CN1977609A - Farm chemical paste for controlling woody plant pests - Google Patents

Farm chemical paste for controlling woody plant pests Download PDF

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Publication number
CN1977609A
CN1977609A CN 200510102208 CN200510102208A CN1977609A CN 1977609 A CN1977609 A CN 1977609A CN 200510102208 CN200510102208 CN 200510102208 CN 200510102208 A CN200510102208 A CN 200510102208A CN 1977609 A CN1977609 A CN 1977609A
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China
Prior art keywords
ointment
acetamiprid
weight
woody plant
carbosulfan
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CN 200510102208
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Chinese (zh)
Inventor
徐汉虹
叶宝鑑
陈小军
张志祥
田永清
江定心
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LUBAO BIOCHEMICAL TECHNOLOGY INST NANHAI DISTRICT FOSHAN CITY
South China Agricultural University
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LUBAO BIOCHEMICAL TECHNOLOGY INST NANHAI DISTRICT FOSHAN CITY
South China Agricultural University
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Priority to CN 200510102208 priority Critical patent/CN1977609A/en
Publication of CN1977609A publication Critical patent/CN1977609A/en
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Abstract

本发明公开了一种控制木本植物害虫的药膏。由啶虫脒重量百分比为1－10％，乙酰甲胺磷或丁硫克百威按重量百分比为1－50％，其余是助剂混配而成，按已有制备方法制成药膏。用本发明药膏涂抹在剥开树皮处，具有良好的粘着力、持效性，施药简便，提高了药剂的利用率，降低了环境污染，药剂可通过植物表皮内吸进植株，并且本发明药膏具有一定的触杀作用，可以阻止害虫在树干上下来回的爬行，从而也可大大减轻对植株的危害。The invention discloses an ointment for controlling woody plant pests. The acetamiprid is 1-10% by weight, acephate or carbosulfan is 1-50% by weight, and the rest are auxiliary agents, and the ointment is prepared according to the existing preparation method. The ointment of the present invention is applied to the place where the bark is peeled off, which has good adhesion and long-lasting effect, is easy to apply, improves the utilization rate of the medicament, and reduces environmental pollution. The medicament can be sucked into the plant through the plant epidermis, and the The invented ointment has a certain contact killing effect, which can prevent pests from crawling up and down the trunk, thereby greatly reducing the damage to plants.

Description

A kind of ointment of controlling the woody plant insect
Technical field
The present invention relates to pesticide field, belong to a kind of ointment of controlling the woody plant insect.
Background technology:
Poplar longicorn is the important trunk borer of seeds such as China poplar, willow, elm, maple, and the poplar longicorn of having reported in China reaches kind more than 100.Because the poplar longicorn life is hidden, the natural enemy kind is few, the history of life is complicated, and willow is China's afforestation, checks winds and fixes drifting sand and one of the first-selected seeds of afforestation such as fast growing, cause poplar longicorn food resource abundance, in China's poplar longicorn harm seriously, year generation area is at 600,000 hm 2About.Over 10 years, yellow spotted star longicorn beetle, anoplophora glabripennis rapid spread, harm is serious, makes the development of willow be subjected to very big restriction, has had a strong impact on the forestry sound development.Because the life of poplar longicorn larva is hidden, brought very big difficulty to preventing and controlling, so the control of poplar longicorn is an instant task.
What the control of poplar longicorn was adopted at present is the strategy of integrated control.Concrete condition is as follows:
1. forest culture and management measure: select to have the improved seeds afforestation such as middle forest 46, middle forest No. 108 of pest-resistant performance, strict nursery stock quarantine avoids being with worm nursery stock afforestation.Newly make poplar forest away from the worm seedbed, or the isolation strip of planting, build mixed forest; Mix with the seeds of longicorn apocleisis and willow collocation and to hand over afforestation, generally be mixed with suitablely with bulk, shelter belt can be adopted section gap to mix and be handed over.Adopt measures such as big cave, seedlings, big flood, duty are applied fertilizer, duty is loosened the soil, promote healthy quick growth of forest, the enhancing insect resistance capacity.
2. biological control measure: adopt controls such as longicorn natural enemy insect, longicorn causal organism, can control the longicorn insect population with woodpecker in the conditional region; New planting site can be had a liking for the moraceae plants etc. of food, trapping longicorn adult with longicorn.It mainly is to adopt the directly stifled longicorn defecation hole that is coated with of white muscardine fungi, green muscardine fungus, bacillus thuringiensis,Bt biologic products such as (Bt) that bio-control method at the longicorn individuality is also arranged.
3. physical measure: mulberry longicorn nocturnalism has stronger phototaxis, available black light lamp trapping.Anoplophora glabripennis is all movable round the clock, and phototaxis is not strong, can manually catch adult.Be coated with from avoiding with trunk and keep away the longicorn adult and lay eggs, can repair the deinsectization branch winter in conjunction with tending [after young plantation, cuts the generation trees that seriously are injured, and eradicates hidden danger.
4. chemical measure: 1. organophosphorus insecticide such as available zinc phosphide is made poison and is signed, and inserts worm channel, the smoked kill larva, and effect can reach 90%.2. with 50-300 times of organophosphorous pesticide dilution injection worm channel, kill larva.3. inject at butt or root punching with systemics agricultural chemicals such as nuvacron, flolimats, seal with wet soil the perfusion back, can prevent and treat tall and big trees larva.4. in adult stage and ovum phase, large tracts of land is sprayed the young urea 1000-2000 times glue suspension that goes out, and can kill adult and ovum.5. use novel contact insecticide " green prestige thunder " control longicorn adult.
More than a difficult problem that each method faced be biological control effect instability, control efficiency is subjected to the influence of factors such as weather, and poplar longicorn is as a kind of borer pest, the biological control medicament is difficult to arrive adult and the larva of longicorn; What still use in large tracts of land at present is chemical prevention and control method, as adopts that poison is signed, the boring injection, buries methods such as medicine, spraying, but these methods run into very hang-up on control efficiency or concrete implementation and operation.Poison label method need find the hole of roundheaded borer and adult, and during large area control, workload is too big; Workload was too big when boring was injected at large area control, and injured the xylem of willow behind the brill sky, and the self-healing ability of willow is limited, and rotten random situation appears in very most of meeting, and the peasant has certain difficulty on reception the method; Dosage is big during spraying, and droplet can need be employed the high pressure spraying mechanical with wind drift, and medicament also is difficult to effectively arrive polypide, and the medicament availability is too low.
Summary of the invention
The object of the invention provides that a kind of lasting period is long, and environmental pollution is little, the ointment of the control woody plant insect that dispenser is easy.
The present invention realizes that the technical scheme of above-mentioned purpose is: by active ingredient Acetamiprid percentage by weight is 1.0-10%%, and carbosulfan or orthene percentage by weight are 1.0-50%, and all the other are that additive mixture forms.
Selected Acetamiprid, orthene and the carbosulfan of the present invention has good systemic action, synergistic effect was obvious after Acetamiprid and orthene or carbosulfan were mixed, the paste of being made is coated in the band girdle place of trunk, medicament has good translocation and reaches the position that insect is caused harm at phloem, the borer pest position of causing harm particularly, simultaneously trunk band girdle place coat have in the medicament of suction and tagging property, can stop insect from the creeping back and forth of trunk bottom and trunk top, significantly reduce the chance that causes harm.
Above-mentioned auxiliary agent is: solvent, sticker and filler, the auxiliary agent weight percentage is as follows in the paste: solvent 2.0-70.0%, sticker 1.0-20.0%, filler 10.0-80.0%.
Preparation paste solvent for use is selected from following one or more: benzene,toluene,xylene, methyl alcohol, ethanol, propyl alcohol, butanols, isobutanol, cyclohexanone, MEK, isophorone, pyrrolidones, N-Methyl pyrrolidone, dimethyl formamide, methyl-sulfoxide, 2-Pyrrolidone, cyclohexanone.
Preparation paste used sticker is selected from following one or more: poly-ethyl acetate, gelatin, polyvinyl alcohol, styrene-butadiene latex, gum Arabic, sodium alginate, xanthans, sodium carboxymethylcellulose, carboxy-propyl cellulose sodium, polyethylene glycol, polyethylene glycol oxide, polyvinylpyrrolidone, polyacrylamide, soluble starch, dextrin, polyvinyl acetate, coumarone resin, Petropols, naphthols-formaldehyde resin.
Preparation paste used filler is to be selected from following one or more: diatomite, Concave-convex clay rod, bentonite, sepiolite, kaolin, potter's clay, precipitated calcium carbonate, sawdust powder, rice husk, tobacco powder, walnut parting, lignin, white carbon.
Ointment of the present invention is made with conventional method, will have after absorption Acetamiprid and orthene or carbosulfan be mixed according to aforementioned proportion in good, adds solvent, sticker, filler in proportion, and canned moulding.Before use, utilize homemade band girdle cutter at willow trunk 0.3-1.8 rice from top to bottom around the about 2-20 of trunk spiral strip off one width centimetre groove, the phloem of only cutting open during cutting, and do not injure xylem, spill xylem (width of strip off bark and play up and down 2 vertical ranges change) because of the vary in diameter of tree, be coated with at strip off bark place and spread the ointment of being made, allow medicament be transmitted to the position that insect is caused harm by the phloem of tree, it is long that this medicament has the lasting period, environmental pollution is little, this is easy and simple to handle simultaneously, only need gently strip off bark once, made ointment is coated in strip off place by the extruding tanning device gets final product, strip off bark and coating can carry out continuously.Simultaneously the ointment that uses of strip off place has very strong action of contace poison, forms the obstruct of certain width up and down between back and forth at trunk, when insect creeps on trunk, can be killed behind the contact ointment, has significantly reduced insect the causing harm to plant of creeping.
Embodiment
The following examples are that technical solution of the present invention is further specified, but content of the present invention is not limited thereto.
Embodiment 1,10.0% Acetamiprid carbosulfan ointment
(all form following examples all by weight percentage)
Acetamiprid 5.0, carbosulfan 5.0, toluene 8.0, methyl alcohol 6.0, poly-ethyl acetate 2.0, gelatin 2.0, diatomite 72.0 will add pesticide active ingredient after binding agent, filler, the solvent under stirring at normal temperature, become paste liquid and tinning.
Embodiment 2:10.0% Acetamiprid orthene paste
Acetamiprid 5.0, orthene 5.0, benzene 7.5, dimethyl formamide 4.5, styrene-butadiene latex 1.0, gum Arabic 4.0, precipitated calcium carbonate 73.0 will add pesticide active ingredient after binding agent, filler, the solvent under stirring at normal temperature, become paste liquid and tinning.
Embodiment 3,20.0% Acetamiprid carbosulfan ointment
Acetamiprid 10.0, carbosulfan 10.0, cyclohexanone 6.5, dimethyl formamide 13.5,2-Pyrrolidone 7.5, precipitated calcium carbonate 30.0, sawdust powder 22.5 will add pesticide active ingredient after binding agent, filler, the solvent under stirring at normal temperature, become paste liquid and tinning.
Embodiment 4:20.0% Acetamiprid orthene ointment
Acetamiprid 10.0, orthene 10.0, dimethyl formamide 16.0, polyvinylpyrrolidone 4.0, polyacrylamide 4.0, attapulgite clay 39.0, bentonite 17.0 will add pesticide active ingredient after binding agent, filler, the solvent under stirring at normal temperature, become paste liquid and tinning.
Embodiment 5,6.0% Acetamiprid carbosulfan ointment
Acetamiprid 1.0, carbosulfan 5.0,2-be than pyrrolidone 2.0, MEK 6.0, dextrin 0.5, polyvinyl acetate 3.0, coumarone resin 3.0, kaolin 79.5 will add pesticide active ingredient after binding agent, filler, the solvent under stirring at normal temperature, become paste liquid and tinning.
Embodiment 6:6.0% Acetamiprid orthene ointment
Acetamiprid 1.0, orthene 5.0, methyl-sulfoxide 1.0, cyclohexanone 6.0, polyethylene glycol 5.0, sepiolite 30.0, kaolin 52.0 will add pesticide active ingredient after binding agent, filler, the solvent under stirring at normal temperature, become paste liquid and tinning.
Embodiment 7,52.0% Acetamiprid carbosulfan ointment
Acetamiprid 2.0, carbosulfan 50.0, toluene 10.0,2-Pyrrolidone 15.0, sodium alginate 8.0, xanthans 2.0, precipitated calcium carbonate 13.0 will add pesticide active ingredient after binding agent, filler, the solvent under stirring at normal temperature, become paste liquid and tinning.
Embodiment 8:52.0% Acetamiprid orthene ointment
Acetamiprid 2.0, orthene 50.0, toluene 10.0, N-Methyl pyrrolidone 10.0, carboxy-propyl cellulose sodium 12.0, lignin 16.0 will add pesticide active ingredient after binding agent, filler, the solvent under stirring at normal temperature, become paste liquid and tinning.
Embodiment 9,60.0% Acetamiprid carbosulfan paste
Acetamiprid 10.0, carbosulfan 50.0, different fluorine that ketone 10.0, MEK 9.0, sodium carboxymethylcellulose 13.0, rice husk 5.0, tobacco powder 3.0 will add pesticide active ingredient after binding agent, filler, the solvent under stirring at normal temperature, become paste liquid and tinning.
Embodiment 10:60.0% Acetamiprid orthene ointment
Acetamiprid 10.0, orthene 10.0, different fluorine that ketone 6.0, MEK 9.0, dimethyl formamide 5.0, polyvinyl alcohol 6.0; styrene-butadiene latex 6.0, walnut parting 4.0, lignin 4.0; will add pesticide active ingredient after binding agent, filler, the solvent under stirring at normal temperature become paste liquid and tinning.
Embodiment 11 indoor mixture synergism toxicity tests
Each reagent agent is made into five concentration of 500,250,125,62.5 and 31.25 μ g/mg respectively, from the low concentration to the high concentration, draw the agricultural chemicals for preparing with microsyringe, drip in the pronotary of anoplophora glabripennis 3 instar larvaes, rinse with acetone between the different medicaments and wash microsyringe, every drips 2 μ L, 30 of every concentration, do contrast with 4% acetone solution, 24h observes the larva death toll, and anoplophora glabripennis larva discrimination method anyway sees Table 1, calculates LC 50Value and virulence regression equation and co-toxicity coefficient.Co-toxicity coefficient adopts the abundant method of Sun Yun to calculate.
The toxicity index that co-toxicity coefficient CTC=100 * actual toxicity index/theory of using with is used with
When co-toxicity coefficient obviously greater than 100 the time, showing has synergistic effect; Near 100, expression has summation action; Be significantly less than 100, showing has antagonism.Result of calculation sees Table 2:
Table 1 anoplophora glabripennis is differentiated by larva anyway
The dead worm of classification worm alive The glossy tarnish of body surface color and luster Polypide elasticity is flexible nonelastic The reflection of Ci Jiing is moved to external world The polypide side view is circular oblate
Table 2: indoor mixture is to the anoplophora glabripennis toxicity test
Reagent agent Virulence regression equation LC 50Value (μ g/mg) Correlation coefficient Co-toxicity coefficient
Orthene Y＝1.476X+1.716 170.62 0.9866
Carbosulfan Y＝1.241X+2.038 243.58 0.9832
Acetamiprid Y＝1.210X+2.366 150.43 0.9906
Acetamiprid: carbosulfan=1: 1 Y＝1.696X+1.514 113.75 0.9939 163.51
Acetamiprid: orthene :=1: 1 Y＝1.141X+2.712 101.26 0.9879 157.90
Acetamiprid: carbosulfan=1: 5 Y＝0.680X+3.563 129.83 0.9903 170.06
Acetamiprid: orthene=1: 5 Y＝1.142X+2.603 125.84 0.9892 132.62
Acetamiprid: carbosulfan=1: 25 Y＝0.851X+3.089 176.18 0.9914 135.04
Acetamiprid: orthene=1: 25 Y＝1.251X+2.308 142.06 0.9966 119.49
Embodiment 12: the field control effectiveness test measurement result
Test site: Feidong County, Anhui Province willow growing area, the growth of poplar condition is consistent with management condition, and this growing area anoplophora glabripennis takes place serious.
Test period: 18-May 18 April, spraying time April 18, April 28 control time and May 18 days.
Weather condition: duration of test is fine entirely, temperature 19-23 ℃, and humidity 55-80%, no rainfall and other anomalous weather.
5 meters in test region willow, 25 centimetres of diameters, growth and management condition unanimity, from 1.5 meters of the vertically about distance of willow tree root with cutter trunk from top to bottom helical ring cut off the willow bark, spiral strip off bark (not remaining silent) from top to bottom, form spiral groove, the Origin And Destination vertical range of strip off is 54 centimetres, 4 centimetres of recess width.
Prepared ointment embodiment 1,2,3,4,5,6,7,8,9,10,11,12 and Acetamiprid, orthene and carbosulfan list agent paste are evenly coated in the groove position of being severed, the death condition of anoplophora glabripennis is calculated lethality and control efficiency in 10 days and 30 days investigation trunk.The results are shown in Table 3:
Table 3 mixture preparation is beaten injection control glabripenis field efficacy
Behind the medicine 10 days Behind the medicine 30 days
Handle Insect population radix (head) before handling Handle back borer population (head) alive Preventive effect (%) Insect population radix (head) before handling Handle back borer population (head) alive Preventive effect (%)
Contrast 152 163 -7.23±0.92 168 241 -43.40±2.15
Orthene 136 49 66.40±1.11 183 39 85.14±2.35
Carbosulfan 156 60 64.13±0.98 159 59 74.13±1.89
Acetamiprid 176 62 67.15±1.41 133 21 88.99±2.02
Embodiment 1 189 11 94.57±0.68 149 4 98.13±1.89
Embodiment 2 178 9 95.29±1.58 126 2 98.89±1.02
Embodiment 3 134 7 95.13±1.43 155 3 98.65±1.01
Embodiment 4 157 5 97.03±1.49 168 3 98.76±1.68
Embodiment 5 146 17 89.14±0.56 159 6 97.37±0.47
Embodiment 6 132 15 89.40±0.78 147 5 97.63±1.08
Embodiment 7 187 7 96.51±0.49 138 2 98.99±0.41
Embodiment 8 202 6 97.23±0.56 158 2 99.12±0.00
Embodiment 9 175 4 96.87±1.25 146 1 99.52±0.00
Embodiment 10 153 3 98.17±0.21 178 0 100.00±0.00

Claims (3)

1. ointment of controlling the woody plant insect, it is characterized in that: by the Acetamiprid percentage by weight is 1.0-10%, and carbosulfan or orthene are 1.0-50% by weight percentage, and all the other are that additive mixture forms.
2. a kind of ointment of controlling the woody plant insect according to claim 1, it is characterized in that: described auxiliary agent is: solvent weight percent is 2.0-70.0%, and the sticker percentage by weight is 1.0-20.0%, and filler weight percentage is 10.0-80.0%.
3. a kind of ointment of controlling the woody plant insect according to claim 2 is characterized in that:
Described solvent is to be selected from following one or more: your ketone of benzene,toluene,xylene, methyl alcohol, ethanol, propyl alcohol, butanols, isobutanol, cyclohexanone, MEK, different fluorine, pyrrolidones, N-Methyl pyrrolidone, dimethyl formamide, methyl-sulfoxide, 2-Pyrrolidone, cyclohexanone;
Described sticker is to be selected from following one or more: poly-ethyl acetate, gelatin, polyvinyl alcohol, styrene-butadiene latex, gum Arabic, sodium alginate, xanthans, sodium carboxymethylcellulose, carboxy-propyl cellulose sodium, polyethylene glycol, polyethylene glycol oxide, polyvinylpyrrolidone, polyacrylamide, soluble starch, dextrin, polyvinyl acetate, coumarone resin, Petropols, naphthols-formaldehyde resin;
Described filler is to be selected from following one or more: diatomite, Concave-convex clay rod, bentonite, sepiolite, kaolin, potter's clay, precipitated calcium carbonate, sawdust powder, rice husk, tobacco powder, walnut parting, lignin.
CN 200510102208 2005-12-05 2005-12-05 Farm chemical paste for controlling woody plant pests Pending CN1977609A (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101444224B (en) * 2009-01-09 2011-08-24 河南科技学院 a compound insecticide
CN102422799A (en) * 2011-09-15 2012-04-25 张冠一 Method for preventing and treating red maple dry-borer
CN103039431A (en) * 2012-12-06 2013-04-17 镇江万山红遍农业园 Method for killing anoplophora nobilis larvae in fruit tree branches and repairing worm-holes
CN103155943A (en) * 2013-03-25 2013-06-19 扬州大学 Plaster for preventing forestry pests poplar longicorn
CN103168796A (en) * 2013-03-25 2013-06-26 扬州大学 Ointment for preventing and treating insect pest longicorn of poplar
CN105010315A (en) * 2015-08-18 2015-11-04 天津市汉邦植物保护剂有限责任公司 Dispersable oil suspending agent containing acetamiprid and carbosulfan and application
CN110692649A (en) * 2019-10-29 2020-01-17 中国热带农业科学院椰子研究所 A kind of ointment for preventing and controlling tree trunk diseases and insect pests
WO2020075167A1 (en) * 2018-10-07 2020-04-16 Adama Makhteshim Ltd. Ternary insecticidal mixture
CN111990406A (en) * 2020-08-31 2020-11-27 青岛泰源科技发展有限公司 Acetamiprid termite-controlling composition and preparation method thereof
CN114097814A (en) * 2020-08-31 2022-03-01 青岛泰源科技发展有限公司 Acetamiprid composition for preventing and treating termites

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101444224B (en) * 2009-01-09 2011-08-24 河南科技学院 a compound insecticide
CN102422799A (en) * 2011-09-15 2012-04-25 张冠一 Method for preventing and treating red maple dry-borer
CN103039431A (en) * 2012-12-06 2013-04-17 镇江万山红遍农业园 Method for killing anoplophora nobilis larvae in fruit tree branches and repairing worm-holes
CN103155943A (en) * 2013-03-25 2013-06-19 扬州大学 Plaster for preventing forestry pests poplar longicorn
CN103168796A (en) * 2013-03-25 2013-06-26 扬州大学 Ointment for preventing and treating insect pest longicorn of poplar
CN103155943B (en) * 2013-03-25 2014-11-05 扬州大学 Plaster for preventing forestry pests poplar longicorn
CN105010315A (en) * 2015-08-18 2015-11-04 天津市汉邦植物保护剂有限责任公司 Dispersable oil suspending agent containing acetamiprid and carbosulfan and application
CN105010315B (en) * 2015-08-18 2017-10-31 天津市汉邦植物保护剂有限责任公司 It is a kind of containing Acetamiprid and the dispersible oil-suspending agent of carbosulfan and application
WO2020075167A1 (en) * 2018-10-07 2020-04-16 Adama Makhteshim Ltd. Ternary insecticidal mixture
CN112955013A (en) * 2018-10-07 2021-06-11 阿达玛马克西姆有限公司 Ternary insecticide mixtures
CN112955013B (en) * 2018-10-07 2023-04-28 阿达玛马克西姆有限公司 Ternary insecticidal mixtures
CN110692649A (en) * 2019-10-29 2020-01-17 中国热带农业科学院椰子研究所 A kind of ointment for preventing and controlling tree trunk diseases and insect pests
CN111990406A (en) * 2020-08-31 2020-11-27 青岛泰源科技发展有限公司 Acetamiprid termite-controlling composition and preparation method thereof
CN114097814A (en) * 2020-08-31 2022-03-01 青岛泰源科技发展有限公司 Acetamiprid composition for preventing and treating termites

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