CN1802931A - Environment friendly agricultural chemicals for wood and flower and its production method - Google Patents

Environment friendly agricultural chemicals for wood and flower and its production method Download PDF

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CN1802931A
CN1802931A CN 200510107782 CN200510107782A CN1802931A CN 1802931 A CN1802931 A CN 1802931A CN 200510107782 CN200510107782 CN 200510107782 CN 200510107782 A CN200510107782 A CN 200510107782A CN 1802931 A CN1802931 A CN 1802931A
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stemona
langdu
hemlock
tuber
root
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万金林
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Abstract

The invention provides a pesticide for forest and flowers, which comprises plant pesticide and single-purposed auxiliary substance, the plant pesticide comprises alocasia rhizome 30-38kg, Conium maculatum 28-35kg, gelsemium elegans 15-25kg, roor of sessile stemona 25-35kg, Tripterygium wilfordii 22-28kg, radix euphorbiae ebracteolatae 14-22kg, Strychnos ignatii Berg. 13-20kg, the auxiliary agent includes emulsifying agent 7-11kg, gum spirit of turpentine 7.5-15kg, penetrating agent 3-5 kg, preservative agent 0.8-1.6kg, and ethanol 23-30kg. The weight ratio of the plant pesticide and the auxiliary agent is 1-1.5:1.

Description

A kind of forest, flowers environment friendly agricultural and production method
Technical field
The present invention relates to a kind of green agriculture chemicals of noresidue that can prevent and treat forest, gardens, flowers and herbaceous plant damage by disease and insect, concrete is to say that a kind of is the environment friendly agricultural that raw material is made with the Chinese herbal medicine, be a kind of environmental type agricultural chemicals that does not have the secondary toxic residue, the invention still further relates to the method for manufacturing of this environment friendly agricultural.
Background technology
At present, the known forestry extermination of disease and insect pest all will be sprayed a large amount of chemical insecticides.These have the agricultural chemicals of Hazardous, have caused the serious residue of pesticide that exceed standard in forestry, ecology and natural environment, and it is encroaching on the human body of animal and human's class, affect the healthy of the ecological balance and the mankind.Current, it has been recognized that the harmfulness of chemical pesticide, these chemical pesticides have changed soil, make alkalization of soils; Polluted environment, caused serious life too uneven, caused a lot of small animals and birds extinction, its residual harmful substance is also having a strong impact on the human healthy and species procreation of working energetically the world.As everyone knows, chemical pesticide is the important assurance of guaranteeing forest development and urban afforestation, but the chemical pesticide pollution level, destroy the ecological balance and also pollute urban environment, the use of these high toxicities, high residue chemical pesticide causes direct threat to the human life, has become human big public hazards.
For example: the use of chemical pesticide makes the barren and alkalization of soils in soil; These contain the residual of a large amount of harmful chemical pesticides; Animal body is included deposit carcinogen; Make transmutation of species; Make a lot of zoos extinction; All misleads of these chemical pesticides, all strong proof chemical public hazards agricultural chemicals increasing to the extent of injury of the ecological balance, animal survival, human life and large natural environment, also make human cancer morbidity more and more higher.Chemical pesticide has hundreds of the kind in the whole world, the annual whole world is nearly 4,000,000 more than because of the number of chemical pesticide poisoning induced death, and it is directly endangering the healthy of people.Therefore, countries in the world government all seek a kind of nuisanceless, avirulence is residual and the novel forest agricultural chemicals of non-secondary pollution.
At present, all there is following point in the development of domestic and international nuisanceless family medicine:
1, existing public nuisance-free agricultural chemicals result of use extreme difference, this is because it does not form the special-purpose agricultural chemicals that a kind of forestry is used.
Though 2, plant pesticide has fine insecticidal activity.But because of prescription not reason such as science, folk prescription insect is developed immunity to drugs in a short time and does not reach the expection insecticidal effect because it does not form the plant pesticide of a kind of special-purpose control forest, gardens, flowers, the woods and herbaceous plant damage by disease and insect.Present existing plant pesticide can be prevented and treated pest, can prevent and treat forestry pest again, this is unscientific, because agricultural and forestry pest are the insects of typical two big class life habits, for example: pine caterpillars is to arrive endanger in wheatland and the rice field the same, so medication cannot treat different things as the same, must have science, branch seasonality and specific aim and use, just can reach good result.More than many shortcomings, demand urgently improving.
Summary of the invention
The objective of the invention is to provide a kind of Greep pesticide wiith no residue that can prevent and treat forest, gardens, flowers, trees and herbaceous plant damage by disease and insect, is a kind of noresidue, environment-friendly type, no secondary toxicity, free from environmental pollution, the heavy duty detergent environment friendly agricultural that can keep ecological balance and the production method of this agricultural chemicals.
The technical solution adopted in the present invention is: forest, flowers environment friendly agricultural, it is formulated by vegetable insecticide and special assistant, vegetable insecticide is made by Alocasia ordora, hemlock, elegant jessamine, the tuber of stemona, thunder godvine, root of langdu prescription, and its prescription is: Alocasia ordora 30-38kg, hemlock 28-35kg, elegant jessamine 15-25kg, thunder godvine 22-28kg, root of langdu 14-22kg.
Can add Luzon fruit in above-mentioned Lin Lin, flowers environment friendly agricultural prescription, its addition is Luzon fruit 13-20kg.
Auxiliary agent comprises that emulsifier, turpentine oil, bleeding agent, preservative, concentration are 85 ℃-95 ℃ ethanol, and the proportion scale of auxiliary agent is emulsifier 7-11kg, turpentine oil 7.5-15kg, bleeding agent 3-5kg, preservative 0.8-1.6kg, ethanol 23-30kg.
Vegetable insecticide is 1-1.5 with the weight batching ratio of auxiliary agent: 1.
The production method of a kind of forest, flowers environment friendly agricultural:
1, get Alocasia ordora, hemlock, elegant jessamine, the tuber of stemona, thunder godvine, the root of langdu, and respectively with Alocasia ordora, hemlock, elegant jessamine, the tuber of stemona, thunder godvine, root of langdu chopping, it is standby that Luzon really is pressed into part.
2, by charge ratio get above-mentioned various raw material be respectively charged into soak the pool jar in, the water that adds 7 times of amounts of above-mentioned crude drug, soaked at normal temperatures 7-9 hour, extract secondary 75-95 ℃ of boiling, carry about 6-8 hour at every turn, crude drug liquid after the second extraction is combined, refilter, seal up for safekeeping the crude drug liquid running into tank after filtering standby.
3, each filtering liquid medicine of gained is imported respectively in the inspissator, the 0.5-0.1Mpa that reduces pressure is concentrated to 1ml and is equivalent to crude drug liquid 3-6g under 70 ℃ of-90 ℃ of temperature, and mother 23-29Be measures content and collects concentrate, can obtain concentrating paste.
4, each concentrate of gained is got Alocasia ordora 8-15kg respectively, hemlock 7-12kg, elegant jessamine 5-9kg, tuber of stemona 7-14kg, thunder godvine 6-10kg, root of langdu 4-7kg Luzon fruit 4-6kg is input in the reactor, add 75% ethanolic solution in 4: 1 ratios, stir 40-80 and divide bracelet, put into the settling tank precipitation 25-35 hour, the elimination insoluble matter, with gained not in the sedimentation and filtration liquid input destilling tower, be heated to 75-95 ℃ of distillation, reclaim ethanol to 1/2 to 1/3 of original volume, collecting mother liquor inputs in the reactor again, add emulsifier 7-11kg successively by required proportion scale, turpentine oil 7.5-15kg, bleeding agent 3-5kg, preservative 0.8-1.6kg, ethanol 23-30kg, with above-mentioned various auxiliary agent mixing and emulsifying 1.5-3h, promptly obtain forest, the flowers environment friendly agricultural.
Optional tween 35-60 of emulsifier etc. in above-mentioned auxiliary agent, preservative can select that sorbic acid, benzoic acid are received etc., bleeding agent can be selected dimethyl sulfoxide (DMSO) etc.
An important feature of the present invention is to contain multiple biological activity and Combination element components in the medicine, the comprehensive insect antibody factor and science preparation, when the contact of the polypide of insect and food are got it filled thing, can by epidermis penetrate to the skin and body in, through not slightly nerve reach nervous centralis, the block nerves conduction makes insect generation excitement and forms the poisoning shape and death by suffocation.It is better that specialty is used for forest, gardens, flowers and herbaceous plant effect, also can be used for the multiple forest and the flowers control of insect in identical crop and same season.This agricultural chemicals except that disorderly skin texture being arranged and tag the effect, and has stomach toxicity to kill and wound, walk quickly and keep away and strong food refusal effect to insect.
Another one characteristics of the present invention are to contain the required trace element of various plants in the medicine.Behind these agricultural chemicals of plant-spraying such as forest, gardens, flowers, not only have characteristics such as leaf surface brightening is blackish green, vitality is strong, and can also maintaining ecological balance, keep air fresh, also be the indispensable agricultural chemicals that develops forestry and keep ecological balance.For showing the control efficiency of this agricultural chemicals to injurious forest-insect, agricultural chemicals of the present invention in Guangxi in the whole nation, ground such as northeast, Shanxi, Shaanxi, Hubei, Shandong, Anhui, Jiangsu, Sichuan, Zhejiang, Fujian made a large amount of vermins-proof effect comparative trials, proved that this agricultural chemicals has very strong insecticidal effect to forest, flowers and herbaceous plant damage by disease and insect, killing rate reaches 100%, this has just illustrated, though this agricultural chemicals does not contain harmful residuals and secondary toxicity, this agricultural chemicals is to using toxicity very big for the first time.
With 2.5% cream of decamethrin contrast proof, 1 day anti-efficient is respectively 100%, 100%, 99% after the dispenser of 1000,1500,2000 times of dilutions of agricultural chemicals of the present invention medicament; And 1600 times of dilutions of 2.5% cream of decamethrin pharmacy control efficacy rate only is about 70%.After 3 days, 1000,1500,2000 times of dilutions of agricultural chemicals of the present invention pharmacy control efficacy rate is 98%; And 1600 times of dilutions of 2.5% cream of decamethrin pharmacy control efficacy rate is 68%.
Prove that according to test data agricultural chemicals of the present invention and 2.5% cream of decamethrin vermins-proof effect have extremely evident difference.Conclusion is an agricultural chemicals of the present invention, can replace existing chemical pesticide fully.
Agricultural chemicals of the present invention not only has the special pesticide performance, regards as the agricultural chemicals of high toxicity, noresidue and non-secondary pollution according to toxicological test, is a kind of novel green agricultural chemicals.And existing chemical pesticide is except that having high toxicity, also has permanent toxic residue problem, the tool residual life, is long, damaging range is wide, the precipitation accumulation causes serious disease and life harm in human body and animal, this is universally acknowledged global pollution problem, and the extensive degree that chemical pesticide pollutes is well imagined.
Agricultural chemicals of the present invention is that the employing pure natural plant is that raw material is formulated through science processing, not only be noresidue and no secondary toxicity, and do not exist air pollution problems inherent, can be to the natural enemy of insect yet---birds produce secondary and kill, more can be to the human and animal, ecologically constitute harm.
This by facts have proved nothing " three cause " and " three wastes " existence.
Comprehensive the above, a kind of forest of the present invention, flowers environment friendly agricultural be a kind of noresidue feature of environmental protection, no secondary toxicity, pollution-free, keep ecological balance, the heavy duty detergent novel agrochemical, it is to have realized ecological forestry, and the evolution environment is had important assurance, has bright prospects.
Embodiment:
A kind of forest, flowers environment friendly agricultural are formulated by vegetable insecticide and special assistant.Vegetable insecticide is made up of Alocasia ordora, hemlock, elegant jessamine, the tuber of stemona, thunder godvine, the root of langdu, and its prescription is: Alocasia ordora 36kg, hemlock 30kg, elegant jessamine 19kg, tuber of stemona 29kg, thunder godvine 25kg, root of langdu 17kg, Luzon fruit 15kg.Auxiliary agent is made up of public fuel-economizing, ethanol, Tween-60, sorbic acid, dimethyl sulfoxide (DMSO), and its charge ratio is that turpentine oil 11.5kg, concentration are 85% ethanol 26kg, 9kg Tween-60, sorbic acid 1.2kg, dimethyl sulfoxide (DMSO) 4kg.Vegetable insecticide and auxiliary agent charge ratio are 1: 1.
The production method of a kind of forest, flowers environment friendly agricultural:
A, learn from else's experience Alocasia ordora 36kg, hemlock 30kg, elegant jessamine 19kg, tuber of stemona 29kg, thunder godvine 25kg, root of langdu 17kg, Luzon fruit 15kg after handling respectively, be respectively charged into to soak and select in the jar, the water that adds 7 times of crude drug amounts of water, soaked at normal temperatures 7-9 hour, steam heated is to 75-95 ℃, 6h is extracted in boiling, secondary is extracted in boiling respectively, the secondary soup is merged filtration, again filtrate is input to respectively in the inspissator, is decompressed under the 0.5Mpa pressure, under 90 ℃, be concentrated to 1ml, be equivalent to crude drug amount 3-6g, concentration 23-29Be;
B, with each concentrate of gained by getting Alocasia ordora 11kg respectively, hemlock 9kg, elegant jessamine 6kg, tuber of stemona 10kg, thunder godvine 6kg, root of langdu 6kg, Luzon fruit 5kg, and be input in the reactor, adding concentration by 4: 1 weight ratios is 75% ethanol, stirred 50 minutes, put into the settling tank precipitation 30 hours, the elimination insoluble matter, in gained filtrate input destilling tower, be heated to 75-95 ℃, reclaim ethanol to original volume 1/2 to 1/3, collect mother liquor and be input in the reactor again, and add turpentine oil 11.5kg successively, ethanol 26kg, sorb 1.2kg, dimethyl sulfoxide (DMSO) 4kg and 9kg Tween-60, mixing and emulsifying 2h promptly gets a kind of forest, flowers environment friendly agricultural finished product.
Make in the main processes and capital equipment:
The FS-20 slicer that raw material section, chopping are used, raw material pulverizing QJ-3 cracker, molten leaching multi-function extractor DJN-6000 filters and use the KLC-650 filter, the decompression farming device SJN-5000 that contracts, detection gas chromatograph, receipts cream 10m 2Basin, solvent essence are taken dynamic multifunctional extractor DJN-6000, I precipitation settling tank CD-6000, and distillation is reclaimed with multi-functional recovery inspissator DJN-2000B-φ 800, and is synthetic with high-order measuring tank reactor m 2, can GZJ-30 type liquid filling machine etc.

Claims (6)

1, a kind of forest, flowers environment friendly agricultural and production method, be formulated by vegetable insecticide and special assistant, it is characterized in that vegetable insecticide is formulated by Alocasia ordora, hemlock, elegant jessamine, the tuber of stemona, thunder godvine, the root of langdu, its prescription is: Alocasia ordora 30-38kg, hemlock 28-35kg, elegant jessamine 15-25kg, tuber of stemona 25-35kg, thunder godvine 22-28kg, root of langdu 14-22kg; Described auxiliary agent comprises that turpentine oil, concentration are 85-95 ℃ ethanol, emulsifier, bleeding agent, preservative, and the charge ratio of auxiliary agent is emulsifier 7-11kg, turpentine oil 7.5-15kg, bleeding agent 3-5kg, preservative 0.8-1.6kg, ethanol 23-30kg; The charge ratio of vegetable insecticide and special assistant is counted 1-1.5 by weight ratio: 1.
2, a kind of forest according to claim 1, flowers environment friendly agricultural and production method is characterized in that, can add Luzon fruit in the described vegetable insecticide, and its addition is Luzon fruit 13-20kg.
3, according to the described a kind of forest of claim 2, flowers environment friendly agricultural and production method, it is characterized in that, described vegetable insecticide really is made up of Alocasia ordora, hemlock, elegant jessamine, the tuber of stemona, thunder godvine, the root of langdu and Luzon, and its prescription is: Alocasia ordora: 36kg, hemlock: 30kg, elegant jessamine: 19kg, tuber of stemona 29kg, thunder godvine 25kg, root of langdu 17kg, Luzon fruit 15kg; Auxiliary agent is made up of emulsifier, turpentine oil bleeding agent, preservative, ethanol, and its charge ratio is emulsifier 9kg, turpentine oil 11.5kg, bleeding agent 4kg, preservative 1.2kg, ethanol 26kg; Vegetable insecticide and auxiliary agent charge ratio are counted 1: 1 by weight ratio.
4, according to claim 1 or 3 described a kind of forests, flowers environment friendly agricultural and production method, it is characterized in that the optional tween 30-60 of described emulsifier, the optional dimethyl sulfoxide (DMSO) of bleeding agent, the optional sorbic acid of preservative.
5, a kind of forest, flowers environment friendly agricultural and production method is characterized in that:
A, respectively with Alocasia ordora, hemlock, elegant jessamine, the tuber of stemona, thunder godvine, root of langdu chopping, it is standby that Luzon really is pressed into powder;
B, get Alocasia ordora, hemlock, elegant jessamine, the tuber of stemona, thunder godvine, the root of langdu and Luzon after the above-mentioned processing by charge ratio and really be respectively charged into and soak in the pool jar, the water that adds 7 times of amounts of crude drug, soaked at normal temperatures 7-9 hour, extract secondary in boiling below 75-95 ℃, carry 6-8 hour at every turn, second extraction crude drug liquid is merged, filter, the crude drug liquid of collecting after gained filters is standby;
C, each filtering liquid medicine of gained is input to respectively in the inspissator, is decompressed to 0.5-0.1Mpa, under 70-90 ℃ of temperature, be concentrated to 1ml and be equivalent to crude drug 3-6g, be i.e. the concentrated paste of 23-29Be;
D, with each concentrate difference Alocasia ordora 8-15kg of above-mentioned gained, hemlock 7-12kg, elegant jessamine 5-9kg, tuber of stemona 7-14kg, thunder godvine 6-10kg, root of langdu 4-7kg, Luzon fruit 4-6kg, be input in the reactor, add 75% ethanolic solution by 4: 1 weight ratios, stirred 40-80 minute, put into the settling tank precipitation 25-35 hour, the elimination insoluble matter, in gained filtered fluid input destilling tower, be heated to 75-95 ℃ of distillation, reclaim ethanol to 1/2 or 1/3 of original volume, collecting mother liquor is input in the reactor again, add turpentine oil 7.5-15kg successively by required charge ratio, concentration is 85-95 ℃ ethanol, 23-30kg, emulsifier 7-11kg, preservative 0.8-1.6kg, bleeding agent 3-5kg, mixing and emulsifying 1.5-3h promptly gets a kind of forest, the flowers environment friendly agricultural.
6, a kind of forest according to claim 5, flowers environment friendly agricultural and production method is characterized in that:
A, respectively get Alocasia ordora, hemlock, elegant jessamine, the tuber of stemona, thunder godvine, the root of langdu and Luzon really be respectively charged into soak the pool jar in, add the water of 7 times of crude drug amounts, soaked at normal temperatures 6-8 hour, steam heated is to below 75-95 ℃, 6h is extracted in boiling, secondary is extracted in boiling respectively, with the secondary medical filtration, is input to filtering liquid medicine in the inspissator respectively again, 0.5MPa reduces pressure, under 90 ℃, be concentrated to 1ml, be equivalent to crude drug amount 3-6g, concentration 23-9Be.
B, get above-mentioned concentrate Alocasia ordora 11kg respectively, hemlock 9kg, elegant jessamine 6kg, tuber of stemona 10kg, thunder godvine 8kg, root of langdu 6kg, Luzon fruit 5kg, and be input in the reactor, adding concentration by 4: 1 weight ratios is 75% ethanol, stirred 50 minutes, put into the settling tank precipitation 30 hours, the elimination insoluble matter, again with in the gained filtrate input destilling tower, be heated to 75-95 ℃, reclaim ethanol to 1/2 to 1/3 of original volume, collecting mother liquor is input in the reaction again, and add turpentine oil 11.5kg successively, ethanol 26kg, the 9kg Tween-60, sorbic acid 1.2kg, dimethyl sulfoxide (DMSO) 4kg, mixing and emulsifying 2h promptly gets a kind of forest, flowers environment friendly agricultural finished product.
CN 200510107782 2005-09-30 2005-09-30 Environment friendly agricultural chemicals for wood and flower and its production method Pending CN1802931A (en)

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102273491A (en) * 2011-06-22 2011-12-14 华南农业大学 Insecticidal activity of three cicuta L. plant extractives
CN102415417A (en) * 2011-12-16 2012-04-18 天长市中能国泰能源技术有限公司 Non-polluted residue-free green pesticide for fruits and vegetables
CN102422846A (en) * 2011-12-16 2012-04-25 天长市中能国泰能源技术有限公司 Wheat green pesticide
CN102428975A (en) * 2011-12-16 2012-05-02 天长市中能国泰能源技术有限公司 Paddy environmentally-friendly pesticide
CN102550612A (en) * 2011-12-16 2012-07-11 天长市中能国泰能源技术有限公司 Ecological environment-friendly pesticide
CN105123801A (en) * 2015-09-30 2015-12-09 界首市保华种植专业合作社 Compound biological insecticide
CN105994417A (en) * 2016-06-13 2016-10-12 南京信息工程大学 Environment-friendly insecticide and preparation method and application thereof
CN106866273A (en) * 2017-03-28 2017-06-20 苏州市啄木鸟园林植物医院有限公司 A kind of rejuvenation of ancient tree nutrient solution and preparation method thereof
WO2018058539A1 (en) * 2016-09-30 2018-04-05 张爱丽 Floricultural chemical and manufacturing method thereof

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102273491A (en) * 2011-06-22 2011-12-14 华南农业大学 Insecticidal activity of three cicuta L. plant extractives
CN102273491B (en) * 2011-06-22 2013-12-18 华南农业大学 Insecticidal activity of three cicuta L. plant extractives
CN102415417A (en) * 2011-12-16 2012-04-18 天长市中能国泰能源技术有限公司 Non-polluted residue-free green pesticide for fruits and vegetables
CN102422846A (en) * 2011-12-16 2012-04-25 天长市中能国泰能源技术有限公司 Wheat green pesticide
CN102428975A (en) * 2011-12-16 2012-05-02 天长市中能国泰能源技术有限公司 Paddy environmentally-friendly pesticide
CN102550612A (en) * 2011-12-16 2012-07-11 天长市中能国泰能源技术有限公司 Ecological environment-friendly pesticide
CN105123801A (en) * 2015-09-30 2015-12-09 界首市保华种植专业合作社 Compound biological insecticide
CN105994417A (en) * 2016-06-13 2016-10-12 南京信息工程大学 Environment-friendly insecticide and preparation method and application thereof
WO2018058539A1 (en) * 2016-09-30 2018-04-05 张爱丽 Floricultural chemical and manufacturing method thereof
CN106866273A (en) * 2017-03-28 2017-06-20 苏州市啄木鸟园林植物医院有限公司 A kind of rejuvenation of ancient tree nutrient solution and preparation method thereof

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