CN201034842Y - Sample valve and reactor equipped with the same - Google Patents

Sample valve and reactor equipped with the same Download PDF

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Publication number
CN201034842Y
CN201034842Y CNU2007200036691U CN200720003669U CN201034842Y CN 201034842 Y CN201034842 Y CN 201034842Y CN U2007200036691 U CNU2007200036691 U CN U2007200036691U CN 200720003669 U CN200720003669 U CN 200720003669U CN 201034842 Y CN201034842 Y CN 201034842Y
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China
Prior art keywords
sampling
shuttle
sample
sample valve
concave area
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Expired - Lifetime
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CNU2007200036691U
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Chinese (zh)
Inventor
许培圣
金宝华
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Jiangsu Fullmark Chemicals Co., Ltd.
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许培圣
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Priority to CNU2007200036691U priority Critical patent/CN201034842Y/en
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Publication of CN201034842Y publication Critical patent/CN201034842Y/en
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  • Sampling And Sample Adjustment (AREA)

Abstract

Disclosed is a sampling valve which comprises a body. The body comprises an end part extending to a sampling area, a sampling shuttle reciprocating inside the body and a driver driving the sampling shuttle to reciprocate for sampling according to the needs. A concave area is arranged near a front end guide part on the sampling shuttle. When in the sampling preparation position, the concave area is dead against a via on the end part of the body along the circumference. When in the sampling execution position, the sampling shuttle is moved to the outermost end, the concave area is connected with a sampling opening of the body and the front end guide part closes a channel to the inside. A joint where the body and the sampling area connect is provided with a sealing. The driver is a screw rod device, comprising a screw rod connected with a rear end of the sampling shuttle and a rotation nut fixedly supported on an outer shell. The screw rod device can be provided with a bearing and the rotation nut which is connected with an inner ring of the bearing and connected through a key and rotated by a handwheel. The driver can also be a reciprocating mechanism driven by a cylinder body which can automatically control and execute sampling according to the set program. The invention also comprises a reaction vessel provided with the sampling valve.

Description

A kind of sample valve and the reactor that is equipped with this sample valve
Invention field
The utility model relates generally to a kind of sample valve, particularly a kind of sample valve of using in the Chemical Manufacture flow process of being suitable for, and the reactor that is equipped with this sample valve.
Background technology
To use sampling continually in each flow process of Chemical Manufacture,, carry out supervision control producing by online or non-online sampling analysis.For example, reactor of the prior art, generally be reacted to mid-term in chemical products will be to product sampling to analyze its every index, then according to result or the affirmation analyzed or make further adjustment.Common sampling method then often will be ended to stir, and ends heating.This not only can make reaction discontinuous, and static sampling down with dynamically down sampling in fact be exist discrepant.In addition, even be not as above-mentioned parking sampling, and the sample valve that uses existing some sample valve, promptly is communicated in the still, adopts common stop valve to control, also have and cause the distortion sampling because of material in the previous sample pipe is residual, perhaps the product material that need discharge volume for the sampling of getting rid of distortion causes the defective of waste or the like.Therefore, expectation has the sample valve that is suitable for using in the Chemical Manufacture flow process and be convenient to be provided with according to demand the sort of type of sampling.Also demand structure is simple, easy and simple to handle simultaneously, the more such sample valves that make things convenient for installation and maintenance and definitely reflect the immediate reaction situation, and the reactor that is provided with this sample valve, or Chemical Manufacture equipment.
Summary of the invention
The present invention is a purpose to satisfy above-mentioned actual demand.A kind of sample valve, it has comprised a body, and this body has an end that extends to sampling area, and one back and forth in this intrinsic sampling shuttle and a driver that makes this sampling shuttle carry out back and forth to take a sample by demand.Closing on the front end guide part on the described sampling shuttle has a concave area, and when being in the sampling ready position, this concave area is over against the through hole of body end along the circumference place; And be moved to outermost end, this moment this concave area and communicate with a sample tap on the body when being in sampling executing location time sampling shuttle, this front end guide part is then sealing the passage with inside.This body is provided with packoff in the junction with sampling area.Driver can be a kind of screw device, and it comprises that one is connected to the screw rod of this sampling shuttle rear end and is fixedly supported on the shell one rotation nut.Described screw device can also include rolling bearing and be connected in this rolling bearing the rotation nut with the handwheel rotation on the ring and that is connected by key.Described driver can also be a kind of reciprocator that is driven by cylinder body, and it can be controlled automatically according to preset program and carry out sampling.
A kind of reactor, its housing is provided with sample valve, and this sample valve has above-mentioned any characteristics.
Preferred embodiment below with reference to drawings attached is further explained the utility model, and those skilled in the art can therefrom recognize potential other many purposes and the advantages among the present invention.
Description of drawings
Fig. 1 is the vertical cross-sectional schematic of sample valve by preferred embodiment of the present invention,
Synoptic diagram when Fig. 2 is in the sampling executing location for sample valve among Fig. 1,
Fig. 3 is the sample valve similar with Fig. 1, but its driver be the reciprocator that drives by cylinder body a kind of sample valve synoptic diagram and
Fig. 4 is that K is to the view synoptic diagram among Fig. 3, and in order to represent another kind of through hole and recess structure, wherein sample valve is in the sampling executing location, and irrelevant member has been done partly to omit.
Specific implementation method
Now a kind of sample valve is described in the mode more more detailed than above general introduction.
Yet, before describing the present invention in detail, need give statement, the present invention is not limited to for example concrete of the description of doing.Can make various variations to described the present invention and replace not deviating from aim of the present invention and scope with equivalent.Unless otherwise defined, in that these all used technology scientific and technical terms should to do common understanding identical with those of ordinary skill in the technical field of the invention.
Sample valve by a preferred embodiment of the present utility model has been shown among Fig. 1.
This sample valve, it can comprise a body apparatus 20.As shown in the figure, this body apparatus 20 has a body 201, and the cylindrical ends 2011 that extends to a sampling area is arranged on it.And so-called sampling area can be any suitable chemical industry facility, for example is reactor 10 (only schematically showing a part among the figure), can certainly be in the Chemical Manufacture flow process place's pipeline sampled point, or the like.
Body apparatus 20 also includes a back and forth sampling shuttle 202 in this body 201, and the driver 30 that sampling shuttle 202 is back and forth taken a sample by the demand execution, or 31.
On sampling shuttle 202, close on guide part 2022 places of front end, have a concave area 2021.Concave area 2021 can be to form a cylindric ring groove of making on the right cylinder that is slidingly matched with cylindrical ends 2011 inside surfaces.When sample valve be in the sampling ready position, promptly during as shown in Figure 1 position; The through hole 2012 of this concave area 2021 over against body end 2011 along the circumference place; And when sample valve be in the sampling executing location, promptly during as shown in Figure 2 position, sampling shuttle 202 is subjected to the back and forth driver 30 of sampling, or 31 driving is moved to outermost end.Sample tap 2013 on this moment this concave area 2021 and the body 201 just constitutes and communicates, like this by instantaneous acquiring to, the sampling material of transient response state can carry out assay by sample tap 2013 taking-ups in the sign flow process.And the front end guide part 2022 of the shuttle 202 of this moment taking a sample is owing to be a kind of being slidingly matched, it and cylindrical ends 2011 inside surfaces are radially almost very close to each other, and can close and inner passage, and then with, for example still in the possible high heat of high pressure (or differ from normality) reaction zone form and isolate.And the sampling shuttle is exactly according to demand, or according to the manipulation of predefined program by driver in sampling ready position and the reciprocating action between the executing location of taking a sample.
In addition, above-mentioned through hole 2012 can be diversified, and quantity also is not limited to single.For example just represented other a kind of form in Fig. 4, through hole 2012 can be a kind of to be circular-arc through hole with the slotting cutter side edge from what two side direction of cylindrical ends 2011 inwardly milled out.Similar with it, the shape of concave area 2021 also can be to make the ring groove that is circular-arc.
Be exactly after sample tap 2013, to be (figure does not show) that to be arranged to be connected in addition with the robotization experiment device.And the product stream in the reaction is realized online detection and chemical examination by corresponding facility, and by the running of a control system reaction conditions is done adaptive adjustment according to assay, and realize the automatic control of production procedure.For ease of the taking-up that is sampled, also can be equipped with gas hole of may command pressure or the like on the opposite of sample tap 2013.
Body apparatus 20 is with chemical production equipment, for example the junction of the sampling area of a reactor 10 also is provided with packoff 2014 (seeing Fig. 1 for details).Its effect is to form with reaction zone to isolate sealing.
30 of drivers can be a kind of screw devices.As an example, it can comprise a screw rod 301 that is connected to these sampling shuttle 201 rear ends, and is fixedly supported to a rotation nut 302 on the shell 306.At the screw device shown in this, also include rolling bearing 303, be connected to this rolling bearing 303 in ring go up and pass through a kind of rotation nut 302 that handwheel 305 rotates by what flat key 304 was connected.Obvious this configuration is not unique.Any suitable screw mechanism all is fine in the prior art.Such as, for simplicity, rotation nut 302 can be to be supported in (figure does not show) on the axial constrained axle sleeve type bearing.
As a kind of replacement scheme, driver can also be a kind of reciprocator 31 that is driven by cylinder body, as shown in Figure 3.And this set is particularly suitable for on-line automatic control model.It includes a piston rod 312 that is connected with shuttle 201 rear ends of taking a sample, and coupled piston 313; Piston 313 is contained within the cylinder cover 316.Cylinder cover 316 two ends have end cap 311,315 respectively.Dispose and control the pipe adapter 314 that the pipe system (figure do not show) of fluid is joined on the end cap 311,315.The fluid of control fluid piping system both can be a hydraulic pressure, also can be pneumatic.Control fluid drives sampling shuttle according to the preset program of design and carry out sampling, assay or the like.Promptly can be implemented in the automatic control of line as previously mentioned.
Sample valve of the present invention can be used in various suitable Chemical Manufacture equipments.For example can be but not only limit be reactor.
A kind of reactor 10, promptly as schematically showing in the accompanying drawing, its housing 101 is provided with sample valve.Sample valve has comprised a body 201, and body 201 has 2011, one a reciprocal sampling shuttle 202 and the drivers 30,31 that make this sampling shuttle 202 carry out back and forth to take a sample by demand in this body 201 in end that extend to sampling area.Closing on front end guide part 2022 on the sampling shuttle 202 has a concave area 2021, when being in the sampling ready position, and the through hole 2012 of this concave area 2021 over against body end along the circumference place; And communicate with a sample tap 2013 on the body 201 when sampling executing location time sampling shuttle is moved to outermost end, this moment this concave area, this front end guide part 2022 is then sealing the passage with inside.
Though the present invention is described with reference to the various characteristics with single example and selectable combination, the present invention is not limited to for example concrete of the description of doing.Self-evident, for the purpose that realizes invention, many modifications of narration being done for the adaptation actual conditions are included within the scope of these claims of doing.

Claims (8)

1. sample valve, it is characterized by it and comprised a body (20), this body has an end (2011) that extends to sampling area (101), and one back and forth in this intrinsic sampling shuttle (202) and a driver (30,31) that makes this sampling shuttle carry out back and forth to take a sample by demand.
2. by the sample valve of claim 1, it is characterized by and close on front end guide part (2022) on the wherein said sampling shuttle (202) concave area (2021) is arranged, when being in the sampling ready position, the through hole (2012) of this concave area over against body end along the circumference place; And be moved to outermost end, this moment this concave area and communicate with a sample tap (2013) on the body when being in sampling executing location time sampling shuttle, this front end guide part (2022) is then sealing the passage with inside.
3. by the sample valve of claim 1, it is characterized by wherein said body and be provided with packoff (2014) in junction with sampling area (101).
4. by the sample valve of claim 1, it is characterized by wherein said driver (30) is a kind of screw device, and it comprises that one is connected to the screw rod (301) of this sampling shuttle rear end and of being fixedly supported on the shell (306) rotates nut (302).
5. by the sample valve of claim 4, it is characterized by wherein said screw device (30), also include rolling bearing (303) and be connected to the rotation nut (302) of using handwheel (305) to rotate that also is connected on the ring in this rolling bearing by key (304).
6. by the sample valve of claim 1, it is characterized by wherein said driver is a kind of reciprocator (31) that is driven by cylinder body, and this reciprocator (31) takes a sample according to programmed control.
7. reactor, its housing (10) is provided with sample valve, it is characterized by wherein said sample valve and comprised a body (20), this body has an end (2011) that extends to sampling area (101), one back and forth in this intrinsic sampling shuttle (202) and a driver (30,31) that makes this sampling shuttle carry out back and forth to take a sample by demand.
8. press the reactor of claim 7, it is characterized by and close on front end guide part (2022) on the wherein said sampling shuttle concave area (2021) is arranged, when being in the sampling ready position, the through hole (2012) of this concave area (2021) over against body end along the circumference place; And be moved to outermost end, this moment this concave area and communicate with a sample tap (2013) on the body when being in sampling executing location time sampling shuttle, this front end guide part (2022) is then sealing the passage with inside.
CNU2007200036691U 2007-01-24 2007-01-24 Sample valve and reactor equipped with the same Expired - Lifetime CN201034842Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNU2007200036691U CN201034842Y (en) 2007-01-24 2007-01-24 Sample valve and reactor equipped with the same

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNU2007200036691U CN201034842Y (en) 2007-01-24 2007-01-24 Sample valve and reactor equipped with the same

Publications (1)

Publication Number Publication Date
CN201034842Y true CN201034842Y (en) 2008-03-12

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CNU2007200036691U Expired - Lifetime CN201034842Y (en) 2007-01-24 2007-01-24 Sample valve and reactor equipped with the same

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102798551A (en) * 2011-05-27 2012-11-28 崔坤华 Closed quantitative sampling valve and manufacturing method thereof
CN107255667A (en) * 2017-07-07 2017-10-17 安庆泽远化工有限公司 A kind of detection means for aluminium-hydroxide powder fire retardant

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102798551A (en) * 2011-05-27 2012-11-28 崔坤华 Closed quantitative sampling valve and manufacturing method thereof
CN107255667A (en) * 2017-07-07 2017-10-17 安庆泽远化工有限公司 A kind of detection means for aluminium-hydroxide powder fire retardant

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
ASS Succession or assignment of patent right

Owner name: JIANGSU FULING CHEMICAL INDUSTRY CO., LTD.

Free format text: FORMER OWNER: XU PEISHENG

Effective date: 20090417

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20090417

Address after: No. 105 Yingbin West Road, Lingang Town, Lingang Town, Jiangsu, Jiangyin: 214445

Patentee after: Jiangsu Fullmark Chemicals Co., Ltd.

Address before: No. 105 Yingbin West Road, Jiangyin, Jiangsu, Jiangyin second synthetic chemical plant, postcode: 214445

Patentee before: Xu Peisheng

CX01 Expiry of patent term

Granted publication date: 20080312

EXPY Termination of patent right or utility model