CN201253570Y - Microwave desorption device of ethanol-loaded active carbon - Google Patents
Microwave desorption device of ethanol-loaded active carbon Download PDFInfo
- Publication number
- CN201253570Y CN201253570Y CNU2008200812733U CN200820081273U CN201253570Y CN 201253570 Y CN201253570 Y CN 201253570Y CN U2008200812733 U CNU2008200812733 U CN U2008200812733U CN 200820081273 U CN200820081273 U CN 200820081273U CN 201253570 Y CN201253570 Y CN 201253570Y
- Authority
- CN
- China
- Prior art keywords
- quartz glass
- ethanol
- active carbon
- microwave
- sieve plate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title claims abstract description 127
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 78
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 58
- 238000003795 desorption Methods 0.000 title claims abstract description 45
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 43
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 42
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 21
- 238000004080 punching Methods 0.000 claims description 10
- WYTGDNHDOZPMIW-RCBQFDQVSA-N alstonine Natural products C1=CC2=C3C=CC=CC3=NC2=C2N1C[C@H]1[C@H](C)OC=C(C(=O)OC)[C@H]1C2 WYTGDNHDOZPMIW-RCBQFDQVSA-N 0.000 claims description 3
- 229920000742 Cotton Polymers 0.000 claims description 2
- 239000000523 sample Substances 0.000 claims description 2
- 230000008878 coupling Effects 0.000 claims 1
- 238000010168 coupling process Methods 0.000 claims 1
- 238000005859 coupling reaction Methods 0.000 claims 1
- 238000001179 sorption measurement Methods 0.000 abstract description 11
- 239000007789 gas Substances 0.000 abstract description 7
- 239000003365 glass fiber Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 16
- 238000011069 regeneration method Methods 0.000 description 13
- 230000000694 effects Effects 0.000 description 11
- 229920006395 saturated elastomer Polymers 0.000 description 10
- 239000003610 charcoal Substances 0.000 description 8
- 238000010438 heat treatment Methods 0.000 description 8
- 230000008929 regeneration Effects 0.000 description 8
- 239000000463 material Substances 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- 238000010521 absorption reaction Methods 0.000 description 6
- 239000003463 adsorbent Substances 0.000 description 6
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 238000000746 purification Methods 0.000 description 5
- 239000002156 adsorbate Substances 0.000 description 4
- 238000013461 design Methods 0.000 description 4
- 229910000831 Steel Inorganic materials 0.000 description 3
- 238000013019 agitation Methods 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- 230000008030 elimination Effects 0.000 description 3
- 238000003379 elimination reaction Methods 0.000 description 3
- 239000008187 granular material Substances 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000005416 organic matter Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- 238000000967 suction filtration Methods 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 230000000274 adsorptive effect Effects 0.000 description 2
- 238000009529 body temperature measurement Methods 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000009418 renovation Methods 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000170793 Phalaris canariensis Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000001684 chronic effect Effects 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 239000010842 industrial wastewater Substances 0.000 description 1
- 239000008235 industrial water Substances 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000010815 organic waste Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
- 238000009279 wet oxidation reaction Methods 0.000 description 1
Images
Landscapes
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
The utility model relates to a microwave desorption device for active carbon carried with ethanol, which is characterized in that the center of the top of the microwave desorption device is provided with a circular hole of which the size is matched with the outside diameter of a quartz glass reactor; the quartz glass reactor is inserted into an inner chamber of the microwave desorption device by the circular hole and is fixed; a detector armored with a thermocouple is inserted into a position of an active carbon bed layer carried with ethanol, and the position is close to the center; the top of the quartz glass reactor is connected with a condenser by an additional pipe; the back of the condenser is connected with a collecting vessel; the quartz glass reactor has the structure jointly formed by a quartz glass pipe and a perforative quartz glass sieve plate; the middle lower part of the inner wall of the quartz glass pipe is provided with the perforative quartz glass sieve plate on which a layer of quartz glass fibre used for supporting the active carbon carried with ethanol is uniformly laid; the bottom of the perforative quartz glass sieve plate is connected with a nitrogen additional pipe; and nitrogen is used as supporting gas. The utility model has the advantages of simple operation, high speed, easy control, high adsorption capacity of regenerated active carbon, little mass loss, sharp curve peak form of exit concentration of ethanol during the desorption, high peak value, respective collection of ethanol with high concentration, and the like.
Description
Technical field: the utility model relates to the device that the ethanol active carbon is carried in a kind of microwave desorb, belongs to the Treatment of Industrial Water technical field.
Background technology: a large amount of weak liquors that produce in the alcohol industry production process mainly contain ethanol (4%～8%), a small amount of lipid and acid.At present this class weak liquor is mainly adopted the method for direct discharging.Because the ethanol content in the weak liquor is very low, and water and ethanol can form azeotropic mixture, so traditional heating fractional method is very difficult with it separation, and is difficult to produce a desired effect with general wastewater processing technology.
Active carbon is a kind of black porous solid adsorption material, is widely used in the environmental protection, is used to eliminate the desulfurization removing nitric of atmosphere pollution, the processing of various industrial wastewaters etc.Active carbon has very strong adsorption capacity to the organic matter in the water.To weak liquor, if adopt active carbon adsorption to handle, both recyclable ethanol wherein can solve problem of environmental pollution again.
With the low-concentration ethanol in the active carbon adsorption recovery weak liquor, whether economically viable decisive factor is except the theoretical research basis of adsorption process for this method, the selection of active carbon desorption regeneration and theoretical research thereof are important too, otherwise will certainly bring the treatment cost height, cause secondary pollution, administer problems such as not thorough.
The economy of active carbon adsorption depends primarily on regeneration.At present, regeneration method of active carbon mainly contains following several big class: thermal regeneration method, medicament method of reproduction, bio-regeneration method, chemical regeneration method, wet oxidation method of reproduction etc.Wherein the thermal regeneration method is that using, study maximum in the various renovation process also is the most ripe a kind of method.The desorb of tradition alternating temperature can realize by indirect adsorbent or direct the contact with hot gas.To active carbon, often utilize steam to come desorb, because the active carbon coefficient of heat conduction is lower, make whole fixed bed be heated to adsorbate by the temperature of desorb, need the chronic of heating.Another shortcoming of alternating temperature desorb is that energy consumption is big, it is temperature required that regeneration needs that not only adsorbate is risen to desorb, and for adsorbent is further activated, also need temperature further is raised to the activation temperature of adsorbent, and after the heating for multiple times cooling, scaling loss is serious.If utilize superheated steam regeneration, fixed bed is also dry again before adsorbing again.If the organic matter of desorb is moisture, water and organic separation equipment must be set also.
The microwave desorption technique is researched and developed at the purified treatment of low-concentration industrial organic exhaust gas, compares with traditional hot renovation process, and the heating using microwave desorption and regeneration has following advantage: 1) microwave plays the deep layer heat effect to reactant; 2) microwave heating temperature is even; 3) desorption rate is fast; 4) under microwave irradiation, the loss of the electronics of the various adsorbates that are evaporated is different, therefore can realize the selection heating to adsorbate.
Reclaim for the purification of low-concentration industrial volatile organic waste gas, it is both economy and effective method that the organic matter active carbon is carried in the microwave desorb, but the microwave desorption apparatus and the method thereof that also do not reclaim at low-concentration ethanol in the weak liquor at present.
It is resultful for the separating of component that this class of water and ethanol in year ethanol active carbon desorption process can form azeotropic mixture that heating using microwave has the selectivity this point.The second alcohol and water causes the desorption rate difference to the absorption efficiency difference of microwave, forms sharp-pointed ethanol exit concentration curve, can divide jar collection to obtain the alcohol product of different stage.Industrial nitrogen has chemical inertness, not with active carbon in C reaction, cost is cheap relatively, selects nitrogen to carry the carrier gas of ethanol active carbon process as the microwave desorption and regeneration.
Summary of the invention: the purpose of this utility model is to solve the deficiency of prior art, provides a kind of microwave desorb to carry ethanol active carbon device, and it utilizes the selectivity heating characteristics of microwave to realize loading on the separation refining effect of the ethanol-water system on the active carbon.Divide and jar to collect a distillate, active carbon is regenerated when obtaining the alcohol product of different stage.
So the purpose of this utility model also in weak liquor to low-concentration ethanol absorption saturated carry the ethanol active carbon, adopt microwave desorption apparatus and method to come desorb to carry the ethanol active carbon, the ethanol-water system of load on the isolating active charcoal, active carbon is regenerated when dividing a jar collection to obtain the different stage alcohol product.
The technical solution of the utility model is: the microwave desorb is carried ethanol active carbon device and is made up of microwave desorption apparatus (1), quartz glass reactor (2), condenser (3), distillate collection container (4), nitrogen cylinder (5), spinner flowmeter (6), armoured thermocouple (8), punching quartz glass sieve plate (9), digital display temperature indicator (11), nitrogen arm (12), open a circular hole that is equivalent to quartz glass reactor (2) diameter at microwave desorption apparatus (1) center of top position, reactor (2) inserts microwave desorption apparatus chamber and fixing by this hole.The punching sieve plate (9) of a silica glass material is installed in position, middle and lower part in reactor (2), and goes up even shakedown one deck quartz glass cotton at sieve plate (9), is used for support and carries the ethanol active carbon.Nitrogen is flowed through and is uniformly distributed in whole year ethanol active carbon bed behind the buffering area under the sieve plate (9).The probe of measuring the armoured thermocouple (8) of temperature is inserted into and carries the position of ethanol active carbon bed near the center.The mixing of the second alcohol and water that reactor (2) top manifold is come out is separated gassing through condenser (3) condensation, and condenser (3) back receives collection container (4).Distillate divides according to ethanol exit concentration curve jar to be collected, can be with the distillate of low concentration again through the activated charcoal adsorption-microwave desorb with further purification ethanol.
This utility model operating process is:
The first step, the logical condensed water of water-cooled serpentine (trombone) cooler for series connection is partially immersed in coiled pipe in the bosh.
Second goes on foot, and opens the main valve and the pressure-reducing valve of nitrogen steel cylinder, by spinner flowmeter control nitrogen flow.After treating stability of flow, regulate microwave power, connection microwave desorption apparatus power supply also picks up counting, and the thermocouple temperature measurement system log (SYSLOG) carries ethanol active carbon bed temperature.
In the 3rd step, microwave irradiation cuts off microwave desorption apparatus power supply during to setting-up time, closes nitrogen, closes condensed water.
In the 4th step, divide a jar collection distillate according to ethanol exit concentration curve.Identify desorption efficiency and the mass rate of material loss of the back active carbon of regenerating with gravimetric method, gas chromatography determination divides the concentration of alcohol in jar distillate of collecting.
To the utility model, result of study shows, microwave power is high more, desorb is fast more, and the peak shape of the ethanol exit concentration curve of desorption process is sharp-pointed more, and peak value is high more, and more early occur, the desorption gas composition difference that the different periods of desorption process are described is big more, and the separating effect of microwave desorb is good more, helps the branch jar and collects the ethanol that obtains high concentration.But increase in power, the mass rate of material loss of regenerated carbon also will increase, and under high microwave power the easy scaling loss of irradiation active carbons, the absorption property that causes regenerated carbon is far below new charcoal.Therefore to take all factors into consideration microwave power to carrying the influence of ethanol active carbon microwave desorb, should select microwave power according to the specific requirement of practical application in industry.
The utlity model has simple in structure, processing ease, speed is fast, it is sharp-pointed that regenerated carbon adsorption capacity height, mass loss reach the ethanol exit concentration curve peak shape of desorption process less, the peak value height can divide jar to collect the advantage of the alcohol product of different stage.
Description of drawings: the utility model is described in further detail below in conjunction with Fig. 1～3 and embodiment, provides the specific design parameter of equipment in conjunction with the embodiments.
Fig. 1 is that each parts annexation structural representation of ethanol active carbon device is carried in microwave desorb of the present utility model.
Fig. 2 is the microwave desorb part and the temperature measurement fraction structural representation of the utility model device.
Fig. 3 is the punching quartz glass sieve plate modular construction schematic diagram of the utility model device.
Among the figure: the 1st, microwave desorption apparatus, the 2nd, quartz glass reactor, the 3rd, condenser, the 4th, distillate collection container, the 5th, nitrogen cylinder, the 6th, spinner flowmeter, the 7th, the ethanol active carbon, the 8th, armoured thermocouple, the 9th, punching quartz glass sieve plate, the 10th, micro-wave oven, the 11st, digital display temperature indicator, the 12nd, nitrogen arm, the 13rd, quartz glass plate, the 14th, sieve aperture.
The specific embodiment:
Embodiment 1: press shown in Fig. 1～3, make the utility model device, its equipment specific design parameter:
1, microwave desorption apparatus 1 is the WP800 type Glanz domestic microwave desorption apparatus of reequiping voluntarily, and microwave power is adjustable continuously;
2, desorption and regeneration quartz glass reactor 2 is the structure of being made up of quartz glass tube and punching quartz glass sieve plate 9, and quartz glass sieve plate 9 is positioned at quartz glass tube apart from 6cm place, inwall lower end; Quartz glass tube is Φ 30mm * 200mm; The sieve plate of punching quartz glass sieve plate 9 is 30mmi.d, and sieve aperture is 2mmi.d., and nine sieve apertures 14 are uniformly distributed in the square area at punching quartz glass sieve plate 9 centers;
3, nitrogen cylinder 5 is a nitrogen steel cylinder commonly used on the general industry, and the technical grade nitrogen of dried and clean enters quartz glass reactor 2 bottoms under the pressure of steel cylinder itself, and regulates control nitrogen gas pressure, flow by pressure-reducing valve and spinner flowmeter;
4, condenser 3 adopts the water-cooled serpentine (trombone) cooler of three series connection, and logical condensed water is partially immersed in coiled pipe in the bosh.
Carry out the active carbon employing ature of coal granular activated carbon that desorb is handled; active carbon is immersed in the hydrochloric acid of mass concentration 6%; in boiling water, boil 30min then; with distilled water repeatedly rinsing to remove bulky grain and impurity; rinsing to the washings pH value 6 back 105 ℃ dry to constant weight; with 80 mesh sieve elimination granule and powder, be stored in the drier, standby as pretreated seed activity carbon adsorbent.
Operating process:
Prepare saturated year ethanol active carbon 7: adopt intermittently dynamics device; adsorption temp is a normal temperature; with 10.000g through pretreated granular activated carbon mixing and absorption in the ethanol water of 300mL mass concentration 4.0%; and with magnetic agitation 2h; with vavuum pump suction filtration 5min, the saturated activity charcoal that leaches is waited until desorb.
The control of microwave desorption and regeneration system and nitrogen flow: above saturated activity charcoal is placed in the quartz glass reactor 2, desorb in above-mentioned microwave desorption apparatus 1, nitrogen flow is controlled at 0.06m
3/ h.When microwave operational frequencies is 2450MHz, microwave power 680W, during exposure time 80s, desorption efficiency is 99.79%, the regenerated carbon mass rate of material loss is 6.89%.
The condenser 3 of desorption gas reclaims: the mixing stripping gas of the second alcohol and water that comes out from the top manifold of quartz glass reactor 2 is through condenser 3 condensations, and distillate divides according to ethanol exit concentration curve jar to be collected.The ethanol mass concentration reaches as high as 45% in the branch jar distillate of collecting.
Can be with the distillate of low concentration again through the activated charcoal adsorption-microwave desorb with further purification ethanol.
The utility model adopts above desorption technique condition, and the weak liquor of ethanol mass concentration 4.0% divides a jar collection distillate, the highest ethanol that can be recovered to mass concentration 94% after three activated charcoal adsorption-microwave desorption cycle.
Embodiment 2: adopt specific design parameter, technological process and the equipment connection of apparatus identical with embodiment one, no longer repeat.
Active carbon is immersed in the hydrochloric acid of mass concentration 8%; in boiling water, boil 30min then; with distilled water repeatedly rinsing to remove bulky grain and impurity; rinsing to the washings pH value 6 back 105 ℃ dry to constant weight; with 80 mesh sieve elimination granule and powder; be stored in the drier, standby as pretreated seed activity carbon adsorbent.
Prepare saturated year ethanol active carbon: adopt intermittently dynamics device; adsorption temp is a normal temperature; with 10.000g through pretreated granular activated carbon mixing and absorption in the ethanol water of 300mL mass concentration 4.0%; and with magnetic agitation 2h; with vavuum pump suction filtration 5min, the saturated activity charcoal that leaches is waited until desorb.
Above saturated year ethanol active carbon placed the desorb of above-mentioned microwave desorption apparatus, and nitrogen flow is controlled at 0.06m
3/ h, when microwave operational frequencies is 2450MHz, microwave power 320W, during exposure time 100s, desorption efficiency is 95.36%, regenerated carbon methylenum careuleum adsorptive value is 156.72mg/g (new charcoal methylenum careuleum adsorptive value is 146.26mg/g), and mass rate of material loss is 3.50%, and the ethanol mass concentration reaches as high as 37% in the branch jar distillate of collecting.
Can be with the distillate of low concentration again through the activated charcoal adsorption-microwave desorb with further purification ethanol.The utility model adopts above desorption technique condition, and the weak liquor of ethanol mass concentration 4.0% divides a jar collection distillate, the highest ethanol that can be recovered to mass concentration 91% after three charcoal absorptions-vacuum microwave desorption cycle.
Embodiment 3: adopt specific design parameter, technological process and the equipment connection of the utility model apparatus identical with embodiment one, no longer repeat.
Active carbon is immersed in the hydrochloric acid of mass concentration 5%; in boiling water, boil 30min then; with distilled water repeatedly rinsing to remove bulky grain and impurity; rinsing to the washings pH value 5 back 105 ℃ dry to constant weight; with 80 mesh sieve elimination granule and powder; be stored in the drier, standby as pretreated seed activity carbon adsorbent.
Prepare saturated year ethanol active carbon 7: adopt intermittently dynamics device; adsorption temp is a normal temperature; with 10.000g through pretreated granular activated carbon mixing and absorption in the ethanol water of 300mL mass concentration 4.0%; and with magnetic agitation 2h; with vavuum pump suction filtration 5min, the saturated activity charcoal that leaches is waited until desorb.
Above saturated year ethanol active carbon placed the desorb of above-mentioned microwave desorption apparatus, and nitrogen flow is controlled at 0.06m
3/ h, when microwave operational frequencies is 2450MHz, microwave power 136W, during exposure time 145s, desorption efficiency is 39.43%, the regenerated carbon mass rate of material loss is 1.49%, divides that the ethanol mass concentration reaches as high as 35% in jar distillate of collecting.
Can be with the distillate of low concentration again through the activated charcoal adsorption-microwave desorb with further purification ethanol.The utility model adopts above desorption technique condition, and the weak liquor of ethanol mass concentration 4.0% divides a jar collection distillate, the highest ethanol that can be recovered to mass concentration 90% after three activated charcoal adsorption-microwave desorption cycle.
Claims (3)
1. ethanol active carbon device is carried in a microwave desorb, comprise microwave desorption apparatus (1), quartz glass reactor (2), condenser (3), distillate collection container (4), nitrogen cylinder (5), spinner flowmeter (6), armoured thermocouple (8), punching quartz glass sieve plate (9), digital display temperature indicator (11), nitrogen arm (12), it is characterized in that opening a circular hole with quartz glass reactor (2) external diameter coupling in microwave desorption apparatus (1) center of top position, quartz glass reactor (2) is inserted microwave desorption apparatus inner chamber and fixing by this circular hole, the probe of armoured thermocouple (8) is inserted into and carries the position of ethanol active carbon (7) bed near the center, quartz glass reactor (2) top connects condenser (3) by arm, and condenser (3) back receives collection container (4).
2. ethanol active carbon device is carried in microwave desorb according to claim 1, it is characterized in that quartz glass reactor (2) is for forming structure jointly by quartz glass tube and punching quartz glass sieve plate (9), a punching quartz glass sieve plate (9) is installed in position, quartz glass inside pipe wall middle and lower part, and, be used for support and carry ethanol active carbon (7) at the upward even shakedown one deck quartz glass cotton of quartz glass sieve plate (9) that punches.
3. ethanol active carbon device is carried in microwave desorb according to claim 1 and 2, it is characterized in that condenser (3) can adopt the water-cooled serpentine (trombone) cooler of series connection, and collection container (4) is industrial receiving flask commonly used.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008200812733U CN201253570Y (en) | 2008-05-29 | 2008-05-29 | Microwave desorption device of ethanol-loaded active carbon |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008200812733U CN201253570Y (en) | 2008-05-29 | 2008-05-29 | Microwave desorption device of ethanol-loaded active carbon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201253570Y true CN201253570Y (en) | 2009-06-10 |
Family
ID=40736882
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNU2008200812733U Expired - Fee Related CN201253570Y (en) | 2008-05-29 | 2008-05-29 | Microwave desorption device of ethanol-loaded active carbon |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201253570Y (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103736474A (en) * | 2014-01-22 | 2014-04-23 | 湖北君集水处理有限公司 | Microwave oven for regenerating powder active carbon |
| CN104841346A (en) * | 2015-04-28 | 2015-08-19 | 华东理工大学 | Disc reactor for gas desorption of absorbents different in viscosity |
-
2008
- 2008-05-29 CN CNU2008200812733U patent/CN201253570Y/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103736474A (en) * | 2014-01-22 | 2014-04-23 | 湖北君集水处理有限公司 | Microwave oven for regenerating powder active carbon |
| CN103736474B (en) * | 2014-01-22 | 2015-06-24 | 湖北君集水处理有限公司 | Microwave oven for regenerating powder active carbon |
| CN104841346A (en) * | 2015-04-28 | 2015-08-19 | 华东理工大学 | Disc reactor for gas desorption of absorbents different in viscosity |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Sun et al. | Activated carbon preparation from lignin by H3PO4 activation and its application to gas separation | |
| CN106966392A (en) | A kind of method that utilization municipal sludge prepares nitrogen sulphur codope porous carbon material | |
| CN109759017A (en) | A kind of preparation method of modified walnut shell charcoal | |
| CN105518147A (en) | Device for manufacturing organic substance and method for manufacturing organic substance | |
| CN107188386A (en) | A kind of method that utilization sewage plant excess sludge prepares charcoal | |
| Yang et al. | Superb VOCs capture engineering carbon adsorbent derived from shaddock peel owning uncompromising thermal-stability and adsorption property | |
| CN101486918A (en) | Novel spouted circulating fluid bed timber rapid pyrolysis apparatus and technological process | |
| CN202343204U (en) | Vacuum microwave desorption ethanol-loaded activated carbon device | |
| CN105505418A (en) | Pyrolysis test device | |
| CN201253570Y (en) | Microwave desorption device of ethanol-loaded active carbon | |
| CN110479223A (en) | A kind of method of the microwave-heating poplar bits preparation simultaneously rich in phenol bio-oil and the biomass carbon for adsorbing heavy metal ion | |
| CN101475430A (en) | Method for purifying ethylene from ethylene-rich gaseous mixture | |
| CN205347328U (en) | Laboratory is with living beings pyrolysis carbonization reaction unit | |
| CN104119215A (en) | Molecular sieve regeneration method in acetone continuous dehydration production process | |
| CN101255096A (en) | Method for purifying and reclaiming alcohol from weak liquor by activated charcoal adsorption-microwave azeotropic distillation desorption | |
| CN110257096A (en) | A method of bio oil is prepared using lignin | |
| CN106180117B (en) | A kind of processing equipment and method of waste | |
| CN201735406U (en) | Microwave activated carbon regenerating unit | |
| CN210855273U (en) | Purification device of high-purity hydrogen sulfide | |
| CN209010457U (en) | A kind of refining system of biology vinegar liquid | |
| CN103752296A (en) | Device and method for regeneration of powdered activated carbon | |
| Yang et al. | Experimental study on microwave modified AC and its adsorption on formaldehyde | |
| CN102719290A (en) | Two-stage fluidized bed coal bed gas non-catalytic deoxidation technology | |
| Klemantan et al. | Microwave Assisted KOH Activation of Salacca Peel Dericed Activated Carbons as Adsorbents for Methylene Blue Removal from Aqueous Phase | |
| Negara et al. | Development of mesoporous activated carbons derived from brewed coffee waste for CO2 adsorption |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20090610 Termination date: 20120529 |