CN201358327Y - Efficient melt electrostatic spinning device capable of realizing continuous production - Google Patents

Efficient melt electrostatic spinning device capable of realizing continuous production Download PDF

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Publication number
CN201358327Y
CN201358327Y CNU2009201058273U CN200920105827U CN201358327Y CN 201358327 Y CN201358327 Y CN 201358327Y CN U2009201058273 U CNU2009201058273 U CN U2009201058273U CN 200920105827 U CN200920105827 U CN 200920105827U CN 201358327 Y CN201358327 Y CN 201358327Y
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China
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electrostatic spinning
reel
efficient
shower nozzle
spinning
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Expired - Lifetime
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CNU2009201058273U
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Chinese (zh)
Inventor
杨卫民
邓荣坚
刘勇
丁玉梅
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Beijing University of Chemical Technology
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Beijing University of Chemical Technology
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Abstract

The utility model discloses an efficient melt electrostatic spinning device capable of realizing continuous production, which belongs to spinning field and comprises a precision extrusion forming machine, a spinning mould head, an efficient nozzle, an electrostatic generator and a receiver device, wherein the precision extrusion forming machine is in bolt connection with the spinning mould head, the efficient nozzle is connected with ground, the winding drum of the receiver device is connected with the anode of the high voltage electrostatic generator through a metal bearing, the winding drum of the receiver is made of conductive material and the bracket of the winding drum is made of insulation material, the belt of the transmission mechanism of the winding drum is made of insulation material, the winding drum of the receiver device is provided with a lifting device , the spinning mould head is in conical tight fit with the efficient nozzle, a plurality of planes are cut off from the conical surface of the efficient nozzle evenly. The utility model relates to melt electrostatic spinning and avoids problems caused by the use of solvent, and greatly improves the efficiency of electrostatic spinning through the efficient nozzle.

Description

But a kind of quantity-produced high-efficiency melt electrostatic spinning device
Technical field
The utility model relates to a kind of electrostatic spinning apparatus, is particularly suitable for the serialization production of melt electrostatic spinning, belongs to the spinning field.
Background technology
Electrospinning process has been acknowledged as the simplest effective method of preparation nanofiber, and existing at present 30 multiple polymers successfully make superfine fibre by the method, and minimum diameter reaches tens nanometers.About the result of study of electrostatic spinning, pertinent literature all was index in recent years increases, yet electrostatic spinning technique is found to more than the 100 year present history from it, also rests on breadboard conceptual phase all the time, does not move towards the industrialization.
The major obstacle that hinders electrostatic spinning technique industrialization paces has two: the one, and electrostatic spinning efficient is too low.Though the existing many reports of patent about the electrostatic spinning apparatus produced in batches, but these devices all are at the solution electrostatic spinning, and solution electrostatic spinning process has 90% solution all to evaporate with the form of solvent, and this is the not high immediate cause of solution electrostatic spinning efficient.The 2nd, the research about electrostatic spinning at present concentrates on solution electrostatic spinning aspect mostly, and the solution electrostatic spinning a series of problem occurs because will use solvent: as the recovery problem of solvent; Be applied to the safety problem of biomedicine field; Some polymer such as polypropylene and polyethylene at room temperature can not find the appropriate solvent wiring solution-forming; The evaporation of solvent causes fiber surface rough, even defective occurs; The use of expensive solvent can increase cost; Fine spinneret orifice stops up easily, and influence is produced or the like continuously.The use of solvent is that electrostatic spinning technique is difficult to industrialized basic reason.
The utility model content
But a kind of quantity-produced high-efficiency melt electrostatic spinning device that the utility model proposes does not need to use solvent to carry out spinning, thereby has avoided using solvent and the problem that occurs; The melt of melt spinning process 100% all is converted into product, realized zero loss, improved the efficient of electrostatic spinning greatly, each efficient shower nozzle of spinning process can both produce the melt jet stream of multiply, thereby has further increased substantially the efficient of melt electrostatic spinning.The utility model has solved industrialized two major obstacles of obstruction electrostatic spinning technique, has promoted the industrialized paces of electrostatic spinning technique greatly.
But the utility model provides a kind of quantity-produced high-efficiency melt electrostatic spinning device, and it comprises precision extrusion molding machine that extrusion capacity can accurate control, is evenly equipped with the spray silk die head of a plurality of spinneret orifices, can makes injection stream be divided into the Height Adjustable receiving system of the efficient shower nozzle of multiply, the HV generator with anodal output and reel etc.The precision extrusion molding machine adopts bolt to be connected with spray silk die head, efficient shower nozzle adopts conical surface tight fit to be connected with spray silk die head, receiving system is made up of reel and tape handler etc., the reel of receiving system has lowering or hoisting gear, be used for the adjusting of its height, reel can be for convenience detach, is easy to change reel after silk twines completely.
Precision extrusion molding machine in the utility model can be single screw extrusion machine or double screw extruder or multi-screw extruder.
The reel lowering or hoisting gear of receiving system can be screw mechanism or pneumatic mechanism or hydraulic mechanism.
For fear of the interference of high-pressure electrostatic to the precision extrusion molding machine, this device adopts inverted electric field promptly, efficiently shower nozzle ground connection, so all unnecessary electric charges by the electrostatic field generation all can flow to the earth rapidly, has protected precision extrusion molding machine and all sensing elements that spray the silk die head such as sensor etc.; The reel of receiving system is a conductive material, it is connected with the positive pole of HV generator by metal bearing, the support and the used belt of tape handler that support reel all are insulating materials, the motor of tape handler and the reel segment distance of being separated by, thus the influence of high-voltage electrostatic field avoided to motor.
The used precision extrusion molding machine of the utility model, it is extruded flow and can accurate control, and minimum speed can be controlled at 0.5r/min, thereby has guaranteed the stability of flow of spray silk die head.Be evenly equipped with a lot of spinneret orifices on the base plate of spray silk die head, the minute aperture of these spinneret orifices and general spray silk die head is different, and its diameter can be greater than 2mm, thereby has reduced difficulty of processing greatly.Spinneret orifice adopts conical surface tight fit to be connected with efficient shower nozzle, owing to cut several planes equably on the mating surface of efficient shower nozzle and spinneret orifice, melt can flow to the spray screw tap face of efficient shower nozzle equably by these fit clearances, just can form the melt jet stream of multiply under the effect of electrostatic field.Efficient shower nozzle can be one or more, and the spray silk unit of being made up of a plurality of efficient shower nozzles can improve the efficient of electrostatic spinning significantly.
But a kind of quantity-produced high-efficiency melt electrostatic spinning device that the utility model proposes, electrostatic spinning technique be used for quantity-produced Polymer Processing equipment precision extrusion molding machine and combine, realized the continuous production of melt electrostatic spinning technology, efficient is improved, for solid foundation has been established in the electrostatic spinning technique industrialization.
Description of drawings
But Fig. 1 a kind of quantity-produced high-efficiency melt electrostatic spinning device schematic diagram that is the utility model
But the assembly drawing of Fig. 2 to be the utility model a kind of quantity-produced high-efficiency melt electrostatic spinning device spray silk die head and efficient shower nozzle
But the axonometric drawing of the efficient shower nozzle of Fig. 3 a kind of quantity-produced high-efficiency melt electrostatic spinning device that is the utility model
Among the figure: 1-precision extrusion molding machine, 2-spray silk die head, the efficient shower nozzle of 3-, 4-HV generator, 5-receiving system.
The specific embodiment
The utility model is described in further detail below in conjunction with specific embodiment.
But a kind of quantity-produced high-efficiency melt electrostatic spinning device of the utility model comprises precision extrusion molding machine 1, spray silk die head 2, efficient shower nozzle 3, HV generator 4, receiving system 5, as shown in Figure 1, precision extrusion molding machine 1 adopts bolt to be connected with spray silk die head 2, efficient shower nozzle 3 adopts conical surface tight fit to be connected with spray silk die head 2, see Fig. 2, several planes have been cut equably on the efficient shower nozzle conical surface, see Fig. 3, receiving system 5 comprises reel and tape handler, reel can be for convenience detach, is easy to change after silk twines full reel.Efficient shower nozzle 3 ground connection, the reel of receiving system 5 is a conductive material, its height can be by screw mechanism or pneumatic mechanism or hydraulic mechanism adjusting, reel is connected by the positive pole of metal bearing with HV generator 4, the support and the used belt of tape handler that support reel all are insulating materials, the motor of tape handler and the reel segment distance of being separated by, thus the influence of high-voltage electrostatic field avoided to motor.
Embodiment:
The screw diameter of used precision extrusion molding machine 1 is in the present embodiment
Figure Y20092010582700051
Minimum speed 0.5r/min; Spray silk die head 2 is evenly equipped with 64 spinneret orifices, and orifice diameter is
Figure Y20092010582700052
The big end circle diameter of spray screw tap face of efficient shower nozzle 3 is
Figure Y20092010582700053
The maximum output voltage of HV generator 4 is+60kv; The drum diameter of receiving system 5 is
Figure Y20092010582700054
Distance between reel and the efficient shower nozzle is 10cm, and this distance is regulated by screw mechanism; Spinning material is PP, and molten the finger is 1500g/10min.Spinning step: earlier the barrel of precision extrusion molding machine 1 and spray silk die head 2 are heated to predetermined temperature, spray silk die head temperature is 250 ℃, complete fusion when making PP arrive spray silk die head, open the main motor and the feeding motor of precision extrusion molding machine 1 then, melt begins to carry toward spray silk die head 2, by the time after being evenly equipped with melt on the spray screw tap face of efficient shower nozzle 3, open the band driving motor of receiving system 5 again, open the power supply of HV generator 4 simultaneously, and till regulation voltage produced to the melt jet flow, output voltage was taken as 50kv in this embodiment.After the melt jet miscarriage was given birth to, the main motor and the feeding motor of precision extrusion molding machine 1 all will suitably be turned down, till spinning can be carried out smoothly continuously.Can produce the superfine fibre of diameter between 700nm~4 μ m by present embodiment, spinning efficiency is about 268g/h.

Claims (4)

1. but quantity-produced high-efficiency melt electrostatic spinning device, it is characterized in that, it comprises the precision extrusion molding machine, spray silk die head, efficient shower nozzle, electrostatic generator and receiving system, the precision extrusion molding machine adopts bolt to be connected with spray silk die head, efficient shower nozzle ground connection, the reel of receiving system is connected with the positive pole of HV generator by metal bearing, the reel of receiving system is a conductive material, the support of reel is an insulating materials, the used belt of the tape handler of reel is an insulating materials, the reel of receiving system has lowering or hoisting gear, and spray silk die head adopts conical surface tight fit with efficient shower nozzle, has cut several planes equably on the efficient shower nozzle conical surface.
2. but a kind of quantity-produced high-efficiency melt electrostatic spinning device according to claim 1 is characterized in that, efficient shower nozzle can be one or more.
3. but a kind of quantity-produced high-efficiency melt electrostatic spinning device according to claim 1 is characterized in that, the precision extrusion molding machine can be single screw extrusion machine or double screw extruder or multi-screw extruder.
4. but a kind of quantity-produced high-efficiency melt electrostatic spinning device according to claim 1 is characterized in that, the lowering or hoisting gear of the reel of receiving system can be screw mechanism or pneumatic mechanism or hydraulic mechanism.
CNU2009201058273U 2009-02-20 2009-02-20 Efficient melt electrostatic spinning device capable of realizing continuous production Expired - Lifetime CN201358327Y (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101871130A (en) * 2010-07-06 2010-10-27 北京化工大学 Novel straight-strut electrostatic spinning spray nozzle
CN101812733B (en) * 2009-02-20 2011-05-18 北京化工大学 Continuously-producing high-efficiency melt electrostatic spinning device
CN103065543A (en) * 2013-01-20 2013-04-24 青岛大学 Portable melt electrostatic spinning teaching demonstration device
CN103866404A (en) * 2014-04-09 2014-06-18 厦门大学 Spinning sprayer device for compound nano-fiber

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101812733B (en) * 2009-02-20 2011-05-18 北京化工大学 Continuously-producing high-efficiency melt electrostatic spinning device
CN101871130A (en) * 2010-07-06 2010-10-27 北京化工大学 Novel straight-strut electrostatic spinning spray nozzle
CN101871130B (en) * 2010-07-06 2011-08-10 北京化工大学 Novel straight-strut electrostatic spinning spray nozzle
CN103065543A (en) * 2013-01-20 2013-04-24 青岛大学 Portable melt electrostatic spinning teaching demonstration device
CN103866404A (en) * 2014-04-09 2014-06-18 厦门大学 Spinning sprayer device for compound nano-fiber

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AV01 Patent right actively abandoned

Granted publication date: 20091209

Effective date of abandoning: 20090220