CN1904096A - Copper wire tower having supporting device used for removing vanadium impurity in titanium tetrachloride - Google Patents
Copper wire tower having supporting device used for removing vanadium impurity in titanium tetrachloride Download PDFInfo
- Publication number
- CN1904096A CN1904096A CN 200610051163 CN200610051163A CN1904096A CN 1904096 A CN1904096 A CN 1904096A CN 200610051163 CN200610051163 CN 200610051163 CN 200610051163 A CN200610051163 A CN 200610051163A CN 1904096 A CN1904096 A CN 1904096A
- Authority
- CN
- China
- Prior art keywords
- tower
- copper wire
- supporting device
- flange
- sealing cover
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Landscapes
- Manufacture And Refinement Of Metals (AREA)
Abstract
The present invention provides a copper wire tower with supporting device. It is composed of tower top, tower body, supporting device and tower bottom, and can be used for removing vanadium impurity from titanium tetrachloride. Said invention also provides the concrete structure of above-mentioned every portion, and working principle of said copper wire tower and its operation method.
Description
Technical Field
The invention belongs to the technical field of non-ferrous metal smelting, and particularly relates to a copper wire tower with a supporting device for removing vanadium impurities in titanium tetrachloride.
Background
The commonly used copper wire tower is composed of a steam pipe, a copper wire ball feeding pipe, a steam interface and a reflux interface part, wherein the steam pipe, the copper wire ball feeding pipe and the steam interface and the reflux interface part are arranged on the tower top, the tower body, the tower bottom and the tower top. The tower top and the tower body, and the tower body and the tower bottom are respectively connected into a whole through a concave flange, a convex flange and a sealing pad which is sleeved on the concave flange and the convex flange by bolts.
When the device works, the copper wire balls are thrown into the tower through the copper wire ball feeding pipe, and the copper wire balls are easily ineffective after being covered by impurities brought by titanium tetrachloride steam and products of chemical reaction, so that the copper wire balls can be continuously used after being leached by water, and then are washed by acid, rinsed by clean water and dried. It is common practice to remove the vapor connection at the bottom of the column and the connection to the reflux connection, remove the bottom of the column, and feed water into the column from the top of the column. The copper wire ball can drop rapidly after being soaked in water, when the friction force generated between substances in the tower and the inner wall of the tower is insufficient to support the copper wire ball, the copper wire ball falls on a sieve plate which is difficult to support at the bottom of the tower, so that the sieve plate deforms, the pressure of the copper wire ball with the weight of several tons acts on a lift truck under the bottom of the tower or is dead by the lift truck or the lift truck is suddenly impacted to separate from a track, and the safety is extremely poor. Meanwhile, due to splashing of falling copper wire balls, a cleaning pool arranged below the tower bottom is easy to be damaged, and maintenance cost is high. When the copper wire ball falls into the cleaning pool for leaching outside the tower, the titanium tetrachloride covered on the copper wire ball can be immediately hydrolyzed and release heat after meeting air and water, and the molecular formula of the chemical reaction is as follows: thus, a large amount of acid mist is formed, and the environment is seriously polluted.
Disclosure of Invention
The invention aims to solve the problems existing in the use of the copper wire tower structure, and provides a copper wire tower with a supporting device, which is used for removing vanadium impurities in titanium tetrachloride and has the advantages that copper wire balls are soaked in the tower in a sealed manner, waste gas is treated and discharged in a centralized manner, environmental pollution is avoided, and the falling speed of the copper wire balls can be safely and effectively controlled and prevented.
The invention relates to a copper wire tower with a supporting device, which consists of a tower top, a tower body, the supporting device and a tower bottom part. A steam pipe is arranged on the tower top, one side of the steam pipe is provided with a copper wire ball feeding pipe, and the other side is provided with a waste gas discharge pipe. The tower bottom is provided with a steam interface and a reflux interface. The tower top and the tower body are connected into a whole through the concave flange and the convex flange on the tower top and the tower body through bolts. A supporting device is arranged between the tower body and the tower bottom, and the tower body is connected with a concave flange on the supporting device into a whole through a bolt through a convex flange on the tower body.
The symmetrical circumferential outer walls of the cylinder body of the supporting device are respectively provided with a nut, and a rib plate is arranged at the joint of the nut and the cylinder body. The screw rod is arranged in the cylinder body through the nut, the tail end of the screw rod is provided with the sealing cover, the sealing cover is not provided with the sealing cover flange, and the sealing cover flange and the nut flange arranged on the nut are connected into a whole through the bolt. The screw rod on the supporting device and the nut are in a threaded rotation mode, power is transmitted by the screw rod, and the copper wire ball in the tower is supported and loosened through axial movement of the screw rod.
The copper wire tower with the supporting device can clean copper wire balls in a sealing way, and the copper wire balls soaked in the tower can be safely and effectively controlled and prevented from dropping rapidly through adjusting the screw rod, so that the copper wire balls are cleaned in a sealing way,waste gas is discharged after being intensively treated in the tower, and the environmental pollution is avoided. The copper wire balls safely fall out from the tower bottom, and are continuously used after acid washing, rinsing with clear water and drying. The novel multifunctional combined type electric power tool is safe to disassemble, simple and convenient to operate, labor-saving, long in service life and good in environmental protection benefit.
Drawings
FIG. 1 is a schematic cross-sectional view of a copper wire tower with a supporting device according to the present invention.
Detailed Description
The following provides a detailed description of the embodiment of the copper-wire tower with supporting device according to the present invention with reference to the above-mentioned examples of the drawings.
An example of the copper wire tower with the supporting device of the invention comprises a tower top 3, a tower body 4, a supporting device 17 and a tower bottom 13. The steam pipe 1 is arranged on the tower top 3, the steam pipe 1 is connected with cooling equipment outside the tower, and gas in the tower is condensed and recycled to obtain a product. One side of the steam pipe 1 is provided with a copper wire ball feeding pipe 2, and the copper wire ball enters the tower through the pipe orifice. The other side of the steam pipe 1 is provided with a waste gas discharge pipe 18 which is connected with the equipment of the three-waste treatment system outside the tower, and the pipeline is normally closed and is opened for use when the copper wire ball in the tower is used and loses efficacy and needs to be soaked. The bottom 13 of the tower is provided with a steam interface 11 and a reflux interface 12, and the steam interface 11 is connected with a steam pipe on the distillation kettle cover outside the tower. The tower top 3 and the tower body 4 are connected into a whole by a sealing pad which is sleeved on the concave flange and the convex flange through bolts. A supporting device 17 is arranged between the tower body 4 and the tower bottom 13 and is composed of a cylinder 9 and a nut 8, a nut flange 14, a rib plate 16, a screw 6, a sealing cover 15 and a sealing cover flange 7 which are respectively arranged on the symmetrical circumferential outer wall of the cylinder. The tower body 4 is connected with the concave flange 5 on the supporting device 17 through the convex flange on the tower body and the sealing pad on the tower body through bolts. The nut 8 is arranged on the symmetrical circumferential outer wall of the barrel 9, and the nut 8 and the barrel 9 are reinforced by the rib plate 16 after the nut 8 and the barrel 9 are welded. The screw rod 6 is arranged in the cylinder 9 through the nut 8, the tail end of the screw rod 6 is provided with a sealing cover 15, and a sealing cover flange 7 and a nut flange 14 are respectively arranged on the sealing cover 15 and the nut 8. The sealing cover flange 7 and the nut flange 14 are sleeved with a sealing pad and connected into a whole through bolts.
The copper wire tower with the supporting device has the advantages that after the copper wire balls in the tower are used, the copper wire balls are easily covered by impurities brought by titanium tetrachloride vapor and products of chemical reaction and lose effectiveness, so that the copper wire balls need to be cleaned. Before cleaning, the devices connected with the outside of the tower on the steam interface 11 and the reflux interface 12 on the tower bottom 13 are disconnected, a drain valve is arranged at the steam interface 11, then a sealing cover 15 on a supporting device 17 is removed, and a screw 6 isscrewed in the direction of the cylinder 9 to support a copper wire ball in the tower. Then, water is fed into the tower from the top 3 of the tower by opening a waste gas discharge pipe 18 on the top 3 of the tower and cutting off a cooling device connected with the steam pipe 1 and the outside of the tower, copper wire balls in the tower are soaked, and waste gas generated during soaking is sucked into a three-waste treatment system outside the tower through the waste gas discharge pipe 18 for centralized treatment.
After the copper wire balls are soaked, a drainage valve arranged on the tower bottom 13 is opened to drain sewage, the tower bottom 13 is disassembled, the sealing cover 15 is disassembled, the screw rod 6 is slowly withdrawn outwards until the copper wire balls are safely placed, the copper wire balls slide into a cleaning pool arranged below the tower bottom 13, and the copper wire balls are used continuously after being washed by acid, rinsed by clean water and dried.
When putting copper wire balls into the tower, the tower bottom 13 is connected with the supporting device 17, the steam connecting buckle 11 and the reflux interface 12 on the tower bottom 13 are connected with devices outside the tower, and then the supporting device 17 is arranged on the sealing cover 15. Finally, the copper wire ball is put into the tower through a copper wire ball feeding pipe 2 on the tower top 3, and then the pipe orifice of the copper wire ball is sealed. At the same time, the three wastes disposal system on the waste gas discharge pipe 18 is closed and the steam pipe 1 and the cooling equipment outside the tower are opened, so that the operator can safely produce the waste gas without being choked by irritant gas.
Claims (3)
1. The utility model provides a be equipped with top of a tower (3), body of the tower (4), the tower bottom (13), be equipped with steam pipe (1) on the top of a tower (3), one side of steam pipe (1) is equipped with copper wire ball charge tube (2), be equipped with steam interface (11) on the bottom of a tower (13), backward flow interface (12), top of a tower (3), body of the tower (4) are through concave, protruding flange on it through bolted connection one-tenth an organic whole be used for detaching titanium tetrachloride in the copper wire tower that has strutting arrangement of vanadium impurity, its characterized in that is equipped with between body of the tower (4) and the bottom of a tower (13) strutting arrangement (17), the opposite side of steam pipe (.
2. The tower with supporting devices according to claim 1, characterised in that the tower body (4) is bolted with its male flange to the female flange (5) of the supporting device (17).
3. The copper wire tower with the supporting device according to claim 1, wherein nuts (8) are respectively arranged on symmetrical circumferential outer walls of a barrel (9) of the supporting device (17), rib plates (16) are arranged at the joints of the nuts (8) and the barrel (9), the screw rod (6) is placed into the barrel (9) through the nuts (8), a sealing cover (15) is arranged at the tail end of the screw rod (6), a sealing cover flange (7) is arranged on the sealing cover (15), and the sealing cover flange (7) and the nut flange (14) arranged on the nut (8) are connected into a whole through bolts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100511638A CN100376699C (en) | 2006-07-28 | 2006-07-28 | Copper wire tower having supporting device used for removing vanadium impurity in titanium tetrachloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100511638A CN100376699C (en) | 2006-07-28 | 2006-07-28 | Copper wire tower having supporting device used for removing vanadium impurity in titanium tetrachloride |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1904096A true CN1904096A (en) | 2007-01-31 |
| CN100376699C CN100376699C (en) | 2008-03-26 |
Family
ID=37673460
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006100511638A Expired - Fee Related CN100376699C (en) | 2006-07-28 | 2006-07-28 | Copper wire tower having supporting device used for removing vanadium impurity in titanium tetrachloride |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN100376699C (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101638248B (en) * | 2008-08-01 | 2012-03-28 | 沈阳铝镁设计研究院有限公司 | Method and system for recovering residual titanium tetrachloride in copper-wire tower |
| CN103130264A (en) * | 2013-02-05 | 2013-06-05 | 仙桃市中星电子材料有限公司 | Titanium tetrachloride copper wire tower with self-cleaning function and cleaning method of copper wire ball of copper wire tower |
| CN103615868A (en) * | 2013-03-12 | 2014-03-05 | 中航天赫（唐山）钛业有限公司 | Copper wire ball forced convection drying method and device |
| CN106946286A (en) * | 2017-03-09 | 2017-07-14 | 金川集团股份有限公司 | A kind of crude titanic chloride is except the chemical reaction equipment and method of vanadium |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3672492B2 (en) * | 2000-12-20 | 2005-07-20 | 住友チタニウム株式会社 | Purification method of TiCl4 |
| CN1199863C (en) * | 2002-07-19 | 2005-05-04 | 锦州铁合金（集团）有限责任公司钛白粉厂 | Technique and method for treating titanium tetrachloride slurry containing vanadium |
| JP4430287B2 (en) * | 2002-08-12 | 2010-03-10 | 東邦チタニウム株式会社 | Titanium tetrachloride production equipment |
-
2006
- 2006-07-28 CN CNB2006100511638A patent/CN100376699C/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101638248B (en) * | 2008-08-01 | 2012-03-28 | 沈阳铝镁设计研究院有限公司 | Method and system for recovering residual titanium tetrachloride in copper-wire tower |
| CN103130264A (en) * | 2013-02-05 | 2013-06-05 | 仙桃市中星电子材料有限公司 | Titanium tetrachloride copper wire tower with self-cleaning function and cleaning method of copper wire ball of copper wire tower |
| CN103130264B (en) * | 2013-02-05 | 2016-05-18 | 仙桃市中星电子材料有限公司 | There is titanium tetrachloride brass wire tower and the copper wire balls cleaning method thereof of self-cleaning function |
| CN103615868A (en) * | 2013-03-12 | 2014-03-05 | 中航天赫（唐山）钛业有限公司 | Copper wire ball forced convection drying method and device |
| CN106946286A (en) * | 2017-03-09 | 2017-07-14 | 金川集团股份有限公司 | A kind of crude titanic chloride is except the chemical reaction equipment and method of vanadium |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100376699C (en) | 2008-03-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1904096A (en) | Copper wire tower having supporting device used for removing vanadium impurity in titanium tetrachloride | |
| CN209481214U (en) | A kind of grid anti-block apparatus of sewage disposal device | |
| CN208500542U (en) | A kind of sewage-treatment plant convenient for scavenger precipitation object | |
| CN212631959U (en) | Wastewater treatment device for metallurgy | |
| CN214211488U (en) | Cleaning equipment for waste water treatment sediment | |
| CN208711191U (en) | Convenient for the filter of filter element replacing and maintenance cleaning | |
| CN212806475U (en) | Slag removing device for rotary kiln | |
| CN210570126U (en) | Movable multifunctional energy-saving and environment-friendly waste heat recovery equipment | |
| CN219922462U (en) | Waste gas spray tower equipment | |
| CN213193986U (en) | Colliery heat sink | |
| CN216863811U (en) | Acidification oil hydrolysis effluent treatment plant | |
| CN220048141U (en) | Reation kettle convenient to overhaul | |
| CN213895251U (en) | Petrochemical sewage treatment plant | |
| CN216371340U (en) | Cooling liquid mechanism for die machining | |
| CN211676645U (en) | Oil-water separator for recovering lubricating oil | |
| CN215654404U (en) | Water mist treatment device of slag flushing tank | |
| CN213537619U (en) | Full-automatic descaling and dirt removing device | |
| CN217069790U (en) | Steel construction production is with removing dust and removing bits device | |
| CN217601618U (en) | Combined wet dust removal negative pressure water seal drainage device | |
| CN214513532U (en) | Numerical control machining center with dust treatment unit | |
| CN213386779U (en) | Dustproof feeding device of smelting reaction tank | |
| CN209840063U (en) | Boiler backwater purifying and sewage discharging device with filter screen spoiler | |
| CN213102430U (en) | Environment-friendly construction waste treatment facility | |
| CN216445393U (en) | Dirt-removing dust-reducing desulfurizing device for slag stewing pool of steel plant | |
| CN209646225U (en) | A kind of emission-control equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20080326 Termination date: 20120728 |