CN201346457Y - Integrated gas-liquid reactor - Google Patents
Integrated gas-liquid reactor Download PDFInfo
- Publication number
- CN201346457Y CN201346457Y CNU2008201440210U CN200820144021U CN201346457Y CN 201346457 Y CN201346457 Y CN 201346457Y CN U2008201440210 U CNU2008201440210 U CN U2008201440210U CN 200820144021 U CN200820144021 U CN 200820144021U CN 201346457 Y CN201346457 Y CN 201346457Y
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- tank body
- reactor
- coiled pipe
- gas
- liquid
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Abstract
The utility model discloses an integrated gas-liquid reactor which comprises a reactor; the upper part of an upper cover is provided with a motor and a speed reducer; and the upper cover is further provided with a manhole, a cleaning port and a reaction liquid inlet. The lower part of the reactor is provided with a reactant outlet; and the upper part of one side of the reactor is provided with a reaction gas inlet and a pH meter interface. The lower part of one side of the reactor is provided with a coil tube inlet; the upper part of the other side of the reactor is provided with a temperature transmitter interface and a coil tube outlet; and the reactor is provided with a stirring paddle. The reactor is further provided with a coil tube; and the outer wall of the reactor is provided with a jacket along the circumstance. The utility model realizes the gas-liquid reaction, stirring, temperature rise and drop, pH value and other monitoring functions on the same device. The integrated gas-liquid reactor has compact structure, shortens the procedures, and realizes the automation of temperature control.
Description
Technical field
The utility model belongs to a kind of chemical reaction device, is specifically related to a kind of a kind of gas-liquid combined reaction device that monitoring functions such as gas liquid reaction, stirring, lifting temperature and pH value can be integrated.
Background technology
Often need carry out gas liquid reaction in the chemical reaction, in course of reaction, need operations such as stirring, heating, cooling.These operations need be finished or finish in certain sequence simultaneously, have caused tank body various like this, and floor space is big, the one-time investment height, and operating cost is also higher.Common gas-liquid reactor has bubbling bed, stirred tank circulation flow reactor etc. at present.In the gas-liquid reaction equipment of prior art, temperature, acid-base value are difficult for monitoring, and poor sealing, easily gas leakage.And heating finishes by a chuck often with cooling, needs cooling fluid and heat medium to exchange, and technical process prolongation has reduced equipment operating efficiency, is difficult to realize automation.
Summary of the invention
The utility model proposes for the shortcoming that overcomes the prior art existence, and its purpose is to provide a kind of gas-liquid combined reaction device.
The technical solution of the utility model is: a kind of gas-liquid combined reaction device comprises that retort, retort be made up of tank body and loam cake.Top at loam cake is provided with motor and speed reducer, also be provided with manhole, Butterworth Hatch and reaction liquid import last covering, be provided with the reactant outlet in the tank body bottom, be provided with reacting gas inlet and pH meter interface at tank body one upper lateral part, reacting gas inlet is connected with air inlet pipe.
At tank body one side lower part the coiled pipe import is set, is provided with the outlet of temperature transmitter interface and coiled pipe on the opposite side top of tank body, be provided with paddle in retort, paddle is connected with the output shaft of reductor.Also be provided with coiled pipe in retort, import is connected with coiled pipe in the lower end of coiled pipe, and outlet is connected with coiled pipe in the upper end of coiled pipe.
Outer wall at tank body is provided with chuck along circumference, in the bottom of chuck cooling water inlet is set, and in the both sides, top of chuck coolant outlet is set respectively.
Air inlet pipe is " L " type, forms a plurality of apertures side by side at the horizontal segment of air inlet pipe, air inlet pipe along inner tank wall vertically reach the bottom always, horizontal segment traverses tank base.
The utility model has realized that monitoring functions such as gas liquid reaction, stirring, lifting temperature and pH value finish on a device.Compact conformation has shortened operation.Temperature transmitter is installed in the reactor,, controls the heating and cooling time, realized temperature controlled automation by monitoring temperature.
Description of drawings
Fig. 1 is the structural representation of gas-liquid combined reaction device.
Wherein:
1 retort, 2 tank bodies
3 loam cakes, 4 motors
5 reductors, 6 manholes
The 8 reaction liquid imports of 7 Butterworth Hatch
9 reactants export 10 reacting gas inlets
11 air inlet pipe, 12 pH meter interfaces
13 temperature transmitter interfaces, 14 paddles
The outlet of 15 coiled pipe imports, 16 coiled pipes
17 coiled pipes, 18 blades
20 chucks, 21 cooling water inlets
22 cold but water out 23 apertures that go
The specific embodiment
Below, in conjunction with the accompanying drawings and embodiments a kind of gas-liquid combined reaction device of the present utility model is elaborated:
As shown in Figure 1, a kind of gas-liquid combined reaction device comprises that retort 1, retort 1 be made up of tank body 2 and loam cake 3, is provided with motor 4 and reductor 5 on the top of loam cake 3, also is provided with manhole 6, Butterworth Hatch 7 and reaction liquid import 8 on loam cake 3.Be provided with reactant outlet 9 in tank body 2 bottoms, being provided with reacting gas inlet 10, reacting gas inlet 10 and air inlet pipe 11 at tank body 2 one upper lateral parts is connected, air inlet pipe 11 is " L " type, horizontal segment in air inlet pipe 11 forms a plurality of apertures 23 side by side, and reacting gas is entered in the retort 1 by aperture 23.Air inlet pipe 11 along tank body 2 inwalls vertically reach the bottom always, horizontal segment traverses tank body 2 bottoms.
At tank body 2 one upper lateral parts pH meter interface 12 is set also, coiled pipe import 15 is set, be provided with temperature transmitter interface 13 and coiled pipe outlet 16 on the opposite side top of tank body 2 at tank body 2 one side lower parts.Be provided with paddle 14 in retort 1, paddle 14 is connected with the output shaft of reductor 5, and paddle 14 has a plurality of blades 18.Also be provided with coiled pipe 17 in retort 1, the lower end of coiled pipe 17 is connected with coiled pipe import 15, and the upper end of coiled pipe 17 is connected with coiled pipe outlet 16.For the endothermic reaction, can feed conduction oil or steam in the coiled pipe 17, so that improve reaction temperature, fast reaction speed.
Middle part, bottom at tank body 2 outer walls are provided with chuck 20 along circumference, in the bottom of chuck 20 cooling water inlet 21 are set, and in the both sides, top of chuck 20 coolant outlet 22 are set respectively.For exothermic reaction, can feed cooling water in the chuck 20, so that the cooling reactant.
The course of work of the present utility model is:
Use the utility model and can realize the reaction of the mixing material and the carbon dioxide of calcium glycerophosphate and calcium hydroxide well, existing is the example explanation course of work with above-mentioned reaction:
At first, to retort 1, add calcium glycerophosphate and calcium hydroxide [Ca (OH) from reaction liquid import 8
2] mixing material, feed carbon dioxide (CO from reacting gas inlet 10
2) gas, motor 4 drives paddle 14 rotations by reductor 5, stirs.Simultaneously, make, use in retort 1 and feed CO by the acid-base value in the pH value instrumentation quantitative response system that is connected pH value interface 12 places
2Control the pH value, reach the value that needs.At this moment, carbon dioxide and calcium hydroxide reaction generate calcium bicarbonate [Ca (HCO)
2] and water (H
2O).For being decomposed, calcium bicarbonate generates calcium carbonate (CaCO
3) precipitation, need heat system, temperature signal be passed to magnetic valve (not shown) on the pipeline that is connected with coiled pipe import 15 by the temperature transmitter that is connected temperature transmitter interface 13, conduction oil or steam are opened, fed to magnetic valve, reaction is heated, generate precipitation of calcium carbonate.Because calcium glycerophosphate does not dissolve when high temperature, need the system cools cooling at this moment, is fed cooling water in the chuck 20, make the calcium glycerophosphate dissolving.
After question response is finished, carry out discharging by reactant outlet 9.Remove calcium carbonate after filtration, do not contained the phosphoglycerol calcium solution of calcium hydroxide.
Utilize the utility model device to pass through CO
2Gas is removed the Ca (OH) in the reactant liquor
2, the result shows: at short notice the calcium hydroxide in the solution is removed fully.Because temperature and the control of pH value is relatively good, other materials in the middle of the reactant liquor is not produced harmful effect.
The utility model has realized that monitoring functions such as gas liquid reaction, stirring, lifting temperature and pH value finish on a device.Compact conformation has shortened operation.Temperature transmitter is installed in the reactor,, controls the heating and cooling time, realized temperature controlled automation by monitoring temperature.
Claims (2)
1, a kind of gas-liquid combined reaction device, comprise retort (1), retort (1) is made up of tank body (2) and loam cake (3), it is characterized in that: be provided with motor (4) and reductor (5) on the top of loam cake (3), on loam cake (3), also be provided with manhole (6), Butterworth Hatch (7) and reaction liquid import (8), be provided with reactant outlet (9) in tank body (2) bottom, be provided with reacting gas inlet (10) and pH meter interface (12) at tank body (2) one upper lateral parts, reacting gas inlet (10) is connected with air inlet pipe (11), at tank body (2) one side lower parts coiled pipe import (15) is set, be provided with temperature transmitter interface (13) and coiled pipe outlet (16) on the opposite side top of tank body (2), in retort (1), be provided with paddle (14), paddle (14) is connected with the output shaft of reductor (5), in retort (1), also be provided with coiled pipe (17), the lower end of coiled pipe (17) is connected with coiled pipe import (15), the upper end of coiled pipe (17) is connected with coiled pipe outlet (16), outer wall at tank body (2) is provided with chuck (20) along circumference, in the bottom of chuck (20) cooling water inlet (21) is set, coolant outlet (22) is set respectively in the both sides, top of chuck (20).
2, a kind of gas-liquid combined reaction device according to claim 1, it is characterized in that: air inlet pipe (11) is " L " type, horizontal segment in air inlet pipe (11) forms a plurality of apertures (23) side by side, air inlet pipe (11) along tank body (2) inwall vertically reach the bottom always, horizontal segment traverses tank body (2) bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008201440210U CN201346457Y (en) | 2008-12-08 | 2008-12-08 | Integrated gas-liquid reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008201440210U CN201346457Y (en) | 2008-12-08 | 2008-12-08 | Integrated gas-liquid reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201346457Y true CN201346457Y (en) | 2009-11-18 |
Family
ID=41365936
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNU2008201440210U Expired - Lifetime CN201346457Y (en) | 2008-12-08 | 2008-12-08 | Integrated gas-liquid reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201346457Y (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105396530A (en) * | 2014-09-12 | 2016-03-16 | 天津法莫西医药科技有限公司 | Biochemical reaction apparatus for preparing biological preparations |
| CN108277362A (en) * | 2018-03-15 | 2018-07-13 | 洛阳万基铝加工有限公司 | A kind of molten aluminum degasification tank rotor feeder |
| CN112774495A (en) * | 2020-12-02 | 2021-05-11 | 安徽扬天金塑新能源装备股份公司 | Continuous efficient vapour-liquid mixer |
| CN114849623A (en) * | 2022-04-18 | 2022-08-05 | 黄迎春 | Liquid phase reaction container |
-
2008
- 2008-12-08 CN CNU2008201440210U patent/CN201346457Y/en not_active Expired - Lifetime
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105396530A (en) * | 2014-09-12 | 2016-03-16 | 天津法莫西医药科技有限公司 | Biochemical reaction apparatus for preparing biological preparations |
| CN108277362A (en) * | 2018-03-15 | 2018-07-13 | 洛阳万基铝加工有限公司 | A kind of molten aluminum degasification tank rotor feeder |
| CN112774495A (en) * | 2020-12-02 | 2021-05-11 | 安徽扬天金塑新能源装备股份公司 | Continuous efficient vapour-liquid mixer |
| CN114849623A (en) * | 2022-04-18 | 2022-08-05 | 黄迎春 | Liquid phase reaction container |
| CN114849623B (en) * | 2022-04-18 | 2024-06-07 | 上海齐达重型装备有限公司 | Liquid phase reaction vessel |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: TIANJIN CHANGLU HUAXIN CHEMICAL INDUSTRY CO., LTD. Free format text: FORMER OWNER: RESEARCH INSTITUTE OF PHYSICAL AND CHEMICAL ENGINEERING OF NUCLEAR INDUSTRY HUAH Effective date: 20150515 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 300384 NANKAI, TIANJIN TO: 300280 BINHAI NEW DISTRICT, TIANJIN |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20150515 Address after: Comprehensive service area Nangang Industrial Zone Development Zone 300280 Tianjin Binhai New Area Office Building second floor D building site 216 Patentee after: Huahe New-Technology Development Company, Research Institute of Physical and Chemical Engineering of Nuclear Industry Address before: The 300384 Tianjin City Huayuan Industrial Zone Development Road six No. 6 Haitai green industry base building J room 104 Patentee before: Huahe New Technology Development Company, Research Institute of Physical and Chemical Engineering of Nuclear Industry |
|
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20091118 |