CN201159722Y - Multifunctional example frame for X-ray diffraction instrument - Google Patents

Multifunctional example frame for X-ray diffraction instrument Download PDF

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Publication number
CN201159722Y
CN201159722Y CNU2008200106627U CN200820010662U CN201159722Y CN 201159722 Y CN201159722 Y CN 201159722Y CN U2008200106627 U CNU2008200106627 U CN U2008200106627U CN 200820010662 U CN200820010662 U CN 200820010662U CN 201159722 Y CN201159722 Y CN 201159722Y
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China
Prior art keywords
plate
motor
ring stand
frame plate
sample
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Expired - Lifetime
Application number
CNU2008200106627U
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Chinese (zh)
Inventor
金文仁
王瑛
李吉成
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DANDONG FANGYUAN INSTRUMENT Co Ltd
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DANDONG FANGYUAN INSTRUMENT Co Ltd
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Priority to CNU2008200106627U priority Critical patent/CN201159722Y/en
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Abstract

The utility model relates to a multifunctional sample rack for an X-ray diffraction, comprising a base (1), an annular rack device (2), a transmission rack plate device (4) and a sample rack plate device (6); the transmission rack device and the sample rack plate device rotate around the central axis (Z) and move back and forth that is the X axis movement through the motor belt; the sample rack plate is enabled to move along the (K) direction; the sample box base (63) of the sample rack plate device is enabled to rotate around the (X) axis so that the sample arranged on the sample box is enabled to have accurate actions in a plurality of directions; the application requirement is completely satisfied; the detection application capability and the application field of the X-ray diffraction are extended.

Description

The X-ray diffractometer multifunctional sample holder
Technical field
The utility model relates to the X-ray diffractometer multifunctional sample holder.
Background technology
X-ray diffractometer is the equipment that the composition of material and atom level structure are studied and identified, usually the angular instrument of X-ray diffractometer is to rotate the position angle difference of promptly placing according to the surface of sample, to the number percent of the atomic arrangement of material, thing phase, each thing phase, grain size, crystallinity etc. detects.But in the research to the stress in the material, texture, the degree of orientation, film etc., then needing sample to do more motion matches, for example: stress measurement just need add this motion of sample inclination, texture measurement need add sample inclination, rotation, swing, the degree of orientation detect to need the sample rotation, and measured thin film needs that sample moves forward and backward, sample inclination etc.
In the past during our research material stress, just need the erection stress specimen holder, the several angles of sample inclination are measured, during research material texture, just need to install the texture specimen holder, sample inclination is added from transferring measurement, just need during the research material degree of orientation Rotary Specimen Rack is installed, sample is measured from transferring, when the film of research plated film outer, just need Φ scanning samples frame is installed, make sample inclination and rotation, when regarding to film sample low angle incident test, also need sample to move forward and backward, and above said sample tilt angle, often needing manual control, this has just brought inconvenience for this research on the one hand.
Prior art is carried out detections such as texture, stress, rotation, plated film, Φ scanning as mentioned above at X-ray diffraction to sample, needing various special measurement specimen holder dresses to be installed on the X-ray diffractometer measures, and some action also do not realize, can't realize measuring.Along with the fast development of modern material science, often the research to material is not limited to single aspect, but same material research when carrying out several aspect.For example, not only need to know the qualitative situation of plated film for the plated film on substrate research, but also the texture, stress, thickness that need to understand plated film situation such as outer film whether.Measure with X-ray diffractometer at present and need following several steps: 1. at first will on X-ray diffractometer, carry out qualitative analysis, check plated film coating situation; 2. change the powdered sample platform, change the texture specimen holder, carry out the sample orientation detection; 3. take off the texture specimen holder, change the stress specimen holder, carry out stress measurement; 4. take off the stress specimen holder, change Φ scanning samples frame, carry out the judgement of outer film; 5. take off the stress specimen holder and change the thickness detection that Rotary Specimen Rack is carried out plated film.These operations almost can not be finished concerning common X-ray diffractometer operating personnel, because not only need numerous specimen holders, but also need the accurate various specimen holders of installing, X-ray diffractometer requires very high to various specimen holder installation accuracies, has only accurate installation specimen holder, the correct sample of putting, just can collect accurate information, specimen holder is repeatedly installed, the information that often collects is not very accurate, satisfying under the situation of above condition, sample of complete measurement needs several days time.Along with popularizing that X-ray diffractometer is used, find that more and more the simple sample frame can not satisfy application requirements.
The utility model content
The purpose of this utility model provides a kind of X-ray diffractometer multifunctional sample holder easy to use.
The utility model includes base 1, ring stand device 2, gear frame panel assembly 4, specimen holder panel assembly 6.
Ring stand device 2 includes ring stand 21, left and right sides slide plate 22a, 22b, tooth plate 23, worm screw 24, motor 25,26, slide block 27a, on ring stand 21 inner ring surfaces, offer chute 28, tooth plate 23 is slidingly matched with chute 28, worm screw 24 on being provided with worm-gear toothing on the tooth plate 23 and being installed in ring stand 21 cooperates transmission, left and right sides slide plate 22a, 22b is slidingly matched by chute with ring stand 21 and fixedlys connected with tooth plate 23, motor 25 drives worm screw 24 and drives left and right sides slide plate 22a by tooth plate 23,22b rotates on ring stand 21, at left and right sides slide plate 22a, the last setting of 22b is connected with slide block 27a, motor 26 is fixedlyed connected installation by link 30 with slide plate 22b, be installed with screw rod and overlap 29 on 26 in motor.This ring stand device 2 drives worm screws 24 by motor 25, and worm screw 24 drives tooth plates 23, and to drive slide plate 22a, 22b on ring stand 21 be the action that rotates of Z axle around ring stand 21 axle center.
Gear frame panel assembly 4 includes frame plate 41, motor 42,43, worm screw 45, worm screw 45 is installed on the frame plate 41 by bearing arrangement, cooperate with conical gear 48 on worm screw 45 axle heads and drive worm screw 45 and rotate being installed with conical gear 47 on motor 43 axle heads, on motor 42 axle heads, be installed with cam 46, on frame plate 41 trailing flanks, be connected with chute 27b by link 37, chute 27b and aforementioned said left and right sides slide plate 22a, slide block 27a on the 22b is connected, make frame plate 41 relative slide plate 22a, slide before and after the 22b to move and be connected, be fixed with at frame plate 41 that hard-wired screw rod cover 29 cooperates drive frame plate 41 to move forward and backward on 26 in nut sleeve 49 and the aforementioned said motor, on frame plate 41 leading flanks, be provided with slide block 50a.
Specimen holder panel assembly 6 includes frame plate 61, sample box 62, sample cassette holder 63, bearing arrangement 64, worm gear 65, drive link 66, chute 50b, the slide block 50a sliding connection that said frame plate 41 leading flanks of chute 50b and preceding art are provided with, make frame plate 61 and frame plate 41 realize that planar slide is connected, sample cassette holder 63 is installed on the mounting hole of offering on the frame plate 61 by bearing arrangement 64, worm gear 65 is fixedly mounted on the sample cassette holder 63, worm gear 65 cooperates the product of drive cassette holder 63 to rotate with aforementioned said worm screw 45, sample box 62 is installed on the sample cassette holder 63, drive link 66 is fixedlyed connected with frame plate 61, be provided with a pair of bearing pin 67a at drive link 66,67b cooperates with hard-wired cam 46 on aforementioned said motor 42 axle heads, drive drive link 66 and frame plate 61 along K to moving.
The utility model is Z axle rotate action around ring stand 21 central shafts by motor 25 band gear frame panel assemblies 4 and specimen holder panel assembly 6 on ring stand 21; Moving forward and backward by motor 26 drive gear frame panel assemblies 4 and sample frame plate loading amount 6 is that X-direction moves; By motor 42 drive frame plates 61 along K to moving; The sample cassette holder 63 that drives on the frame plate 61 by motor 43 rotates promptly around the X-axis rotation, thereby realize being installed on the sample box 62 sample multi-direction accurate action, fully satisfy application demand, expand the detection application power and the application of diffractometer, can make common X-ray diffractometer become the multi-functional X-ray diffractometer, be investigation of materials work, a kind of very reliable detection equipment is provided.
Description of drawings
Fig. 1, the 2nd, the utility model example structure synoptic diagram, Fig. 2 are that the rear side of Fig. 1 is to view.
Fig. 3,4, the 5th, ring stand device 2 structural representations, wherein Fig. 4 is the C-C cut-open view of Fig. 3, Fig. 5 is the D-D cut-open view of Fig. 4.
Fig. 6, the 7th, gear frame panel assembly 4 structural representations, Fig. 7 are the B-B cut-open views of Fig. 6.
Fig. 8, the 9th, specimen holder panel assembly 6 structural representations, Fig. 9 are the A-A cut-open views of Fig. 8.
Figure 10 is Fig. 5,9 E-E cut-open view, i.e. chute 27b, 50b and slide block 27a, the 50a structural representation that is connected.
Embodiment
The utility model is made of base 1, ring stand device 2, gear frame panel assembly 4, specimen holder panel assembly 6.
Referring to accompanying drawing 3,4, shown in 5, ring stand device 2 includes ring stand 21, left and right sides slide plate 22a, 22b, tooth plate 23, worm screw 24, motor 25,26, slide block 27a, on ring stand 21 inner ring surfaces, offer chute 28, tooth plate 23 is slidingly matched with chute 28, worm screw 24 on being provided with worm-gear toothing on the tooth plate 23 and being installed in ring stand 21 cooperates transmission, left and right sides slide plate 22a, 22b is slidingly matched by chute with ring stand 21 and fixedlys connected with tooth plate 23, promptly at ring stand 21 sides and left and right sides slide plate 22a, the last correspondence of 22b offers V-shaped groove, in the V groove, be provided with ball 32 and form the chute sliding connection, motor 25 is fixedlyed connected installation by link 33 with ring stand 21,25 in motor passes through shaft coupling 35 and is connected with worm screw 24, motor 25 drives worm screw 24 and drives left and right sides slide plate 22a by tooth plate 23,22b rotates on ring stand 21, at left and right sides slide plate 22a, be provided with on the 22b and connect slide block 27a, motor 26 is fixedlyed connected installation by link 30 with slide plate 22b, be installed with screw rod and overlap 29 on 26 in motor.This ring stand device 2 drives worm screws 24 by motor 25, and worm screw 24 drives tooth plates 23, and to drive slide plate 22a, 22b on ring stand 21 be the action that rotates of Z axle around ring stand 21 axle center.
Referring to Fig. 6, shown in 7, gear frame panel assembly 4 includes frame plate 41, motor 42,43, worm screw 45, worm screw 45 is installed on the frame plate 41 by bearing arrangement 40, cooperate with conical gear 48 on worm screw 45 axle heads and drive worm screw 45 and rotate being installed with conical gear 47 on motor 43 axle heads, on motor 42 axle heads, be installed with cam 46, on frame plate 41 trailing flanks, pass through link 37 (referring to accompanying drawing 4,5) be connected with chute 27b, chute 27b and aforementioned said left and right sides slide plate 22a, slide block 27a on the 22b is connected, make frame plate 41 relative slide plate 22a, slide before and after the 22b to move and be connected, hard-wired screw rod cover 29 cooperates drive frame plate 41 to move forward and backward on 26 in nut sleeve 49 and the aforementioned said motor being fixed with on the frame plate 41, is provided with slide block 50a on frame plate 41 leading flanks.
Referring to accompanying drawing 8, shown in 9, specimen holder panel assembly 6 includes frame plate 61, sample box 62, sample cassette holder 63, bearing arrangement 64, worm gear 65, drive link 66, chute 50b, the slide block 50a sliding connection that said frame plate 41 leading flanks of chute 50b and preceding art are provided with, make frame plate 61 and frame plate 41 realize that planar slide is connected, sample cassette holder 63 is installed on the mounting hole of offering on the frame plate 61 by bearing arrangement 64, worm gear 65 is fixedly mounted on the sample cassette holder 63, worm gear 65 cooperates the product of drive cassette holder 63 to rotate with aforementioned said worm screw 45, sample box 62 is installed on the sample cassette holder 63, drive link 66 is fixedlyed connected with frame plate 61, be provided with a pair of bearing pin 67a at drive link 66,67b, and at bearing pin 67a, 67b is provided with bearing and cooperates with hard-wired cam 46 on aforementioned said motor 42 axle heads, drives drive link 66 and frame plate 61 and moves along the K direction.
The utility model is provided with the grating dish and cooperates the control motor to rotate with optoelectronic switch on 25,26,42,43 in motor, the optoelectronic switch 36,56 that is provided with on grating dish 34,44 and the motor link that is provided with on 26,42 in motor shown in accompanying drawing 3,7 cooperates and controls the motor rotation.Being provided with limit switch 38,39 on ring stand 21 sides cooperates spacing with slide plate 22b.

Claims (2)

1, X-ray diffractometer multifunctional sample holder is characterized in that including base (1), ring stand device (2), gear frame panel assembly (4), specimen holder panel assembly (6);
Ring stand device (2) includes ring stand (21), left and right sides slide plate (22a, 22b), tooth plate (23), worm screw (24), motor (25,26), slide block (27a), on ring stand (21) inner ring surface, offer chute (28), tooth plate (23) is slidingly matched with chute (28), worm screw (24) on being provided with worm-gear toothing on the tooth plate (23) and being installed in ring stand (21) cooperates transmission, left and right sides slide plate (22a, 22b) be slidingly matched by chute and fixedly connected with tooth plate (23) with ring stand (21), promptly at ring stand (21) side and left and right sides slide plate (22a, 22b) go up correspondence and offer V-shaped groove, in the V groove, be provided with ball (32) and form the chute sliding connection, motor (25) drives worm screw (24) and drives left and right sides slide plate (22a by tooth plate (23), 22b) go up rotation at ring stand (21), at left and right sides slide plate (22a, be provided with 22b) and connect slide block (27a), motor (26) is fixedlyed connected installation by link (30) with slide plate (22b), on motor (26) axle, be installed with screw rod cover (29), this ring stand device (2) drives worm screw (24) by motor (25), and worm screw (24) drives tooth plate (23) and drives slide plate (22a, 22b) go up around ring stand (21) axle center promptly the action that rotates of (Z) axle at ring stand (21);
Gear frame panel assembly (4) includes frame plate (41), motor (42,43), worm screw (45), worm screw (45) is installed on the frame plate (41) by bearing arrangement (40), cooperate with conical gear (48) on worm screw (45) axle head and drive worm screw (45) and rotate being installed with conical gear (47) on motor (43) axle head, on motor (42) axle head, be installed with cam (46), on frame plate (41) trailing flank, be connected with chute (27b) by link (37), chute (27b) and left and right sides slide plate (22a, slide block 22b) (27a) is connected, make frame plate (41) slide plate (22a relatively, slide 22b) to move and be connected, be fixed with nut sleeve (49) at frame plate (41) and cooperate drive frame plate (41) to move forward and backward with hard-wired screw rod cover (29) on motor (26) axle, on frame plate (41) leading flank, be provided with slide block (50a);
Specimen holder panel assembly (6) includes frame plate (61), sample box (62), sample cassette holder (63), bearing arrangement (64), worm gear (65), drive link (66), chute (50b), slide block (50a) sliding connection that chute (50b) and frame plate (41) leading flank are provided with, make frame plate (61) and frame plate (41) realize that planar slide is connected, sample cassette holder (63) is installed on the mounting hole of offering on the frame plate (61) by bearing arrangement (64), worm gear (65) is fixedly mounted on the sample cassette holder (63), worm gear (65) cooperates drive product cassette holders (63) to rotate with preceding worm screw (45), sample box (62) is installed on the sample cassette holder (63), drive link (66) is fixedlyed connected with frame plate (61), be provided with a pair of bearing pin (67a at drive link (66), 67b), and at bearing pin (67a, 67b) be provided with bearing and cooperate, drive drive link (66) and frame plate (61) and move along (K) direction with hard-wired cam (46) on motor (42) axle head.
2, X-ray diffractometer multifunctional sample holder according to claim 1 is characterized in that being provided with the grating dish and cooperates the control motor to rotate with optoelectronic switch on motor (25,26,42,43) axle; Being provided with limit switch (38,39) on ring stand (21) side cooperates spacing with slide plate (22b).
CNU2008200106627U 2008-02-02 2008-02-02 Multifunctional example frame for X-ray diffraction instrument Expired - Lifetime CN201159722Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNU2008200106627U CN201159722Y (en) 2008-02-02 2008-02-02 Multifunctional example frame for X-ray diffraction instrument

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNU2008200106627U CN201159722Y (en) 2008-02-02 2008-02-02 Multifunctional example frame for X-ray diffraction instrument

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Publication Number Publication Date
CN201159722Y true CN201159722Y (en) 2008-12-03

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101231255B (en) * 2008-02-02 2010-08-25 丹东方圆仪器有限公司 Multifunctional sample shelf for X-ray diffractometer
CN105403541A (en) * 2014-09-10 2016-03-16 冠研(上海)企业管理咨询有限公司 Sample adjustment controller
CN105468026A (en) * 2014-09-10 2016-04-06 冠研(上海)企业管理咨询有限公司 Sample adjusting controller with three degrees of freedom
CN105466963A (en) * 2014-09-10 2016-04-06 冠研(上海)企业管理咨询有限公司 Electron microscope having sample adjustment controller
CN105468027A (en) * 2014-09-10 2016-04-06 冠研(上海)企业管理咨询有限公司 Sample adjusting controller of superhigh vacuum degree
CN105466739A (en) * 2014-09-10 2016-04-06 冠研(上海)企业管理咨询有限公司 Photo electron spectroscopy equipment having sample adjustment controller
CN105466962A (en) * 2014-09-10 2016-04-06 冠研(上海)企业管理咨询有限公司 Sample adjustment controller having oxygen free copper material
CN110961171A (en) * 2018-09-30 2020-04-07 中国科学院上海微系统与信息技术研究所 Low-temperature sample support

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101231255B (en) * 2008-02-02 2010-08-25 丹东方圆仪器有限公司 Multifunctional sample shelf for X-ray diffractometer
CN105403541A (en) * 2014-09-10 2016-03-16 冠研(上海)企业管理咨询有限公司 Sample adjustment controller
CN105468026A (en) * 2014-09-10 2016-04-06 冠研(上海)企业管理咨询有限公司 Sample adjusting controller with three degrees of freedom
CN105466963A (en) * 2014-09-10 2016-04-06 冠研(上海)企业管理咨询有限公司 Electron microscope having sample adjustment controller
CN105468027A (en) * 2014-09-10 2016-04-06 冠研(上海)企业管理咨询有限公司 Sample adjusting controller of superhigh vacuum degree
CN105466739A (en) * 2014-09-10 2016-04-06 冠研(上海)企业管理咨询有限公司 Photo electron spectroscopy equipment having sample adjustment controller
CN105466962A (en) * 2014-09-10 2016-04-06 冠研(上海)企业管理咨询有限公司 Sample adjustment controller having oxygen free copper material
CN105466963B (en) * 2014-09-10 2018-02-13 冠研(上海)专利技术有限公司 Electron microscope with sample adjustment controller
CN105468027B (en) * 2014-09-10 2018-03-23 冠研(上海)专利技术有限公司 Sample adjustment controller with ultrahigh vacuum degree
CN105468026B (en) * 2014-09-10 2018-04-03 冠研(上海)专利技术有限公司 Sample adjustment controller with three degree of freedom
CN105466962B (en) * 2014-09-10 2018-04-06 冠研(上海)专利技术有限公司 Sample adjustment controller with oxygenless copper material
CN105403541B (en) * 2014-09-10 2018-06-29 冠研(上海)专利技术有限公司 Sample adjusts controller
CN110961171A (en) * 2018-09-30 2020-04-07 中国科学院上海微系统与信息技术研究所 Low-temperature sample support
CN110961171B (en) * 2018-09-30 2021-11-02 中国科学院上海微系统与信息技术研究所 Low-temperature sample support

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GR01 Patent grant
AV01 Patent right actively abandoned

Granted publication date: 20081203

Effective date of abandoning: 20080202