CN1985613A - Production process of vitamin A peanut oil - Google Patents
Production process of vitamin A peanut oil Download PDFInfo
- Publication number
- CN1985613A CN1985613A CNA2006101462535A CN200610146253A CN1985613A CN 1985613 A CN1985613 A CN 1985613A CN A2006101462535 A CNA2006101462535 A CN A2006101462535A CN 200610146253 A CN200610146253 A CN 200610146253A CN 1985613 A CN1985613 A CN 1985613A
- Authority
- CN
- China
- Prior art keywords
- peanut oil
- vitamin
- reaction
- order reaction
- standard
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Landscapes
- Edible Oils And Fats (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The production process of vitamin A peanut oil includes the following steps: 1. inspecting the physical and chemical indexes of first grade peanut oil based on GB1546-2003 standard; 2. mixing the peanut oil and vitamin A acetate in the weight ratio of 100000 to 6.65-13.30 in the first reactor at normal pressure and 40 -120deg.c via stirring at 30-80 rpm to produce the first reaction for 60-80 min; 3. measuring the over gasification value, acid number, vitamin A content of the product, and finishing the first reaction after reaching the required indexes; 4. mixing the first reacted oil in 1 weight portions and first grade peanut oil in 4 weight portions in the second reactor at normal pressure and 40 -120deg.c via stirring at 20-60 rpm to produce the second reaction for 60-120 min, and detecting the product indexes regularly until reaching the standard; and 5. light-proof packing.
Description
One, technical field
The present invention relates to the edible oil field, particularly a kind of production method of vitamin A peanut oil.
Two, background technology
The content of existing peanut oil vitamin A is lower, has only 480-500 μ g/kg, shows that according to the nutrition survey data there is the VAD situation in domestic part resident, influences healthyly, and especially childhood dystrophy has been a worldwide problem.A national nutrition survey shows, China's city student's vitamin A intake is the 59%-76% of RDA (recommended intake), rural students power is the 48%-57% of RDA, and indivedual poverty-stricken areas only are 30%, and the shortage of vitamin A is exactly the key factor that concerns that people are healthy.
Three, summary of the invention
The production method that the purpose of this invention is to provide a kind of improved vitamin A peanut oil, shortcoming or deficiency that it can overcome effectively or avoid existing in the above-mentioned prior art increase the content of peanut oil vitamin effectively, improve the health of people level.
The production method of vitamin A peanut oil of the present invention, its processing step carries out physical and chemical inspection for (A) to one-level peanut oil, to reach the GB1546-2003 standard, further comprising the steps of: as (B) one-level peanut oil to be pumped in the first class reaction pot, the vitamin A amyl acetate that adds weight ratio 100000: 6.65-13.30 again carried out first order reaction 60-80 minute under normal pressure 40-120 ℃, 30-80 rev/min stirring; (C) content of crossing gasification value, acid number, vitamin A of mensuration grease, first order reaction is finished in qualified back; (D) the first order reaction oil pump of 1 part of weight portion is gone into the second order reaction jar, pump into the one-level peanut oil of 4 parts of weight portions again, under normal pressure 40-120 ℃, 20-60 rev/min stirring, carried out second order reaction 60-120 minute, in this course of reaction, the various physical and chemical indexs of testing product regularly finish second order reaction after reaching standard; (E) with product according to national standard and company standard, it is canned to carry out product with conventional compound anti-light technology.
Wherein, the flow process of the production method of described vitamin A peanut oil is that the peanut oil storage tank is connected first class reaction pot by pump with pipeline, is connected first class reaction pot and second order reaction jar with pump by pipeline.Described firsts and seconds retort is provided with temperature-measuring port and detects sample tap.
The present invention has following advantage compared with prior art:
1, second order reaction technology: first order reaction density is higher, and second level reaction density is within standard.Vitamin A content is controlled between the 4000-8000 μ g/kg in the oil, and second order reaction had both guaranteed that vitamin A was evenly distributed in product, can effectively control concentration content again.
2, Yan Ge temperature: vitamin A is very responsive to temperature, and the too high easy generation oxidation of temperature is crossed the low production reaction not exclusively, by experiment repeatedly, finds specific temperature of phase.
3, compound anti-light packing technique: vitamin A places under the light direct projection for a long time, and oxidation deterioration easily takes place, and compound anti-light packing effectively suppresses the light irradiation, and anti-oxidation takes place, and has guaranteed the content of vitamin A in the product.
Four, description of drawings
Accompanying drawing is a reaction process structural representation of the present invention.
Five, the specific embodiment
Consult accompanying drawing, a kind of production method of vitamin A peanut oil, its processing step carries out physical and chemical inspection for (A) to one-level peanut oil, to reach the GB1546-2003 standard, further comprising the steps of: as (B) one-level peanut oil to be pumped in the first class reaction pot, the vitamin A amyl acetate that adds weight ratio 100000: 6.65-13.30 again carried out first order reaction 60-80 minute under normal pressure 40-120 ℃, 30-80 rev/min stirring; (C) content of crossing gasification value, acid number, vitamin A of mensuration grease, first order reaction is finished in qualified back; (D) the first order reaction oil pump of 1 part of weight portion is gone into the second order reaction jar, pump into the one-level peanut oil of 4 parts of weight portions again, under normal pressure 40-120 ℃, 20-60 rev/min stirring, carried out second order reaction 60-120 minute, in this course of reaction, the various physical and chemical indexs of testing product regularly finish second order reaction after reaching standard; (E) with product according to national standard and company standard, it is canned to carry out product with conventional compound anti-light technology.
Provide three embodiment below:
Embodiment one: the production method of vitamin A peanut oil, its processing step carries out physical and chemical inspection for (A) to one-level peanut oil, to reach the GB1546-2003 standard, further comprising the steps of: as (B) one-level peanut oil to be pumped in the first class reaction pot, add 100000: 6.65 vitamin A amyl acetate of weight ratio again, under 40 ℃ of normal pressures, 30 rev/mins of stirrings, carried out first order reaction 60 minutes; (C) content of crossing gasification value, acid number, vitamin A of mensuration grease, first order reaction is finished in qualified back; (D) the first order reaction oil pump of 1 part of weight portion is gone into the second order reaction jar, pump into the one-level peanut oil of 4 parts of weight portions again, under 40 ℃ of normal pressures, 20 rev/mins of stirrings, carried out second order reaction 60 minutes, in this course of reaction, the various physical and chemical indexs of testing product regularly finish second order reaction after reaching standard; (E) with product according to national standard and company standard, it is canned to carry out product with conventional compound anti-light technology.
Embodiment two: the production method of vitamin A peanut oil, its processing step carries out physical and chemical inspection for (A) to one-level peanut oil, to reach the GB1546-2003 standard, further comprising the steps of: as (B) one-level peanut oil to be pumped in the first class reaction pot, add 100000: 13.30 vitamin A amyl acetate of weight ratio again, under 120 ℃ of normal pressures, 80 rev/mins of stirrings, carried out first order reaction 80 minutes; (C) content of crossing gasification value, acid number, vitamin A of mensuration grease, first order reaction is finished in qualified back; (D) the first order reaction oil pump of 1 part of weight portion is gone into the second order reaction jar, pump into the one-level peanut oil of 4 parts of weight portions again, under 120 ℃ of normal pressures, 80 rev/mins of stirrings, carried out second order reaction 120 minutes, in this course of reaction, the various physical and chemical indexs of testing product regularly finish second order reaction after reaching standard; (E) with product according to national standard and company standard, it is canned to carry out product with conventional compound anti-light technology.
Embodiment three: the production method of vitamin A peanut oil, its processing step carries out physical and chemical inspection for (A) to one-level peanut oil, to reach the GB1546-2003 standard, further comprising the steps of: as (B) one-level peanut oil to be pumped in the first class reaction pot, add 100000: 10.00 vitamin A amyl acetate of weight ratio again, at normal pressure, under 80 ℃, the 50 rev/mins stirrings, carried out first order reaction 70 minutes; (C) content of crossing gasification value, acid number, vitamin A of mensuration grease, first order reaction is finished in qualified back; (D) the first order reaction oil pump of 1 part of weight portion is gone into the second order reaction jar, pump into the one-level peanut oil of 4 parts of weight portions again, at normal pressure, under 80 ℃, the 30 rev/mins stirrings, carried out second order reaction 90 minutes, in this course of reaction, the various physical and chemical indexs of testing product regularly finish second order reaction after reaching standard; (E) with product according to national standard and company standard, it is canned to carry out product with conventional compound anti-light technology.
The production method flow process of vitamin A peanut oil comprises that first class reaction pot 2 is connected with second order reaction jar 3 with one-level peanut oil tank 1 respectively with pump 6 by pipeline 7.Temperature survey mouth 4 and sample tap 5 all are installed on first class reaction pot and the second order reaction jar.
Claims (3)
1, a kind of production method of vitamin A peanut oil, its processing step carries out physical and chemical inspection for (A) to one-level peanut oil, to reach the GB1546-2003 standard, it is characterized in that further comprising the steps of: (B) one-level peanut oil is pumped in the first class reaction pot, the vitamin A amyl acetate that adds weight ratio 100000: 6.65-13.30 again carried out first order reaction 60-80 minute under normal pressure 40-120 ℃, 30-80 rev/min stirring; (C) content of crossing gasification value, acid number, vitamin A of mensuration grease, first order reaction is finished in qualified back; (D) the first order reaction oil pump of 1 part of weight portion is gone into the second order reaction jar, pump into the one-level peanut oil of 4 parts of weight portions again, under normal pressure 40-120 ℃, 20-60 rev/min stirring, carried out second order reaction 60-120 minute, in this course of reaction, the various physical and chemical indexs of testing product regularly finish second order reaction after reaching standard; (E) with product according to national standard and company standard, it is canned to carry out product with conventional compound anti-light technology.
2, a kind of flow process of production method of vitamin A peanut oil is that the peanut oil storage tank is connected first class reaction pot by pump with pipeline, is connected first class reaction pot and second order reaction jar with pump by pipeline.
3, the production method of vitamin A peanut oil according to claim 2 is characterized in that described firsts and seconds retort is provided with temperature-measuring port and detects sample tap.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006101462535A CN100515218C (en) | 2006-12-14 | 2006-12-14 | Production process of vitamin A peanut oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006101462535A CN100515218C (en) | 2006-12-14 | 2006-12-14 | Production process of vitamin A peanut oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1985613A true CN1985613A (en) | 2007-06-27 |
| CN100515218C CN100515218C (en) | 2009-07-22 |
Family
ID=38182657
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006101462535A Expired - Fee Related CN100515218C (en) | 2006-12-14 | 2006-12-14 | Production process of vitamin A peanut oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100515218C (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102919385A (en) * | 2012-11-20 | 2013-02-13 | 曾晓飞 | Novel food with rich omega 3 compound food supplements |
-
2006
- 2006-12-14 CN CNB2006101462535A patent/CN100515218C/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102919385A (en) * | 2012-11-20 | 2013-02-13 | 曾晓飞 | Novel food with rich omega 3 compound food supplements |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100515218C (en) | 2009-07-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Soo et al. | Reversing methanogenesis to capture methane for liquid biofuel precursors | |
| Rao et al. | Respiration and denitrification in permeable continental shelf deposits on the South Atlantic Bight: Rates of carbon and nitrogen cycling from sediment column experiments | |
| CN205146108U (en) | Quick gas -liquid looks balancing unit under high pressure condition | |
| CN202486030U (en) | Simulative corrosion tester for upper deck on oil cargo tank | |
| Schultz et al. | Sulfite oxidation as a measure of aeration effectiveness | |
| CN100515218C (en) | Production process of vitamin A peanut oil | |
| CN201532329U (en) | Experiment device of seabed gas hydrates | |
| CN203117149U (en) | Device for simulating evaluation of natural gas hydrate inhibitor by using tetrahydrofuran | |
| CN112816379A (en) | Device and method for measuring particle concentration of solid-liquid two-phase flow pump based on electric signals | |
| CN102590108A (en) | Method for quickly and efficiently detecting content of trace elements in quartz sand through microwave digestion | |
| Novelli et al. | Hydrogen distributions in marine sediments 1, 2 | |
| Li et al. | Evaluation of experimental setup and procedure for rapid preparation of natural gas hydrate | |
| CN101520394A (en) | Method for determining anaerobic sludge activity | |
| CN109856126B (en) | Method for rapidly detecting corrosion rate of chelated acid | |
| Sugai‐Guérios et al. | Mathematical model of the CO2 solubilisation reaction rates developed for the study of photobioreactors | |
| CN203479678U (en) | Strong-acid resistant static high-temperature and high-pressure kettle | |
| CN101368902A (en) | Method for measuring silicon dioxide content in oil-contaminated water of oil field | |
| CN201749113U (en) | Natural gas hydrate decomposition rate experimental device | |
| CN203249584U (en) | Detection tooling for bearing box of pump | |
| CN106986956A (en) | A kind of preparation method for being crosslinked synanthrin | |
| CN101819138A (en) | Measuring method of activity of beta-glucanase | |
| Xianfang et al. | Application of lithium isotopes in genetic study of pegmatite deposits | |
| Vavilin et al. | Dynamic isotope equations for 13CH4 and 13CO2 describing methane formation with a focus on the effect of anaerobic respiration in sediments of some tropical lakes | |
| CN105699615A (en) | Online selective water quality detection method and equipment | |
| CN102353424B (en) | Triaxial liquid level meter with magnetic reversible column |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20090722 Termination date: 20100114 |