CN201326032Y - Silicon core electrode for polysilicon reducing furnace - Google Patents

Silicon core electrode for polysilicon reducing furnace Download PDF

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Publication number
CN201326032Y
CN201326032Y CNU2008201899310U CN200820189931U CN201326032Y CN 201326032 Y CN201326032 Y CN 201326032Y CN U2008201899310 U CNU2008201899310 U CN U2008201899310U CN 200820189931 U CN200820189931 U CN 200820189931U CN 201326032 Y CN201326032 Y CN 201326032Y
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CN
China
Prior art keywords
electrode body
electrode
silicon core
hole
reducing furnace
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Expired - Fee Related
Application number
CNU2008201899310U
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Chinese (zh)
Inventor
周积卫
茅陆荣
程佳彪
郝振良
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Morimatsu Jiangsu Heavy Industry Co Ltd
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Shanghai Senhe Investment Co Ltd
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Priority to CNU2008201899310U priority Critical patent/CN201326032Y/en
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Abstract

The utility model discloses a silicon core electrode for a polysilicon reducing furnace, which comprises an electrode body, a heating graphite heat silicon core, an electrode seat and an insulating sleeve pipe, wherein the heating graphite heat silicon core is sheathed on the top of the electrode body; the electrode seat is sheathed on the outer edge of the electrode body; the insulating sleeve pipe is positioned between the electrode body and the electrode seat; the middle of the inner side of the electrode body forms a blind hole; and the electrode body is positioned outside the reducing furnace, i.e. the open end of the blind hole is provided with a cooling device which can make cooling water circularly enter the inner side of the blind hole of the electrode body for further cooling the electrode body. The silicon core electrode can prevent the electrode punchthrough caused by failure of the insulating sleeve pipe because of the overhigh temperature.

Description

Silicon core electrode for polysilicon reducing furnace
Technical field
The relevant polycrystalline silicon reducing furnace technology of the utility model, more particularly, the silicon core electrode of using about a kind of polycrystalline silicon reducing furnace.
Background technology
The mainstream technology of polycrystalline silicon reducing furnace is trichlorosilane (SiHCl 3) reduction method, process gas is heated to about 1100 ℃ by silicon core electrode in the production process, makes trichlorosilane (SiHCl 3) and hydrogen (H 2) react the generation polysilicon and be deposited on the silicon core electrode surface, form silicon rod.The operating voltage of silicon core electrode is 15, and is about 000V, under the condition of High Temperature High Pressure like this, very high to the requirement of silicon core electrode.The silicon core electrode that adopts mainly comprises electrode body, heating graphite head silicon core, electrode holder at present, wherein insulate with insulating sleeve between electrode holder and the electrode body, and the composition of insulating sleeve is a tetrafluoroethylene.Because temperature is very high in the reduction furnace, though cool off by equipment chassis counter electrode seat, the temperature of teflon insulation body environment of living in is still very high, loses efficacy easily behind long-play, cause between electrode holder and the electrode body to puncture, cause industrial accident.
The utility model content
In view of this, the purpose of this utility model is to provide a kind of can further reduce temperature, effectively prevent to cause the silicon core electrode for polysilicon reducing furnace of electrode punch-through, guarantee polycrystalline silicon reducing furnace stability and high efficiency ground operation under high-temperature and high-pressure conditions because of insulating sleeve loses efficacy.
For achieving the above object, the technical solution of the utility model is achieved in that silicon core electrode for polysilicon reducing furnace of the present utility model, comprises:
Electrode body, the heating graphite head silicon core that is placed on this electrode body top, the electrode holder that is sheathed on the electrode body outer rim, and insulating sleeve between electrode body and electrode holder;
Described electrode body bosom is formed with blind hole, and it is that the opening end of blind hole is provided with and can makes the cooling water circulation electrode body blind hole inside that enters that described electrode body is carried out further refrigerative refrigerating unit that electrode body is positioned at the reduction furnace outside.
This refrigerating unit includes the cooling water outlet pipe that directly extends into the electrode body blind-hole bottom, the entrance of cooling water pipe that is communicated with the blind hole opening end, and be located at sleeve and the hold-down nut that electrode body blind hole opening end is used for fixing cooling water outlet pipe, entrance of cooling water pipe.
The outer rim that electrode body is positioned at the blind hole opening end is processed into step-like that diameter contracts, on the sidewall of the reduced diameter section of electrode body, be provided with the through hole that is communicated with blind hole, jacket casing is at the reduced diameter section of described electrode body, and on the sleeve lining face with respect to described reduced diameter section sidewall on the position of through hole be provided with annular ditch groove, this annular ditch groove is communicated with through hole on the reduced diameter section sidewall, and described telescopic sidewall is provided with the through hole that is communicated with and is connected with the entrance of cooling water seal of tube with groove.And the bottom of hold-down nut is provided with the but through hole that extends into of water outlet pipe sealing of cooling.
Be located by connecting by step between electrode holder and the electrode body, be formed with stepped hole in the middle part of electrode holder inwall, the outer wall periphery of electrode body is provided with the flange corresponding with stepped hole, and described insulating sleeve is corresponding with stepped hole stepped.
Be provided with the High-Voltage Insulation ring in the gap near an end that heats graphite head silicon core between electrode body and the insulating sleeve, the ring of High-Voltage Insulation simultaneously is covered on the chassis inner surface of reduction furnace, be positioned at reduction furnace chassis outside surface in electrode body and be arranged with fitting nut, in order to the electrode body that is locked, electrode holder and insulating sleeve.
Also be provided with elastic washer between the step of electrode holder inwall stepped hole and the insulating sleeve.
The two ends of electrode holder outer peripheral edges are welded to connect with the upper plate and the lower shoe on reduction furnace chassis respectively.
By silicon core electrode for polysilicon reducing furnace of the present utility model, can prevent effectively that insulating sleeve from causing the generation of punch-through between electrode holder and the electrode body because of high temperature failure, be fit to that the polycrystalline silicon reducing furnace high-voltage starts, the requirement of hot conditions operation.
Description of drawings
Fig. 1 is the structural section synoptic diagram of the utility model silicon core electrode for polysilicon reducing furnace.
Embodiment
As shown in Figure 1, silicon core electrode for polysilicon reducing furnace of the present utility model mainly comprises heating graphite head silicon core 7, electrode body 8, insulating sleeve 9 and electrode holder 11.The outer rim at electrode holder two ends about in the of 11 welds together with the upper plate 13 and the lower shoe 14 on polycrystalline silicon reducing furnace chassis respectively, and the middle part of electrode holder 11 inwalls is formed with stepped hole, is placed with elastic washer 10 on the step of electrode holder 11 inwall stepped holes; Stepped hole is processed in insulating sleeve 9 inboards, the outside processes crossette, edge sleeve 9 is stepped with the corresponding one-tenth of stepped hole of electrode holder 11, insulating sleeve 9 from top to bottom is nested with in the stepped hole of electrode holder 11, the crossette of insulating sleeve 9 is stuck on the elastic washer 10, and the two ends up and down of insulating sleeve 9 respectively with electrode holder about in the of 11 two ends concordant; The outer wall periphery of electrode body 8 is provided with the flange corresponding with stepped hole, electrode body 8 penetrates insulating sleeve 9 endoporus from top to bottom, the flange of the outer wall of electrode body 8 is stuck on the insulating sleeve 9 endoporus steps, and be equipped with High-Voltage Insulation ring 6 in the gap near an end that heats graphite head silicon core 7 between electrode body 8 and insulating sleeve 9, its upper end diameter is greater than lower end diameter, and the upper end of High-Voltage Insulation ring 6 is covered on the chassis inner surface of reduction furnace; Be positioned at reduction furnace chassis outer surface in electrode body 8 and be arranged with fitting nut 5, this fitting nut 5 can be locked electrode body 8, insulating sleeve 9, elastic washer 10 and be in the same place with electrode holder 11.Electrode body 8 tops are equipped with heating graphite head silicon core 7, and blind hole 81 is arranged at electrode body 8 intermediate formation, it is that the opening end of blind hole 81 is provided with and can makes the cooling water circulation blind hole 81 inner counter electrode bodies 8 that enter electrode body carry out further refrigerative refrigerating unit that electrode body 8 is positioned at the reduction furnace outside, this refrigerating unit includes the cooling water outlet pipe 1 of blind hole 81 bottoms that directly extend into electrode body, with the entrance of cooling water pipe 12 that blind hole 81 opening ends are communicated with, blind hole 81 opening ends that are located at electrode body are used for fixing described cooling water outlet pipe 1, the sleeve 3 and the hold-down nut 2 of entrance of cooling water pipe 12.Electrode body 8 is processed into step-like that diameter contracts in the outer rim that is positioned at blind hole 81 opening ends, on the sidewall of the reduced diameter section of electrode body 8, be provided with the through hole 80 that is communicated with blind hole 81, and sleeve 3 is set in the reduced diameter section of electrode body 8, position with respect to through hole 80 on the reduced diameter section sidewall on sleeve 3 inner-wall surfaces is provided with annular ditch groove, this annular ditch groove is communicated with this through hole 80, and these sleeve 3 sidewalls are provided with the through hole 30 that is communicated with this groove and entrance of cooling water pipe 12; Cooling water outlet pipe 1 inserts electrode body 8 intermediary blind holes 81 from the bottom to top, and hold-down nut 2 is nested with bottom in electrode body 8, in order to cooling water outlet pipe 1 and sleeve 3 tightly are locked on the electrode body 8, the bottom of hold-down nut 2 is provided with the but through hole 20 that extends into of water outlet pipe 1 sealing of cooling, between the blind hole 81 of electrode body 8 and cooling water outlet pipe 1, form an annulus like this, treated water coolant is entered in the blind hole 81 by the through hole 80 on the electrode body 8 lower end sidewalls from the cannelure of entrance of cooling water pipe 12 through sleeve 3, blind hole 81 and the rising of the annulus between the cooling water outlet pipe 1 along electrode body 8 are turned back to cooling water outlet pipe 1, flow out from cooling water outlet pipe 1, realize the cooling of counter electrode body 8.Connect conducting plates 4 clampings of high-voltage power supply and be fixed on the outer peripheral edges of electrode body 8.
In the equipment running process; cooling channel, reduction furnace chassis 15 internal cooling water counter electrode seats 11 cool off; further reduced the temperature of electrode holder 11 and electrode body 8; simultaneously High-Voltage Insulation ring 6 also can further completely cut off protection insulating sleeve 9 and contact with hot environment, prevents to cause owing to temperature is too high insulating sleeve 9 inefficacies to cause breakdown accident between electrode holder 11 and the electrode body 8.Being provided with of elastic washer 10 can effectively be reduced the silicon rod growth and be removed influence to silicon core electrode.
The above is preferred embodiment of the present utility model only, is not to be used to limit protection domain of the present utility model.

Claims (8)

1, a kind of silicon core electrode for polysilicon reducing furnace comprises:
Electrode body, the heating graphite head silicon core that is placed on this electrode body top, the electrode holder that is sheathed on the electrode body outer rim, and insulating sleeve between electrode body and electrode holder;
It is characterized in that, described electrode body bosom is formed with blind hole, and it is that the opening end of blind hole is provided with and can makes the cooling water circulation described electrode body blind hole inside that enters that described electrode body is carried out further refrigerative refrigerating unit that described electrode body is positioned at described reduction furnace outside.
2, silicon core electrode for polysilicon reducing furnace as claimed in claim 1, it is characterized in that, described refrigerating unit includes the cooling water outlet pipe that directly extends into described electrode body blind-hole bottom, with the entrance of cooling water pipe that described blind hole opening end is communicated with, be located at sleeve and hold-down nut that described electrode body blind hole opening end is used for fixing described cooling water outlet pipe, entrance of cooling water pipe.
3, silicon core electrode for polysilicon reducing furnace as claimed in claim 2, it is characterized in that, the outer rim that described electrode body is positioned at described blind hole opening end is processed into step-like that diameter contracts, on the sidewall of the reduced diameter section of described electrode body, be provided with the through hole that is communicated with described blind hole, described jacket casing is at the reduced diameter section of described electrode body, and on the described sleeve lining face with respect to described reduced diameter section sidewall on the position of through hole be provided with the annular ditch groove that is communicated with through hole on the reduced diameter section sidewall, described telescopic sidewall is provided with described groove and is communicated with, and the through hole that is connected with the described entrance of cooling water seal of tube.
4, silicon core electrode for polysilicon reducing furnace as claimed in claim 2 is characterized in that, the bottom of described hold-down nut is provided with the but through hole that extends into of water outlet pipe sealing of cooling.
5, silicon core electrode for polysilicon reducing furnace as claimed in claim 2, it is characterized in that, be located by connecting by step between described electrode holder and the described electrode body, middle part at described electrode holder inwall is formed with stepped hole, the outer wall periphery of described electrode body is provided with the flange corresponding with stepped hole, and described insulating sleeve is corresponding stepped with described stepped hole.
6, silicon core electrode for polysilicon reducing furnace as claimed in claim 5, it is characterized in that, be provided with the High-Voltage Insulation ring in the gap of an end of close described heating graphite head silicon core between described electrode body and the described insulating sleeve, simultaneously described High-Voltage Insulation ring is covered on the chassis inner surface of described reduction furnace, is positioned at the fitting nut that described reduction furnace chassis outside surface is arranged be used to be locked described electrode body, electrode holder and insulating sleeve in described electrode body.
7, silicon core electrode for polysilicon reducing furnace as claimed in claim 6 is characterized in that, is provided with elastic washer between the step of described electrode holder inwall stepped hole and the described insulating sleeve.
As any described silicon core electrode for polysilicon reducing furnace in the claim 1 to 7, it is characterized in that 8, the two ends of described electrode holder outer peripheral edges are welded to connect with the upper plate and the lower shoe on reduction furnace chassis respectively.
CNU2008201899310U 2008-12-11 2008-12-11 Silicon core electrode for polysilicon reducing furnace Expired - Fee Related CN201326032Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNU2008201899310U CN201326032Y (en) 2008-12-11 2008-12-11 Silicon core electrode for polysilicon reducing furnace

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNU2008201899310U CN201326032Y (en) 2008-12-11 2008-12-11 Silicon core electrode for polysilicon reducing furnace

Publications (1)

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CN201326032Y true CN201326032Y (en) 2009-10-14

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101440519B (en) * 2008-12-11 2012-02-01 上海森和工程投资有限公司 Silicon core electrode for polysilicon reducing furnace
CN106524776A (en) * 2016-10-19 2017-03-22 嘉峪关宏电铁合金有限责任公司 Method for blowing out submerged arc furnace for long time to protect electrode

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101440519B (en) * 2008-12-11 2012-02-01 上海森和工程投资有限公司 Silicon core electrode for polysilicon reducing furnace
CN106524776A (en) * 2016-10-19 2017-03-22 嘉峪关宏电铁合金有限责任公司 Method for blowing out submerged arc furnace for long time to protect electrode

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C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee

Owner name: SHANGHAI SENHE ENGINEERING INVESTMENT CO., LTD.

Free format text: FORMER NAME: SHANGHAI SENHE INVESTMENT CO., LTD.

CP03 Change of name, title or address

Address after: 201323 Shanghai city Pudong New Area Zhuqiao gold smell Road No. 29

Patentee after: Shanghai Senhe Engineering Investment Co., Ltd.

Address before: Nanhui District 201323 Shanghai Zhu Bridge Industrial Zone gold smell Road No. 29

Patentee before: Shanghai Senhe Investment Co., Ltd.

ASS Succession or assignment of patent right

Owner name: MORIMATSU (JIANGSU) HEAVY INDUSTRY CO., LTD.

Free format text: FORMER OWNER: SHANGHAI SENHE ENGINEERING INVESTMENT CO., LTD.

Effective date: 20140304

COR Change of bibliographic data

Free format text: CORRECT: ADDRESS; FROM: 201323 PUDONG NEW AREA, SHANGHAI TO: 226532 NANTONG, JIANGSU PROVINCE

TR01 Transfer of patent right

Effective date of registration: 20140304

Address after: 226532, room 319, building 306, spring garden, Changjiang town (Rugao port area), Nantong, Jiangsu, Rugao

Patentee after: Morimatsu (Jiangsu) Heavy Industry Co., Ltd.

Address before: 201323 Shanghai city Pudong New Area Zhuqiao gold smell Road No. 29

Patentee before: Shanghai Senhe Engineering Investment Co., Ltd.

TR01 Transfer of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20091014

Termination date: 20141211

EXPY Termination of patent right or utility model