CN201346405Y - Multi-overflow ring shaped column plate - Google Patents

Multi-overflow ring shaped column plate Download PDF

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Publication number
CN201346405Y
CN201346405Y CNU2008201695243U CN200820169524U CN201346405Y CN 201346405 Y CN201346405 Y CN 201346405Y CN U2008201695243 U CNU2008201695243 U CN U2008201695243U CN 200820169524 U CN200820169524 U CN 200820169524U CN 201346405 Y CN201346405 Y CN 201346405Y
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CN
China
Prior art keywords
column plate
liquid
tower
tray
tower tray
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Expired - Fee Related
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CNU2008201695243U
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Chinese (zh)
Inventor
顾燕新
唐清建
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Hangzhou Hangyang Co Ltd
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Hangzhou Hangyang Co Ltd
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Priority to CNU2008201695243U priority Critical patent/CN201346405Y/en
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Publication of CN201346405Y publication Critical patent/CN201346405Y/en
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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model relates to a multi-overflow ring shaped column plate, comprising at least a circular tray. The center of the circular tray is provided with a center support tube and forms a ring shaped tray. The ring shaped tray is cut into sector segments equally according to the number of overflow. Each sector segment is also cut into three blocks of a liquid pan, a sector tray and a liquid falling area. The liquid falling area of the next layer column plate is positioned right below the liquid falling area of the ring shaped tray. The liquid falling area is connected with the liquid pan of the next layer column plate through a slope. The middle of the center support tube of the ring shaped tray is provided with a circular ring shaped liquid communicating vessel. The bottom surface of the communicating vessel has the same level with the bottom surface of the liquid pan; the top surface is higher than the maximum liquid level of the liquid pan by about 50mm; and the external surface is communicated with the liquid falling tube. The multi-overflow ring shaped column plate has the advantages that the column plate improves the efficiency of the column plate, reduces the differential pressure of the column plate, decreases the separation energy consumption, lessens the size of the rectifying tower, reduces the equipment cost, meets the high requirements for the separation property of the column plate in the modern separation process and the like.

Description

Multi-overflow circle tower plate
Invention field
The utility model relates to a kind of core component of plate distillation column---column plate, belong to the vapor-liquid separating device technical field.
Background technology
In the work of petrochemical industry was produced, distillation operation affected the energy consumption of petrochemical industry industry significantly.For example the U.S.'s about 40,000 rectifying column consumed energies in the whole nation in 1989 account for 41.2% of petrochemical industry total energy consumption, account for 2.99% in the national total energy consumption.And plate distillation column accounts for very big proportion in the rectifying column, so the small raising of plate distillation column efficient just can produce huge economic benefit.The research of current rectifying mainly comprises two aspects: distillation process simulation and rectifying device design.The main task of rectifying simulation is exactly to instruct the rectifying device design in theory.Introduce the relation of point efficiency on plate efficiency in the rectifying simulation and the column plate below, and then how to instruct the design column plate.
Following hypothesis is used in the derivation of point efficiency relation on plate efficiency and the column plate.
Plug flow model: consider a two-component fractionation tower, wherein column plate is the certain rectangle column plate of length for every layer, and hypothesis liquid carries out plug-flow on column plate.
Lewis situation 1: suppose that into the gas of column plate mixes fully, promptly column plate gas component everywhere is identical, sees shown in Figure 1.
Lewis situation 2: suppose that gas is unmixed fully between the column plate, promptly gas leaves that the form with piston flow enters the last layer column plate after the liquid on the column plate, and liquid flow direction is identical on all column plates, sees shown in Figure 2.
Lewis situation 3: suppose that gas is unmixed fully between the column plate, promptly gas leaves that the form with piston flow enters the last layer column plate after the liquid on the column plate, but liquid flow direction is opposite on adjacent two blocks of column plates, sees shown in Figure 3.
The hypothesis gas-liquid phase equilibrium is a linear relation in addition in derivation, promptly
Y=mx+b m---gas-liquid phase equilibrium slope y---gas phase molar fraction
X---liquid phase molar fraction E OG---Murphree gas phase rectifiying plate point efficiency
E MV---Murphree gas phase rectifiying plate efficient ζ---plate efficiency synergistic factor, ζ=E MV/ E OG
L---liquid molar flow rate on the column plate, mol/h V---gas molar flow rate on the column plate, mol/h
The slope of R---operating line, R=L/V λ---the stripping factor, λ=m/R
Concrete theoretical derivation can be seen the 8th chapter content in " the rectifying simulation " that professor Song Haihua writes.
Be that a plate efficiency synergistic factor ζ is with point efficiency E below 0GThe numerical value tables that under different Lewis situations, changes with the stripping factor lambda.
Though the aforementioned calculation model has used several hypothesis, do not lose generality, how more it indicated good utilisation column plate top liquids and gases component difference and improved plate efficiency.But in addition this principle body by two kinds of fluids in the design of heat exchanger adopt adverse current and and when flowing the discrepant characteristics of mean temperature difference understand.
The research and development of column plate now, concentrate on greatly and improve on the column plate liquid flow condition, as pilot hole is set, adopt better circulation type tower plate of flow pattern or the like, and the reflection plate efficiency increases sharply 10%~20% quickly on so slight many data of change and the patent, plate pressure drop reduces 5%~15%, even more.Regrettably Jue Dabufen research and development person does not explain theoretically fully, and in fact is that so slight improvement makes on the column plate liquid flow form near plug-flow, has produced plate efficiency synergistic factor ζ.Yet how to maximize synergistic factor, that be exactly the column plate of design by it more near Lewis situation 2, the efficient of column plate can maximize like this, the efficient of veneer is above 1 also being normal.
The design guidance principle:
(1) liquid adopts piston flow.
(2) gas adopts piston flow.
(3) the liquid flow direction unanimity of levels column plate.
Summary of the invention
The purpose of this utility model is to overcome the deficiency that prior art exists, and maximum these characteristics of the column plate synergistic factor that a kind of Lewis of utilization situation 2 is provided instruct the design column plate and then improve plate efficiency, the pressure that reduces column plate falls, reduce separating energy consumption, dwindle the rectifying column size, thereby reduce equipment cost and satisfy the multi-overflow circle tower plate of modern separation process column plate separating property high request.
The purpose of this utility model is to be achieved through the following technical solutions, which comprises at least a circular tower tray, the center of described circular tower tray is provided with a central support tube and constitutes an annular tower tray, cut into secter pat according to overflow number equal portions on this annular tower tray, every part of secter pat is cut into seal pot, fan-shaped tower tray again and falls three of liquid zones.
Described annular tower tray the liquid zone that falls for one deck column plate down falls under the liquid zone, the described liquid zone that falls joins by the seal pot of a slope with following one deck column plate.
Is provided with an annular fluid connection device in the middle of the central support tube of described annular tower tray, the bottom surface of this linker and seal pot bottom surface flush, and end face is than in the seal pot about maximum level height~50mm, and lateral surface and downspout are communicated with.
Be provided with an annular gas linker in the middle of the central support tube of described annular tower tray, the bottom surface of this linker is the end face of fluid connection device, and the end face of linker flushes with the upper strata column plate, and the gas compartment of lateral surface and the different sectors of column plate is communicated with.
Pipe and outer tube in the central support tube of described annular tower tray is divided into; Seal at the top of interior pipe, communicates at the bottom of bottom and the tower, forms an annular region in the middle of outer tube and the interior pipe annular fluid connection device and annular gas linker are set.
The central support tube cross-sectional area of described annular tower tray accounts for 1/4~1/16 of whole tower tray cross-sectional area.
The utility model belongs to a kind of big improvement to prior art, and it has the raising plate efficiency, and the pressure that reduces column plate falls, reduce separating energy consumption, dwindle the rectifying column size, can reduce equipment cost, can satisfy modern separation process characteristics such as column plate separating property high requests.
Description of drawings
Fig. 1 is the illustraton of model of Lewis situation 1.
Fig. 2 is the illustraton of model of Lewis situation 2.
Fig. 3 is the illustraton of model of Lewis situation 3.
Fig. 4 is a structural representation of the present utility model.
Fig. 5 is the A-A view of Fig. 4, and wherein: I is interior pipe; II is the gas linker; III is the fluid connection device.
Fig. 6 is the B-B view of Fig. 4, and the design of liquid zone falls in reflection.
The specific embodiment
Below in conjunction with accompanying drawing to structural representation of the present utility model.The utility model includes a circular tower tray at least, the center of described circular tower tray is provided with a central support tube and constitutes an annular tower tray, cut into secter pat according to overflow number equal portions on this annular tower tray, every part of secter pat is cut into seal pot 1, fan-shaped tower tray 3 again and falls 5 three of liquid zones.
Described annular tower tray fall under the liquid zone 5 for one deck column plate down liquid zone 5 falls, the described liquid zone 5 that falls joins by the seal pot 1 of a slope with following one deck column plate.
Is provided with an annular fluid connection device in the middle of the central support tube of described annular tower tray, the bottom surface of this linker and seal pot bottom surface flush, and end face is than in the seal pot about maximum level height~50mm, and lateral surface and downspout are communicated with.
Be provided with an annular gas linker in the middle of the central support tube of described annular tower tray, the bottom surface of this linker is the end face of fluid connection device, and the end face of linker flushes with the upper strata column plate, and the gas compartment of lateral surface and the different sectors of column plate is communicated with.
Pipe and outer tube in the central support tube of described annular tower tray is divided into; Seal at the top of interior pipe, communicates at the bottom of bottom and the tower, forms an annular region in the middle of outer tube and the interior pipe annular fluid connection device and annular gas linker are set.
The central support tube cross-sectional area of described annular tower tray accounts for 1/4~1/16 of whole tower tray cross-sectional area.
Shown in the accompanying drawing 4 is that the overflow number is 3 multi-overflow circle tower plate vertical view, and wherein: 1 is seal pot; 2 is that inlet weir, 3 is that fan-shaped tower tray, 4 is that exit weir, 5 is for falling the liquid zone; 6 is central support tube.
Shown in Figure 5 is: I is interior pipe; II is the gas linker; III is the fluid connection device.
Shown in Figure 6 is: it has reflected the structure of falling the liquid zone.
Shown in above accompanying drawing, with traditional circular tower tray, remove a circle that accounts for whole tower cross-sectional area 1/4~1/16 at the center, place central support tube, obtain an annular tower tray then, annular tower tray is cut into fan-shapedly according to overflow number equal portions, every part fan-shaped is cut into seal pot, fan-shaped tower tray again and falls three of liquid zones again.Liquid flow direction on all fan-shaped tower trays is consistent, all is clockwise or counter clockwise direction.Rotate a circle in the tower plate number of process and overflow number of liquid equates.
Column plate liquid flowing state design: design principle: the liquid that flow out from the inlet weir simultaneously (1) must flow into downspout simultaneously.(2) liquid is made the circular arc line plug-flow on fan-shaped column plate.For meeting above two design principles, carried out following design.Import and exit weir adopt flat weir, the height of weir top margin prolongs radially and reduces slightly from inside to outside, on fan-shaped column plate, pilot hole is set in addition, this pilot hole is to form through for many years improvement research and development on Chinese patent 912070846 bases of my research institute of company, pilot hole is stamped to form on column plate, one horizontal breach is arranged, gas sprays from horizontal breach to liquid and transmits momentum, improve the flowing velocity of liquid and the flow direction of change liquid, this pilot hole set-up mode be prolong fan-shaped column plate radially ecto-entad successively decrease, fan-shaped column plate arranged outside is maximum, the inboard of fan-shaped column plate generally is not provided with, have only when fan-shaped column plate is inboard to form big gradient of liquid level just to be provided with, the particular location of pilot hole and quantity must be by strict calculating.
The design of liquid zone is fallen: fall the liquid zone under for following one deck column plate the liquid zone rather than the seal pot of one deck column plate down fall, liquid is to be sent to the seal pot of one deck column plate down by a slope in falling the liquid zone.The advantage of this design is, liquid can produce still less bubble from the slope of exit weir inflow downspout, thereby reduce gas backmixing, when being moved upward, gas on the tower tray reduces to mix, also handlebar a part of infinite region of falling liquid zone top gives seal pot, thereby has improved the finite region of column plate.
Fluid connection device design: design principle be make with the liquid level of liquid in the different sectors seal pot on one deck column plate consistent with component.Design is to adopt the linker of an annular in central support tube, and the bottom surface of linker and seal pot bottom surface flush, and end face is than in the seal pot about maximum level height~50mm, and lateral surface and downspout are communicated with.This fluid connection device need all not be provided with at every layer of column plate, and certain column plate is provided with one at interval, and suggestion is that 5 layers of column plate are provided with one.
The design of gas linker: design principle is that the pressure with the different sectors of one deck column plate gas is equated.Design also is to adopt the linker of an annular in central support tube, and the bottom surface of linker is the end face of fluid connection device, and the end face of linker flushes with the upper strata column plate, and the gas compartment of lateral surface and the different sectors of column plate is communicated with.Every layer of column plate of this linker all must be provided with.
Central support tube design: pipe and outer tube in this central support tube is divided into; Interior pipe is a stay pipe truly, and seal at the top of interior pipe, communicates at the bottom of bottom and the tower, forms an annular region in the middle of outer tube and the interior pipe fluid connection device and gas linker are set.
Embodiment 1, nitrogen tower in the air separation plant model KOD-900 type high-purity nitrogen plant, and the design parameter of tower: the overflow number is 2, and the tower body diameter is 600mm, and the diameter of central support tube is 200mm, and theoretical tray is 43, and actual plate is 60; The composition of the 50th block of actual plate place nitrogen of test run report reflection reaches design load, and tower overall presure drop and design load are identical substantially, and tower can also stable operation under 34% operating mode.That is to say that the efficient than the whole tower of conventional design improves 20%, the pressure of every theoretical plate reduces by 20%, transfers the ability of load can reach 34% operating mode.

Claims (6)

1, a kind of multi-overflow circle tower plate, which comprises at least a circular tower tray, the center that it is characterized in that described circular tower tray is provided with a central support tube and constitutes an annular tower tray, cut into secter pat according to overflow number equal portions on this annular tower tray, every part of secter pat is cut into seal pot (1), fan-shaped tower tray (3) again and falls (5) three of liquid zones.
2, multi-overflow circle tower plate according to claim 1, it is characterized in that described annular tower tray fall under the liquid zone (5) for one deck column plate down liquid zone (5) falls, the described liquid zone (5) that falls joins by the seal pot of a slope with following one deck column plate.
3, multi-overflow circle tower plate according to claim 1, the middle annular fluid connection device that is provided with of central support tube that it is characterized in that described annular tower tray, the bottom surface of this linker and seal pot bottom surface flush, end face is than the high 50mm of maximum level in the seal pot, and lateral surface and downspout are communicated with.
4, multi-overflow circle tower plate according to claim 1, the central support tube centre that it is characterized in that described annular tower tray is provided with an annular gas linker, the bottom surface of this linker is the end face of fluid connection device, the end face of linker flushes with the upper strata column plate, and the gas compartment of lateral surface and the different sectors of column plate is communicated with.
5, multi-overflow circle tower plate according to claim 1 is characterized in that the central support tube of described annular tower tray is divided into interior pipe and outer tube; Seal at the top of interior pipe, communicates at the bottom of bottom and the tower, forms an annular region in the middle of outer tube and the interior pipe annular fluid connection device and annular gas linker are set.
6, multi-overflow circle tower plate according to claim 1 is characterized in that the central support tube cross-sectional area of described annular tower tray accounts for 1/4~1/16 of whole tower tray cross-sectional area.
CNU2008201695243U 2008-12-02 2008-12-02 Multi-overflow ring shaped column plate Expired - Fee Related CN201346405Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNU2008201695243U CN201346405Y (en) 2008-12-02 2008-12-02 Multi-overflow ring shaped column plate

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Application Number Priority Date Filing Date Title
CNU2008201695243U CN201346405Y (en) 2008-12-02 2008-12-02 Multi-overflow ring shaped column plate

Publications (1)

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CN201346405Y true CN201346405Y (en) 2009-11-18

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111330303A (en) * 2020-03-24 2020-06-26 深圳市海格金谷工业科技有限公司 Single overflow sieve plate tower

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111330303A (en) * 2020-03-24 2020-06-26 深圳市海格金谷工业科技有限公司 Single overflow sieve plate tower

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C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20091118

Termination date: 20131202