mixing speed, and adopt the feed liquor liquid distributor to overcome this situation, improve and be very limited and be difficult to overcome natural separation between them, and some product and the natural separation between them.The good product quality that present technique makes production; And because the shortening energy savings of mixing afterreaction time.
Description of drawings
Accompanying drawing 1 is a kind of specific embodiment structure chart of the present utility model;
Accompanying drawing 2 is vertical views of mobile tube portion;
The vertical view of accompanying drawing 3 ring type buoyancy aids part.
The specific embodiment:
With reference to accompanying drawing 1, kettle 1.2 outer setting feed inlet and outlets, drive motors.Kettle inside is provided with V shape agitator 1.1 structures, and design feature is with coaxial 2 forks of stirring motor or pitches structure more; Bottom or other positions of each fork have bifurcated, are used for the stirring of each material in the reactor.Below slot type buoyancy aid 2.2.1, have centre chamber's pipe 1.3 so that the member work of complex reaction device inside.The design feature of member 1.3 is vertical at the center of reactor, and its cross section is circular or other geometries and cross section, differing heights place can be different; It is exposed at the interface that is partly with of shell of reactor, and inside is used to install the adjustment member member, and cooperating.
Adjustment member is by the pipe 2.1 of collaborating, slot type buoyancy aid 2.2.1, the mobile pipe 2.2.2 of buoyancy aid, fixed disk 2.3 on the interior guide rail, interior guide rail lower fixed disk 2.4, outer guide lower fixed disk 2.5, fixed disk 2.6 on the outer guide, interior guide rail 2.7, outer guide 2.8, ring type buoyancy aid 2.9.1, connecting rod 2.9.2, retaining liquid pipe 2.9.3 forms. and wherein: the pipe 2.1 of collaborating is fixed on the outer guide on the fixed disk for the lower end and passes 2.6 and ventilate below it, the pore that communicates with the reactor gas phase is left in the upper end. and its effect is the ring type buoyancy aid 2.9.1 that guarantees to be in the reactor center chamber pipe 1.3, the pressure of its gas phase is identical with the interior gaseous pressure of the mobile pipe 2.2.2 of buoyancy aid when sliding up and down, so that make the inside and outside liquid level of the mobile pipe 2.2.2 of buoyancy aid identical. slot type buoyancy aid 2.2.1, the mobile pipe 2.2.2 of buoyancy aid welds together, its structure sees that the design feature of accompanying drawing 2. slot type buoyancy aid 2.2.1 is the airtight buoyancy tank that is welded on the upper end of moving pipe 2.2.2, its geometry guarantees its center of gravity, the buoyancy point drops on and moves the center, upper end of managing 2.2.2. and leave groove in the middle of its upper and lower covers and communicate with mobile pipe 2.2.2. its effect is that the low density liquid of reactor inner top when opening high-speed centrifugal slush pump 3.1 enters in the mobile pipe 2.2.2 along groove, fixed disk 2.3 on the interior guide rail, interior guide rail lower fixed disk 2.4 is discoid and is connected as a single entity by interior guide rail 2.7. and interior guide rail 2.7 is fixed disk 2.3 on the guide rail in being distributed on, cylinder on interior guide rail lower fixed disk 2.4 peripheries, it and move between the outer wall of pipe 2.2.2 and leave appropriate gap. its effect is to guarantee to move pipe 2.2.2 easy on and off to slide, a spot of liquid is flow through by fixed disk on the interior guide rail 2.3 and the outer wall gap of moving pipe 2.2.2. outer guide lower fixed disk 2.5, fixed disk 2.6 on the outer guide, the structure of outer guide 2.8 and effect and interior guide rail are similar, it is guaranteed to keep off liquid pipe 2.9.3 and moves along outer guide 2.8 easy on and off. ring type buoyancy aid 2.9.1, connecting rod 2.9.2, retaining liquid pipe 2.9.3 welds together, its structure sees that accompanying drawing 3. ring type buoyancy aid 2.9.1 design features are for being connected as a single entity by connecting rod 2.9.2 and retaining liquid pipe 2.9.3, be an airtight circular ring type body structure. its effect is that the variation along with liquid levels in the reactor center chamber pipe 1.3 drives retaining liquid pipe 2.9.3 by connecting rod 2.9.2 and moves up and down. connecting rod 2.9.2 is between the guide rail of outer guide 2.8. the design feature of retaining liquid pipe 2.9.3 is cylindric, effect be by move up and down change be in the fluid passage cross-sectional sizes between the fixed disk 2.6 on fixed disk 2.3 and the outer guide on the guide rail.
The operation principle of this equipment: guarantee during design present technique equipment: 1, the buoyancy of slot type buoyancy aid 2.2.1, ring type buoyancy aid 2.9.1 is greater than its gravity; 2, flow into the fluid flow Q that moves pipe 2.2.2 by slot type buoyancy aid 2.2.1 groove
1Add by the fluid flow Q between the outer guide 2.8 the first half guide rails between the fixed disk 2.6 on fixed disk 2.3 and the outer guide on the guide rail in being in
2The flow Q that is a bit larger tham high-speed centrifugal slush pump 3.1
3And Q
3Greater than Q
1Open during work that V shape stirs 1.1, high-speed centrifugal slush pump 3.1 and gateway valve thereof, or reactor control valve 3.2 or pump flow divider 3.3, (or only opening 3.1) are because of Q
3Greater than Q
1Thereby the liquid level decline of moving in pipe 2.2.2 and the reactor center chamber pipe 1.3 makes ring type buoyancy aid 2.9.1, the connecting rod 2.9.2, the retaining liquid pipe 2.9.3 that weld together and then descend while Q
2Strengthen Q
2Strengthen prevention decline conversely, thereby reach the balance in liquid level somewhere in moving pipe 2.2.2.If open reactor control valve 3.2. or pump flow divider 3.3 this moment, perhaps by charging valve 3.6 liquid make-up in reactor, in like manner Q
2To reduce corresponding flow, reach the balance of liquid level.So just make that the liquid that enters high-speed centrifugal slush pump 3.1 is heavy liquid of minimum liquid of reactor inner top density and bottom density or the mixture that passes through charging valve 3.6. additional liquid in reactor.They are quick Forced Mixing under the effect of the impeller of high-speed centrifugal slush pump 3.1 high speed rotating.Open the mixing that big pump flow divider 3.3 is strengthened difficult mixing material according to the difference of material properties; Also can open the mixing that big reactor control valve 3.2 comes liquid in the enhanced reactor; Liquid moment of replenishing in reactor by charging valve 3.6 enters the impeller district and obtains Forced Mixing.Reaction for the solid participation, earlier solid and certain specific liquid are added in the reactor, liquid level is controlled at centre chamber and manages below 1.3 tops, only open V shape and stir 1.1 this moment, and closing high-speed centrifugal mud pump 3.1, make solid and certain specific liquid transfer the slurry form of suspension to by stirring, present technique is equal to single liquid for the slurry adaptability that suspends, so slurry is identical with the mixing principle between non-intersolubility liquid recited above with the mixing principle of other non-intersolubility liquid.
Find out that by the foregoing description it is adjusting part in kettle inside that present technique is mainly improved, can dispose according to actual needs for the outside of kettle and have the chuck of regulating temperature, add discharging opening, thermometric, window etc.
Claims (3)
1. a self-adjusting quick reaction kettle comprises kettle and the feed inlet and outlet, the drive motors that are arranged on the kettle, and is arranged on the agitator in the kettle, it is characterized in that: agitator is that V shape stirs (1.1) structure; Upwards be fixed with centre chamber's pipe (1.3) at kettle (1.2) inner bottom part, the cross section forms "T"-shaped post chamber after centre chamber's pipe (1.3) top hole enlargement, upper port in centre chamber's pipe (1.3) hole enlargement part is fixed with fixed disk on the outer guide (2.6), the inward flange of fixed disk on the outer guide (2.6) axially is provided with outer guide (2.8), fixed disk (2.3) and outer guide lower fixed disk (2.5) on the guide rail in being fixed with respectively up and down of outer guide (2.8), fixed disk on interior guide rail (2.3) inward flange is vertically to having interior guide rail (2.7) and interior guide rail lower fixed disk (2.4); Outer guide (2.8) outside of fixed disk on outer guide (2.6) below is provided with ring type buoyancy aid (2.9.1), this ring type buoyancy aid (2.9.1) is inboard upwards to be fixed with retaining liquid pipe (2.9.3) by connecting rod (2.9.2), and retaining liquid pipe (2.9.3) is positioned at the below of fixed disk on the inner orbit (2.3); Fixed disk on interior guide rail (2.3) top is provided with slot type buoyancy aid (2.2.1), this slot type buoyancy aid (2.2.1) bottom has to be run through lower fixed disk on the inner orbit and manages the mobile pipe (2.2.2) of (1.3) bottom to centre chamber, and the top radial distribution several and the mozzle that moves pipe (2.2.2) conducting.
2. self-adjusting quick reaction kettle according to claim 1 is characterized in that: be fixed with the pipe (2.1) of collaborating upwards symmetrical and connection T-shape post chamber on fixed disk on the outer guide, the pipe top of collaborating is provided with pore.
3. self-adjusting quick reaction kettle according to claim 1 and 2 is characterized in that: also be provided with heat exchange jacket on the kettle wall, set up isocon and control valve between kettle (1.2) top and bottom and centre chamber's pipe (1.3).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009200243949U CN201454525U (en) | 2009-03-27 | 2009-03-27 | Self-adjusting quick reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009200243949U CN201454525U (en) | 2009-03-27 | 2009-03-27 | Self-adjusting quick reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201454525U true CN201454525U (en) | 2010-05-12 |
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ID=42381870
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009200243949U Expired - Lifetime CN201454525U (en) | 2009-03-27 | 2009-03-27 | Self-adjusting quick reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201454525U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101518724B (en) * | 2009-03-27 | 2012-01-11 | 张新军 | Self-adjusting quick reaction kettle |
| CN106000243A (en) * | 2016-06-14 | 2016-10-12 | 李良军 | Low-rotation-speed multifunctional stirring device and integrated multistage pressurizer thereof |
| CN116492950A (en) * | 2023-06-29 | 2023-07-28 | 江苏福赛乙德药业有限公司 | Microchannel reactor structure |
-
2009
- 2009-03-27 CN CN2009200243949U patent/CN201454525U/en not_active Expired - Lifetime
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101518724B (en) * | 2009-03-27 | 2012-01-11 | 张新军 | Self-adjusting quick reaction kettle |
| CN106000243A (en) * | 2016-06-14 | 2016-10-12 | 李良军 | Low-rotation-speed multifunctional stirring device and integrated multistage pressurizer thereof |
| CN116492950A (en) * | 2023-06-29 | 2023-07-28 | 江苏福赛乙德药业有限公司 | Microchannel reactor structure |
| CN116492950B (en) * | 2023-06-29 | 2023-10-20 | 江苏福赛乙德药业有限公司 | Microchannel reactor structure |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| AV01 | Patent right actively abandoned |
Granted publication date: 20100512 Effective date of abandoning: 20090327 |