CN1844340A - Filling candle and process for preparing same - Google Patents
Filling candle and process for preparing same Download PDFInfo
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- CN1844340A CN1844340A CN 200610019056 CN200610019056A CN1844340A CN 1844340 A CN1844340 A CN 1844340A CN 200610019056 CN200610019056 CN 200610019056 CN 200610019056 A CN200610019056 A CN 200610019056A CN 1844340 A CN1844340 A CN 1844340A
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- water
- dodecylbenzene sulfonate
- tensio
- glycerides
- glycerine
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Abstract
This invention relates to a filled candle and the preparation process thereof. The formula by weight ratio is: water 5-25%, glycerin or sorbic alcohol 10-35%, industrial alcohol or methanol 20-69%, monoglyceride 10-59%, aliphatic acid, sodium dodecylbenzene sulfonate, polyglycerol ester or surface activator 1-5%, and optionally degrease 1-49%. The process comprises: firstly mixing water, glycerin or sorbic alcohol, and industrial alcohol or methanol, heated to 70-75deg C, then adding monoglyceride, aliphatic acid, sodium dodecylbenzene sulfonate, polyglycerol ester or surface activator, degrease, heated to 70-75deg C for dissolving, then emulsifying by stirring, neutralizing the pH, and filling into glasses or other containers after cooling to 35-45deg C. This product is characterized of being smokeless, innocuous and smelless when burned, and is a new candle material in substitution of petroleum product.
Description
Technical field
The invention belongs to the candle field, relate to a kind of filling candle and preparation technology thereof.
Background technology
Candle is as the traditional lighting articles for use, use historical remote, prior art is gradually by the processing to its single component paraffin, add some subsidiary material or to the improvement of traditional material to reach the performance that changes candle, as: notification number 1236033, denomination of invention " candle ", adopting paraffin wax fully refined is that major ingredient is equipped with stearic acid again and whipping agent is made.And for example publication number 1271765, denomination of invention " hard transparent wax and manufacture method thereof ", it is by polyamide resin, lipid acid, Fatty Alcohol(C12-C14 and C12-C18), oxidation inhibitor, tensio-active agent, fatty acid ester, Unimac 5680 can be made into the artistic taper and candle of various moulding.Current, face under the day by day nervous situation of petroleum resources, more and more develop for the requirement of candle material towards low-cost, renewable and oligosaprobic environmental protection direction.Therefore, the kind of candle material also needs further to enrich in the prior art, to satisfy real needs of society.
Summary of the invention
Up to the present, still find no the data of any destruction novelty of the present invention, the present invention has obtained best effect by various experiments, thereby has finished the present invention.
It is the filling candle that combination of raw materials forms that one of purpose of the present invention will provide a kind of low cost, renewable and oligosaprobic green material exactly, in particular for substituting existing candle material based on petroleum products.
Two of purpose of the present invention will provide a kind of preparation technology of filling candle exactly.
Filling candle of the present invention is to realize like this, it comprises water, a kind of in glycerine or the sorbyl alcohol, a kind of in industrial spirit or the methyl alcohol, mono-glycerides, and a kind of in lipid acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or the tensio-active agent, it is characterized in that: the each component weight percent is: water 5～25%, glycerine or sorbyl alcohol 10～35%, industrial spirit or methyl alcohol 20～69%, mono-glycerides 10～59%, lipid acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1～5%.
Described component is preferably: described each component weight percent also comprises grease 1～49%.
Requirement to the gross weight of water is: the gross weight of water is greater than 5% of the component gross weight, less than 30% of component gross weight in the component.
One of further preferred be: described lipid acid is stearic acid, described each component weight percent is: water 15%, glycerine or sorbyl alcohol 20%, industrial spirit or methyl alcohol 25%, mono-glycerides 39%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1%.
Further preferred two are: described lipid acid is stearic acid, and described each component weight percent is: water 12%, glycerine or sorbyl alcohol 22%, industrial spirit or methyl alcohol 26%, mono-glycerides 10%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 2%, grease 28%.
The preparation technology of filling candle: earlier with water 5～25%, glycerine or sorbyl alcohol 10～35%, industrial spirit or methyl alcohol 20～69% mix, be heated to 70～75 degree, again with mono-glycerides 10～59%, lipid acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1～5% drop into and wherein are heated to 70～75 degree dissolvings, stirring and emulsifying then, if use lipid acid, need be neutralized to the neutrality of pH value 6.9～7.1 again, be cooled to 35～45 cans when spending at last in the glass cylinder that is placed with the wax core or other containers.
The preparation technology of filling candle is preferably: described lipid acid is stearic acid, also comprise grease in the described component, earlier with water 12%, glycerine or sorbyl alcohol 22%, industrial spirit or methyl alcohol 26% mix, be heated to 70～75 degree, with mono-glycerides 10%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 2% increase grease 28% more again, drop into and wherein be heated to 70～75 degree dissolvings, stirring and emulsifying if use stearic acid, needs to be neutralized to the sodium hydroxide solution of 0.1～1.0 mol the neutrality of pH value 6.9～7.1 again then, use the clarifixator homogeneous, be cooled to 35～45 cans when spending at last in the glass cylinder that is placed with the wax core or other containers.
The filling candle material that the present invention adopts be low-cost, renewable and oligosaprobic green material entirely, filling candle plastic by force, smokelessly nonpoisonous and tasteless during burning, be a kind of candle of new candle material of alternative petroleum products.
Embodiment
Embodiment 1: it comprises water filling candle, a kind of in glycerine or the sorbyl alcohol, a kind of in industrial spirit or the methyl alcohol, mono-glycerides, and a kind of in lipid acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or the tensio-active agent, the each component weight percent is: water 5～25%, glycerine or sorbyl alcohol 10～35%, industrial spirit or methyl alcohol 20～69%, mono-glycerides 10～59%, lipid acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1～5%.
Requirement to the gross weight of water is: the gross weight of water is greater than 5% of the component gross weight, less than 30% of component gross weight in the component.
In the present embodiment: described lipid acid is stearic acid, described each component weight percent is: water 15%, glycerine or sorbyl alcohol 20%, industrial spirit or methyl alcohol 25%, mono-glycerides 39%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1%.
Preparation technology: earlier with water 15%, glycerine or sorbyl alcohol 20%, industrial spirit or methyl alcohol 25% mix, be heated to 70～75 degree, again with mono-glycerides 39%, lipid acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1% drop into and wherein are heated to 70～75 degree dissolvings, stirring and emulsifying then, if use lipid acid, need be neutralized to the neutrality of pH value 6.9～7.1 again, be cooled to 35～45 cans when spending at last in the glass cylinder that is placed with the wax core or other containers.Can add an amount of pigment, essence, sanitas and antioxidant as required.
Embodiment 2: the each component weight percent is: water 5～25%, glycerine or sorbyl alcohol 10～35%, industrial spirit or methyl alcohol 20～69%, mono-glycerides 10～59%, lipid acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1～5%, grease 1～49%.
Requirement to the gross weight of water is: the gross weight of water is greater than 5% of the component gross weight, less than 30% of component gross weight in the component.
In the present embodiment: described lipid acid is stearic acid, and described each component weight percent is: water 12%, glycerine or sorbyl alcohol 22%, industrial spirit or methyl alcohol 26%, mono-glycerides 10%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 2%, grease 28%.Greasy iodine number is 0.1～60.
Preparation technology: earlier with water 12%, glycerine or sorbyl alcohol 22%, industrial spirit or methyl alcohol 26% mix, be heated to 70～75 degree, again with mono-glycerides 10%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 2%, increase grease 28% again, drop into and wherein be heated to 70～75 degree dissolvings, stirring and emulsifying if use stearic acid, needs to be neutralized to the sodium hydroxide solution of 0.1～1.0 mol the neutrality of pH value 6.9～7.1 again then, use the clarifixator homogeneous, be cooled to 35～45 cans when spending at last in the glass cylinder that is placed with the wax core or other containers.Can add an amount of pigment, essence, sanitas and antioxidant as required.
Embodiment 3: the each component weight percent is: water 20%, and glycerine or sorbyl alcohol 30%, industrial spirit or methyl alcohol 20%, mono-glycerides 29%, lipid acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1%, preparation technology is similar with embodiment 1.
Embodiment 4: the each component weight percent is: water 5%, glycerine or sorbyl alcohol 35%, industrial spirit or methyl alcohol 20%, mono-glycerides 33%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 2%, grease 5%.Preparation technology such as embodiment 2 are similar.
Embodiment 5: water 25%, glycerine or sorbyl alcohol 22%, industrial spirit or methyl alcohol 28%, mono-glycerides 23%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 2%.Preparation technology is similar with embodiment 1.
Embodiment 6: water 5%, glycerine or sorbyl alcohol 15%, industrial spirit or methyl alcohol 60%, mono-glycerides 10%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1%, grease 9%.Preparation technology such as embodiment 2 are similar.
Claims (7)
1, a kind of filling candle, it comprises water, a kind of in glycerine or the sorbyl alcohol, a kind of in industrial spirit or the methyl alcohol, mono-glycerides, and a kind of in lipid acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or the tensio-active agent, it is characterized in that: the each component weight percent is: water 5～25%, glycerine or sorbyl alcohol 10～35%, industrial spirit or methyl alcohol 20～69%, mono-glycerides 10～59%, lipid acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1～5%.
2, according to the described a kind of filling candle of claim 1, it is characterized in that: described each component weight percent also comprises grease 1～49%.
3, according to claim 1 or 2 described a kind of filling candles, it is characterized in that: the gross weight of water is greater than 5% of the component gross weight, less than 30% of component gross weight in the described component.
4, according to the described a kind of filling candle of claim 1, it is characterized in that: described lipid acid is stearic acid, described each component weight percent is: water 15%, glycerine or sorbyl alcohol 20%, industrial spirit or methyl alcohol 25%, mono-glycerides 39%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1%.
5, according to the described a kind of filling candle of claim 2, it is characterized in that: described lipid acid is stearic acid, described each component weight percent is: water 12%, glycerine or sorbyl alcohol 22%, industrial spirit or methyl alcohol 26%, mono-glycerides 10%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 2%, grease 28%.
6, preparation technology according to the described a kind of filling candle of claim 1, it is characterized in that: earlier with water 5～25%, glycerine or sorbyl alcohol 10～35%, industrial spirit or methyl alcohol 20～69% mix, be heated to 70～75 degree, again with mono-glycerides 10～59%, lipid acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 1～5% drop into and wherein are heated to 70～75 degree dissolvings, stirring and emulsifying then, if use lipid acid, need be neutralized to the neutrality of pH value 6.9～7.1 again, be cooled to 35～45 cans when spending at last in the glass cylinder that is placed with the wax core or other containers.
7, preparation technology according to the described a kind of filling candle of claim 6, it is characterized in that: described lipid acid is stearic acid, also comprise grease in the described component, earlier with water 12%, glycerine or sorbyl alcohol 22%, industrial spirit or methyl alcohol 26% mix, be heated to 70～75 degree, again with mono-glycerides 10%, stearic acid or Sodium dodecylbenzene sulfonate or polyglycerol ester or tensio-active agent 2%, increase grease 28% again, drop into and wherein to be heated to 70～75 degree dissolvings, stirring and emulsifying then is if use stearic acid, need to be neutralized to the sodium hydroxide solution of 0.1～1.0 mol again the neutrality of pH value 6.9～7.1, use the clarifixator homogeneous.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100190567A CN100455648C (en) | 2006-05-10 | 2006-05-10 | Filling candle and process for preparing same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100190567A CN100455648C (en) | 2006-05-10 | 2006-05-10 | Filling candle and process for preparing same |
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| Publication Number | Publication Date |
|---|---|
| CN1844340A true CN1844340A (en) | 2006-10-11 |
| CN100455648C CN100455648C (en) | 2009-01-28 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006100190567A Expired - Fee Related CN100455648C (en) | 2006-05-10 | 2006-05-10 | Filling candle and process for preparing same |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101575555B (en) * | 2009-06-05 | 2012-02-08 | 张犀诚 | Birthday candle using vegetable oil as raw material and preparation method thereof |
| WO2012071306A1 (en) * | 2010-11-23 | 2012-05-31 | Elevance Renewable Sciences, Inc. | Lipid-based wax compositions substantially free of fat bloom and methods of making |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1030466C (en) * | 1991-12-12 | 1995-12-06 | 陕西省化学研究所 | Composition of colour flame candle and its making method |
-
2006
- 2006-05-10 CN CNB2006100190567A patent/CN100455648C/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101575555B (en) * | 2009-06-05 | 2012-02-08 | 张犀诚 | Birthday candle using vegetable oil as raw material and preparation method thereof |
| WO2012071306A1 (en) * | 2010-11-23 | 2012-05-31 | Elevance Renewable Sciences, Inc. | Lipid-based wax compositions substantially free of fat bloom and methods of making |
| AU2011332097B2 (en) * | 2010-11-23 | 2016-03-31 | Elevance Renewable Sciences, Inc. | Lipid-based wax compositions substantially free of fat bloom and methods of making |
| US9458411B2 (en) | 2010-11-23 | 2016-10-04 | Cargill, Incorporated | Lipid-based wax compositions substantially free of fat bloom and methods of making |
| US10179888B2 (en) | 2010-11-23 | 2019-01-15 | Cargill, Incorporated | Lipid-based wax compositions substantially free of fat bloom and methods of making |
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| Publication number | Publication date |
|---|---|
| CN100455648C (en) | 2009-01-28 |
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Granted publication date: 20090128 Termination date: 20110510 |