CN1981864A - Oil-solvent extraction of ginger extract - Google Patents
Oil-solvent extraction of ginger extract Download PDFInfo
- Publication number
- CN1981864A CN1981864A CNA2006100440666A CN200610044066A CN1981864A CN 1981864 A CN1981864 A CN 1981864A CN A2006100440666 A CNA2006100440666 A CN A2006100440666A CN 200610044066 A CN200610044066 A CN 200610044066A CN 1981864 A CN1981864 A CN 1981864A
- Authority
- CN
- China
- Prior art keywords
- oil
- rhizoma zingiberis
- zingiberis recens
- ginger
- gingerol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
A process for extracting the active components from ginger, even if poor-quality ginger includes such steps as breaking, preparing ginger juice, preparing ginger starch and ginger juice, extracting in oil, and separating ginger oil from gingerol. Its extracts include ginger starch, ginger oil, gingerol, amino acids and trace elements.
Description
Technical field
The present invention relates to a kind of oil-solvent extraction that from natural medicinal plant, extracts the method, particularly a kind of Rhizoma Zingiberis Recens extract of active substance.
Background technology
Rhizoma Zingiberis Recens is the bright rhizome of zingiberaceous plant zingiber offcinale Rose, be the important economic crops of China, not only can be used as natural spice, and have multiple uniqueness and significant biological activity and medical care effect, be a kind of traditional Chinese medicine, in China plantation is widely arranged, even if cold northern area also has plantation, but Rhizoma Zingiberis Recens all has disease to take place every year, especially bacterial wilt of ginger, endanger very greatly, cause low-quality, low yield, make peasant benefit be subjected to heavy losses.For many years, how solve on the problem of bacterial wilt of ginger and adopted many measures, but all eradicate, therefore, seek the approach of the comprehensive utilization of a sick Rhizoma Zingiberis Recens, mashed Rhizoma Zingiberis Recens, deteriorated ginger, will bring remarkable economic efficiency to the peasant.Many data show, Rhizoma Zingiberis Recens has multiple medical value, but directly use Rhizoma Zingiberis Recens, truly have many insurmountable problems, as supply inconvenience, too pungent, take difficulty, poor quality's control, the bad grasp of dosage etc., therefore extract the effective ingredient of Rhizoma Zingiberis Recens, use respectively, particular importance just seems.According to the interrelated data record, mainly having natural activity and natural flavour mountaineous composition in the Rhizoma Zingiberis Recens is oil of ginger and gingerol two big class materials.Oil of ginger is an oily liquids, and (((γ-munrolene), citral (eitral) etc. become to be grouped into for tens of kinds for β-phellandrene), γ-Cananga odorata oil alkene for α-zingiberene), β-phellandrene by zingiberol (zingiberrol), camphene (camphene), α-zingiberene.Gingerol is the main component that is multiple pharmacological effect in the Rhizoma Zingiberis Recens, and gingerol (gingerol) is made up of shogaol (N-shogaol) and gingerol series phenol analog derivatives such as (N-gingerol).Oil of ginger and gingerol are two the highest parts of medical value, this two part that present so-called extraction also mainly refers to.The chemical property of oil of ginger and gingerol is all unstable, in the storage of Rhizoma Zingiberis Recens raw material, deep processing, leaching process, oxidation, hydrolysis take place easily, wave the reactions such as reaching decomposition of loosing, be difficult to keep original natural activity and local flavor, and the physicochemical property difference of two active components, molecular polarity as the oil of ginger class is less, has volatility, gingerol quasi-molecule polarity is relatively large, do not have a volatility, their chemical property is all unstable, therefore, extract oil of ginger simultaneously and gingerol has certain difficulty, influenced the deep processing development utilization of Rhizoma Zingiberis Recens.The method of simple at present extraction oil of ginger is more, as steam distillation, percolation, infusion process, decocting method, cold-press, the use alcohol reflux extraction method that then has for simple extraction gingerol, more than the weak point of these methods be to extract oil of ginger, gingerol, amino acid of Rhizoma Zingiberis Recens and vitamin and microelement kind simultaneously, as cold-press, high-quality oil of ginger can be extracted, but gingerol can not be extracted; Decocting method can make oil of ginger lose fully; The way of distillation can only be extracted oil of ginger.Therefore, this has not only influenced the comprehensive development and utilization of Rhizoma Zingiberis Recens, has also influenced the production cost of oil of ginger and gingerol.Domestic generally acknowledged best extracting method is a supercritical CO at present
2Extraction can extract oil of ginger and gingerol simultaneously from Rhizoma Zingiberis Recens, the quality of its extraction is also higher, but significantly deficiency is: the one, and equipment investment is big, needs 100,000,000 yuans as a cover 500L France import equipment, has strengthened production cost; The 2nd, complicated operation generally will be cut Rhizoma Zingiberis earlier, and lyophilization again can extract after the pulverizing, is not suitable for the Rhizoma Zingiberis Recens large-scale industrial and extracts; The 3rd, because CO
2Polarity and gingerol difference to some extent, so relatively poor relatively to the gingerol extracting power, extraction yield is lower; The 4th, can not adopt mashed Rhizoma Zingiberis Recens, sick Rhizoma Zingiberis Recens, deteriorated ginger processing to extract, the comprehensive utilization of unresolved sick Rhizoma Zingiberis Recens, mashed Rhizoma Zingiberis Recens, deteriorated ginger does not fully reduce production costs and promotes the planting benefit of Jiang Nong; The 5th, do not extract amino acid of Rhizoma Zingiberis Recens and vitamin and microelement kind extract, production cost is further reduced.
Summary of the invention
The object of the present invention is to provide that a kind of equipment is simple, small investment, operation easily, can extract oil of ginger and gingerol and other effective extracts simultaneously, and can not only be to good Jiang Jinhang extraction, also can be to sick Rhizoma Zingiberis Recens, mashed Rhizoma Zingiberis Recens, deteriorated ginger extraction, thereby reduce production costs the oil-solvent extraction of a kind of Rhizoma Zingiberis Recens extract of the planting benefit of promotion Jiang Nong to greatest extent.
For reaching above purpose, the technical solution adopted in the present invention is: the oil-solvent extraction of this a kind of Rhizoma Zingiberis Recens extract, at first the Jiang Jinhang roguing is cleaned as the Rhizoma Zingiberis Recens raw material, and it is characterized in that it is realized by following steps: (1) fragmentation; (2) cross the elimination Rhizoma Zingiberis Recens dregs and make Rhizoma Zingiberis Recens juice; (3) starch in the Rhizoma Zingiberis Recens juice is separated, make Rhizoma Zingiberis Recens starch and destarch Sucus Zingberis: Rhizoma Zingiberis Recens starch can be packed separately, becomes isolated effective product, and the destarch Sucus Zingberis is as the raw material of next step extraction; (4) the destarch Sucus Zingberis is added the sealing of extraction oil preparation and mix the extraction of heating: the extraction oil preparation is a vegetable oil, and its extraction time is so that extract is divided into oil of ginger clearly is as the criterion with vitamin mixture layer, microelement kind mixing liquid layer with gingerol mixing liquid layer, aminoacid; (5) with stratified oil of ginger and gingerol mixing liquid layer, aminoacid and vitamin mixture layer, microelement kind mixing liquid layer extraction separation, be respectively charged into jar special: aminoacid and vitamin mixture and the independent packing of microelement kind mixed liquor, as product, the jar special that oil of ginger and gingerol mixed liquor are packed into and sealed is as the raw material of next step extraction; (6) separate oil of ginger and gingerol: oil of ginger and gingerol mixed liquor are packed into separately behind the jar special that seals, extract oil of ginger by squeezing again,, and isolate gingerol as the oil of ginger product, isolated gingerol, remaining oil of ginger and the aminoacid in the gingerol is removed in the washing of reuse pure water; (7) produce the gingerol powder: through the low-temperature vacuum drying powdering, bottling is product to isolated gingerol.Described vegetable oil is one of following or its combination of two kinds: oil of ginger, Oleum Arachidis hypogaeae semen, Oleum sesami, Oleum Glycines, Oleum Brassicae campestris, Petiolus Trachycarpi oil, Oleum Gossypii semen, Semen Maydis oil, sunflower oil, these vegetable oil all can buy from the market, and the adding proportion of vegetable oil is that 1000kg Rhizoma Zingiberis Recens raw material adds 2 to 3kg; Described vegetable oil is preferably oil of ginger, adopt oil of ginger to make the extraction oil preparation, can save oil of ginger and the isolating operation of extraction oil preparation, make operation more easy, test shows, vegetable oil has good affinity interaction to the molecule of oil of ginger and gingerol, and can produce the stratified character of extraction material, in addition, adopt Oleum Arachidis hypogaeae semen also relatively good as the extraction oil preparation, because Oleum Arachidis hypogaeae semen is easy to separate with oil of ginger at low temperatures, its operation is also easier; In broken step, describedly be broken for the low speed fragmentation, can adopt the stainless steel ball grinding machine, rotating speed is 30-80 rev/min, broken fineness is 100 orders, can reduce the loss of oil of ginger like this; Produce in the step of Rhizoma Zingiberis Recens juice crossing the elimination Rhizoma Zingiberis Recens dregs, described filtration can be adopted the typing oil press, and at normal temperatures, pressure is 5-8kg, carry out filter pressing and produce, this method than vacuum, centrifugal, to filter the oil of ginger loss little; Starch in the Rhizoma Zingiberis Recens juice is being separated in the step that makes Rhizoma Zingiberis Recens starch and destarch Sucus Zingberis, be to use the elimination Rhizoma Zingiberis Recens dregs to produce the Rhizoma Zingiberis Recens juice of producing in the Rhizoma Zingiberis Recens juice step, through 1-3 hour natural subsidence, isolate Rhizoma Zingiberis Recens starch, produce the destarch Sucus Zingberis simultaneously, this sedimentation can not be heated, the room temperature sedimentation, prevent to become pasty state, disturb extraction; In the step of extraction that destarch Sucus Zingberis adding extraction oil preparation sealing mixing is heated, after the destarch Sucus Zingberis adds extraction equipment, need add vegetable oil extraction oil preparation in proportion, sealing mixed 30-40 minute, it is fully mixed, heat again to 30-100 ℃, extracted 0.5-4 hour, make the extract in the extraction equipment can find out oil of ginger and gingerol mixing liquid layer clearly, aminoacid and vitamin mixture layer, can stop during microelement kind mixing liquid layer, also can be through pick test, can stop when requiring extraction yield for 95-98%, if do not reach the standard that extraction yield is 95-98%, continuing increases by 0.5 hour extraction time, makes the extract in the extraction equipment can find out oil of ginger and gingerol mixing liquid layer clearly, aminoacid and vitamin mixture layer, stop during microelement kind mixing liquid layer; In the step of separating oil of ginger and gingerol, to remove remaining oil of ginger and the storage of amino acid whose cleaning mixture in the gingerol with the pure water washing, return and the destarch Sucus Zingberis is added the sealing of extraction oil preparation mix in the extraction step of heating, to reduce oil of ginger and amino acid whose loss; In producing gingerol powder step, gingerol under 40-50 ℃ temperature, is become the yellow-gray powdered extract through vacuum drying, bottling becomes product again; Generally speaking the theoretical value of oil of ginger and gingerol accounts for 0.55% of raw material Rhizoma Zingiberis Recens total amount, and extraction yield is 95-98%; The theoretical value of aminoacid and vitamin accounts for 69.45% of raw material total amount, wherein contains Tianmen radon propylhomoserin, glycine, serine, glutamic acid etc. and vitamin B, C; Microelement kind mixing liquid layer contains calcium, zinc, ferrum, magnesium, nickel etc.; Clean in the step of Rhizoma Zingiberis Recens in roguing, remove silt, and good Rhizoma Zingiberis Recens and mashed Rhizoma Zingiberis Recens, pestilence Rhizoma Zingiberis Recens, deteriorated ginger are classified, processing extraction respectively, when making good use of the Rhizoma Zingiberis Recens extraction, to aminoacid and vitamin mixture and microelement kind mixed liquor after sterilizing, packing can be done food seasoning or food additive respectively; During with deteriorated ginger, mashed Rhizoma Zingiberis Recens, the extraction of pestilence Rhizoma Zingiberis Recens, to aminoacid and vitamin mixture and microelement kind mixed liquor production ginger special-purpose fertilizer after 100 ℃ of high-temperature sterilization sterilizations.The extract oil of ginger is for faint yellow, liquid; Extract gingerol powder is yellow-gray, fine-powdered, granule 80mesh, typical abnormal smells from the patient, humidity 5percentage, heavy metal 10ppmmax, non agricultural chemical residuum, total plate count 1000cfu/gmax, and assay method is that Hplc measures; Extract aminoacid and vitamin mixture when making good use of the Rhizoma Zingiberis Recens extraction, are apricot, and liquid state during with mashed Rhizoma Zingiberis Recens, deteriorated ginger, the extraction of pestilence Rhizoma Zingiberis Recens, is dark-brown, liquid state; Extract microelement kind mixed liquor, powdering is light gray after drying.
Beneficial effect of the present invention is: compare with the present conventional extracting method that uses, this method can not only be extracted oil of ginger, can also extract gingerol, aminoacid and vitamin, trace element and Rhizoma Zingiberis Recens starch simultaneously, and Rhizoma Zingiberis Recens is fully utilized fully; With supercritical CO
2Extraction is compared, and can not only extract oil of ginger and gingerol simultaneously, and equipment is simple, small investment, easy to operate, production cost is low, can also extract aminoacid and vitamin, trace element and Rhizoma Zingiberis Recens starch simultaneously, thereby production cost is reduced significantly.In addition, prior being also advantageous in that of this method adopts pestilence Rhizoma Zingiberis Recens, mashed Rhizoma Zingiberis Recens, deteriorated ginger to extract, and makes Rhizoma Zingiberis Recens reach comprehensive development and use, not only improved the economic benefit of Rhizoma Zingiberis Recens comprehensive process, also improved the planting benefit of Jiang Nong.
The specific embodiment
Embodiment 1
The Rhizoma Zingiberis Recens raw material adopts the local generation in Laiwu Rhizoma Zingiberis Recens, and mashed Rhizoma Zingiberis Recens, pestilence Rhizoma Zingiberis Recens 1000kg at first clean Rhizoma Zingiberis Recens, remove silt and impurity, produce according to the following steps again:
(1) fragmentation: to the Rhizoma Zingiberis Recens raw material that cleaned, carry out fragmentation in the stainless steel ball grinding machine of packing into, rotating speed is 50 rev/mins, and broken fineness is 100 orders;
(2) cross the elimination Rhizoma Zingiberis Recens dregs and produce Rhizoma Zingiberis Recens juice: the Rhizoma Zingiberis Recens raw material of fragmentation is packed in the typing oil press, its drainage screen is 120 orders, under normal temperature laboratory, pressure is that 5kg carries out filter pressing, elimination Cortex Zingiberis, Rhizoma Zingiberis Recens fiber and not broken thin Rhizoma Zingiberis Recens piece, make Rhizoma Zingiberis Recens juice, the Cortex Zingiberis that leaches, Rhizoma Zingiberis Recens fiber can be made feed additive after sterilization;
(3), the starch in the Rhizoma Zingiberis Recens juice is separated, make Rhizoma Zingiberis Recens starch and destarch Sucus Zingberis: the Rhizoma Zingiberis Recens juice that makes is put into the sealed plastic jar, natural subsidence 3 hours, get the destarch Sucus Zingberis, isolated Rhizoma Zingiberis Recens starch is packed separately as product after sterilizing, batching capable of using as feed, the destarch Sucus Zingberis is as next step raw materials for production;
(4), the destarch Sucus Zingberis is added the sealing of extraction oil preparation mix the extraction of heating: the destarch Sucus Zingberis is added in the extraction equipment, add the extraction oil preparation again, adopt oil of ginger as the extraction oil preparation, add 3kg extraction oil preparation, after adding the extraction oil preparation, under sealing state, mixed 35 minutes, heat again to 50 ℃, extracted 2 hours, after observing the clear layering of extract, stop extraction, also can pass through pick test, extraction yield reaches more than 95%, be layering after static half an hour, in extraction equipment, be divided into oil of ginger and gingerol mixing liquid layer from top to bottom successively, aminoacid and vitamin mixture layer, microelement kind mixing liquid layer, wherein oil of ginger and the gingerol mixing liquid layer the superiors are based on oil of ginger, and orlop is based on gingerol;
(5), with stratified oil of ginger and gingerol mixing liquid layer, aminoacid and vitamin mixture layer, microelement kind mixing liquid layer extraction separation, be respectively charged into jar special: extraction deposits in the jar special separately to the microelement kind mixed liquor earlier, again aminoacid and vitamin mixture are proposed separately to deposit in the corresponding jar special, at last oil of ginger and gingerol mixed liquor are deposited in separately in the corresponding sealing jar special by extracting;
(6), separate oil of ginger and gingerol: to being sealed in oil of ginger and the gingerol mixed liquor in the jar special, extract oil of ginger, separately bottling by squeezing, promptly get final products, and isolate gingerol, to isolated gingerol reuse pure water washing, remove remaining oil of ginger and aminoacid in the gingerol;
(7), produce the gingerol powder: isolated gingerol is packed in the drying baker,, become gingerol powder packing, promptly get final products through 45 ℃ of dryings;
(8), aminoacid and the vitamin mixture that proposes packed after sterilizing, can make ginger special-purpose fertilizer;
(9), the microelement kind mixed liquor to proposing, the powdering pack of drying sterilization back, its application process is with aminoacid and vitamin mixture.
Embodiment 2
The Rhizoma Zingiberis Recens raw material adopts that the Laiwu is local to produce Rhizoma Zingiberis Recens, and the Laiwu Rhizoma Zingiberis Recens 1000kg that enters factory is cleaned, and flush away silt and impurity have been Rhizoma Zingiberis Recens entirely, and (promptly not having speck, anosis Rhizoma Zingiberis Recens), its production stage is:
(1), fragmentation: to the Rhizoma Zingiberis Recens raw material that cleaned, it is 78 rev/mins that the stainless steel ball grinding machine of packing into carries out broken rotating speed, and broken fineness is 100 orders;
(2), cross the elimination Rhizoma Zingiberis Recens dregs and produce Rhizoma Zingiberis Recens juice: the Rhizoma Zingiberis Recens raw material of fragmentation is packed in the typing oil press, its drainage screen is 120 orders, at normal temperatures, pressure is that 8kg carries out filter pressing, elimination Cortex Zingiberis, Rhizoma Zingiberis Recens fiber and not broken thin Rhizoma Zingiberis Recens piece, make Rhizoma Zingiberis Recens juice 750kg, the Cortex Zingiberis that leaches, Rhizoma Zingiberis Recens fiber can be made feed additive;
(3), the starch in the Rhizoma Zingiberis Recens juice is separated, make Rhizoma Zingiberis Recens starch and destarch Sucus Zingberis: the Rhizoma Zingiberis Recens juice 750kg that makes is put into the sealed plastic jar, natural subsidence 2 hours, get destarch Sucus Zingberis 740kg, isolated starch 10kg can use as food, the rare batching of dish separately as the packing of product; The destarch Sucus Zingberis is as next step raw materials for production;
(4), the destarch Sucus Zingberis is added the sealing of extraction oil preparation mix the extraction of heating: destarch Sucus Zingberis 740kg is added in the extraction equipment, add the extraction oil preparation again, adopt oil of ginger as the extraction oil preparation, add 2.5kg, after adding the extraction oil preparation, under sealing state, mixed 30 minutes, heat again to 50 ℃, extracted 2 hours, pass through pick test, extraction yield reaches more than 95%, be layering after static half an hour, in extraction equipment, be divided into oil of ginger and gingerol mixing liquid layer from top to bottom successively, aminoacid and vitamin mixture layer, microelement kind mixing liquid layer, wherein oil of ginger and the gingerol mixing liquid layer the superiors are based on oil of ginger, and orlop is based on gingerol;
(5), with stratified oil of ginger and gingerol mixing liquid layer, aminoacid and vitamin mixture layer, microelement kind mixing liquid layer extraction separation, be respectively charged into jar special: deposit in the extraction of microelement kind mixed liquor in the jar special separately earlier, again aminoacid and independent extraction of vitamin mixture are deposited in the corresponding jar special, at last oil of ginger and the extraction of gingerol mixed liquor are deposited in separately in the jar special of sealing;
(6), separate oil of ginger and gingerol: to being sealed in oil of ginger and the gingerol mixed liquor in the jar special, extracting oil of ginger by squeezing is finished product, is contained in the bottle separately; Isolated gingerol, reuse pure water washing, remaining oil of ginger and aminoacid in the flush away gingerol, the waste liquid of washing usefulness enters in the extraction process, recycles;
(7), produce the gingerol powder: isolated gingerol is packed in the drying baker, and through 40 ℃ of dryings, dried gingerol is 2.9kg, is product in the bottle of packing into;
(8), aminoacid and the vitamin mixture to proposition packs after sterilizing: proposing the mixed liquid of aminoacid and vitamin is 680kg, is respectively charged in the sealed plastic bag of 680 vacuum, directly as eating or do food additive;
(9), the microelement kind mixed liquor 30kg to proposing, drying sterilization back powdering is packed in 30 plastic bags, its application process is with aminoacid and vitamin mixture.
Embodiment 3
Adopt the Laiwu Rhizoma Zingiberis Recens, buy the sick Rhizoma Zingiberis Recens of 1000kg, mashed Rhizoma Zingiberis Recens, deteriorated ginger.
Production stage is with embodiment 1
Making oil of ginger is 2.3kg, and gingerol is 2.8kg, measures through Hplc, and quality index is identical.
Make aminoacid and vitamin 590kg, dark-brown, the trace element 30kg that makes is canescence, and is aseptic after testing through high temperature sterilization sterilization running into tank, can be used as the raw material of ginger special-purpose fertilizer or directly use.
Claims (8)
1, a kind of oil-solvent extraction of Rhizoma Zingiberis Recens extract at first cleans as the Rhizoma Zingiberis Recens raw material the Jiang Jinhang roguing, it is characterized in that it is by following steps production:
(1) fragmentation;
(2) cross the elimination Rhizoma Zingiberis Recens dregs and produce Rhizoma Zingiberis Recens juice;
(3) starch in the Rhizoma Zingiberis Recens juice is separated, make Rhizoma Zingiberis Recens starch and destarch Sucus Zingberis;
(4) the destarch Sucus Zingberis is added the sealing of extraction oil preparation and mix the extraction of heating: the extraction oil preparation is a vegetable oil, and its extraction time is so that extract is divided into oil of ginger clearly is as the criterion with vitamin mixture layer, microelement kind mixing liquid layer with gingerol mixing liquid layer, aminoacid;
(5) with stratified oil of ginger and gingerol mixing liquid layer, aminoacid and vitamin mixture layer, microelement kind mixing liquid layer extraction separation, be respectively charged into jar special;
(6) separate oil of ginger and gingerol: oil of ginger and gingerol mixed liquor are packed into separately behind the jar special of sealing, extract oil of ginger by squeezing again, and isolate gingerol, remaining oil of ginger and aminoacid in the isolated gingerol reuse pure water washing removal gingerol;
(7) produce the gingerol powder: to isolated gingerol through the low-temperature vacuum drying powdering.
2, the oil-solvent extraction of a kind of Rhizoma Zingiberis Recens extract according to claim 1, it is characterized in that described vegetable oil is one of following or its combination of two kinds: oil of ginger, Oleum Arachidis hypogaeae semen, Oleum sesami, Oleum Glycines, Oleum Brassicae campestris, Petiolus Trachycarpi oil, Oleum Gossypii semen, Semen Maydis oil, sunflower oil, the adding proportion of vegetable oil are that 1000kg Rhizoma Zingiberis Recens raw material adds 2 to 3kg; Described vegetable oil is preferably oil of ginger.
3, the oil-solvent extraction of a kind of Rhizoma Zingiberis Recens extract according to claim 1 is characterized in that in broken step, describedly is broken for the low speed fragmentation, can adopt the stainless steel ball grinding machine, and rotating speed is 30-80 rev/min, and broken fineness is 100 orders.
4, the oil-solvent extraction of a kind of Rhizoma Zingiberis Recens extract according to claim 1 is characterized in that producing in the step of Rhizoma Zingiberis Recens juice at mistake elimination Rhizoma Zingiberis Recens dregs, and described filtration can be adopted the typing oil press, and at normal temperatures, pressure is 5-8kg, carries out filter pressing and produces.
5, the oil-solvent extraction of a kind of Rhizoma Zingiberis Recens extract according to claim 1, it is characterized in that the starch in the Rhizoma Zingiberis Recens juice being separated in the step that makes Rhizoma Zingiberis Recens starch and destarch Sucus Zingberis, be to use the elimination Rhizoma Zingiberis Recens dregs to produce the Rhizoma Zingiberis Recens juice of producing in the Rhizoma Zingiberis Recens juice step, through 1-3 hour natural subsidence, isolate Rhizoma Zingiberis Recens starch, produce the destarch Sucus Zingberis simultaneously.
6, the oil-solvent extraction of a kind of Rhizoma Zingiberis Recens extract according to claim 1, it is characterized in that in the step of extraction that destarch Sucus Zingberis adding extraction oil preparation sealing mixing is heated, after the destarch Sucus Zingberis adds extraction equipment, need add vegetable oil extraction oil preparation in proportion, sealing mixed 30-40 minute, heat again to 30-100 ℃, extracted 0.5-4 hour, and made extract in the extraction equipment can find out that clearly oil of ginger can stop during with vitamin mixture layer, microelement kind mixing liquid layer with gingerol mixing liquid layer, aminoacid.
7, the oil-solvent extraction of a kind of Rhizoma Zingiberis Recens extract according to claim 1, it is characterized in that in the step of separating oil of ginger and gingerol, to remove remaining oil of ginger and the storage of amino acid whose cleaning mixture in the gingerol with pure water washing, return and the destarch Sucus Zingberis is added the sealing of extraction oil preparation mix in the extraction step of heating.
8, the oil-solvent extraction of a kind of Rhizoma Zingiberis Recens extract according to claim 1 is characterized in that in producing gingerol powder step gingerol under 40-50 ℃ temperature, being become the yellow-gray powdered extract through vacuum drying.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100440666A CN100569275C (en) | 2006-05-11 | 2006-05-11 | A kind of oil-solvent extraction of Rhizoma Zingiberis Recens extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100440666A CN100569275C (en) | 2006-05-11 | 2006-05-11 | A kind of oil-solvent extraction of Rhizoma Zingiberis Recens extract |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1981864A true CN1981864A (en) | 2007-06-20 |
| CN100569275C CN100569275C (en) | 2009-12-16 |
Family
ID=38164894
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006100440666A Expired - Fee Related CN100569275C (en) | 2006-05-11 | 2006-05-11 | A kind of oil-solvent extraction of Rhizoma Zingiberis Recens extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100569275C (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104970329A (en) * | 2015-06-30 | 2015-10-14 | 南阳汇萃植物制品有限公司 | Allocable flavored oil and preparation method thereof |
| CN107281063A (en) * | 2017-06-28 | 2017-10-24 | 广州科玛生物科技股份有限公司 | A kind of true Jiang Jinghua hair conditioner and preparation method thereof |
| CN107460032A (en) * | 2017-09-18 | 2017-12-12 | 广西大学 | A kind of method for extracting effective components of ginger |
| CN108175717A (en) * | 2016-12-08 | 2018-06-19 | 广州栋方生物科技股份有限公司 | The industrialized utilization of ginger and the antiallergic composition of structure |
| CN108359019A (en) * | 2018-01-18 | 2018-08-03 | 大连豪翔生物酶工程有限公司 | A kind of method of the integrated extraction of multiple biological activities ingredient in turmeric |
| CN112806549A (en) * | 2020-12-30 | 2021-05-18 | 西安银能生物科技股份有限公司 | Ginger full-recycling treatment method |
-
2006
- 2006-05-11 CN CNB2006100440666A patent/CN100569275C/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104970329A (en) * | 2015-06-30 | 2015-10-14 | 南阳汇萃植物制品有限公司 | Allocable flavored oil and preparation method thereof |
| CN108175717A (en) * | 2016-12-08 | 2018-06-19 | 广州栋方生物科技股份有限公司 | The industrialized utilization of ginger and the antiallergic composition of structure |
| CN107281063A (en) * | 2017-06-28 | 2017-10-24 | 广州科玛生物科技股份有限公司 | A kind of true Jiang Jinghua hair conditioner and preparation method thereof |
| CN107460032A (en) * | 2017-09-18 | 2017-12-12 | 广西大学 | A kind of method for extracting effective components of ginger |
| CN108359019A (en) * | 2018-01-18 | 2018-08-03 | 大连豪翔生物酶工程有限公司 | A kind of method of the integrated extraction of multiple biological activities ingredient in turmeric |
| CN112806549A (en) * | 2020-12-30 | 2021-05-18 | 西安银能生物科技股份有限公司 | Ginger full-recycling treatment method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100569275C (en) | 2009-12-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103355666B (en) | Preparation method of plant enzyme beverage capable of improving cardiovascular and cerebrovascular metabolic functions | |
| CN100569275C (en) | A kind of oil-solvent extraction of Rhizoma Zingiberis Recens extract | |
| CN102311900B (en) | Health care yellow wine rich in nutrients | |
| CN101191115A (en) | Honeysuckle fruit vinegar beverage | |
| CN106262824A (en) | A kind of production method of Chinese herbal medicine ferment stock solution | |
| CN1891239A (en) | Method for preparing Chinese herb medicine utilizing enzyme preparation | |
| CN106085750A (en) | A kind of processing method of Rhizoma Bistortae Radix ziziphi mauritianae health promoting wine | |
| CN102344872B (en) | Method for preparing sweet potato yellow wine containing anthocyanidin | |
| CN107307254A (en) | One kind moistens the lung and relieve the cough tendril-leaved fritillary bulb Chinese herbal health-caring beverage and preparation method thereof | |
| CN101223995B (en) | Preparing method for garlic and onion compound essential oil | |
| CN103215163B (en) | Circium japonicum mushroom rice wine and preparation method thereof | |
| CN102994309A (en) | Ginkgo-sorghum liquor and ginkgo-sorghum health-care liquor | |
| CN103549584B (en) | Production method for vinegar beverage for nourishing qi and blood | |
| CN102845803B (en) | Preparation method of instant chrysanthemum powder | |
| CN109082357A (en) | The brewage process of health care soft-taste white spirit | |
| CN1243742A (en) | Natural peony juice and its extraction process | |
| CN110317708A (en) | A kind of olive vinegar and preparation method thereof | |
| CN1036470C (en) | Products made by mixed fermentation of mushroom and chinese herbal medicine and its method | |
| CN102477105A (en) | Method for combined preparation of polysaccharide and flavone by using pumpkin stems and leaves as raw material | |
| CN102626193B (en) | Vinegar beverage with efficacy of invigorating qi and blood and production method thereof | |
| CN102311901B (en) | Health-care low-alcohol-volume nutritional yellow wine with fruit fragrance | |
| CN103205342B (en) | Rice wine with geckos and Taibai-tea and preparation method thereof | |
| CN101607145B (en) | Method for extracting interfacial active sapindoside and organic matter from soapberry fruit and finished product | |
| CN108220256A (en) | A kind of preparation method of enzyme | |
| CN105131059B (en) | A method of extracting geniposide from cape jasmine |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20091216 Termination date: 20170511 |