CN1769365A - Oil extraction microbial conenoses nutrient solution - Google Patents
Oil extraction microbial conenoses nutrient solution Download PDFInfo
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- CN1769365A CN1769365A CN 200510010349 CN200510010349A CN1769365A CN 1769365 A CN1769365 A CN 1769365A CN 200510010349 CN200510010349 CN 200510010349 CN 200510010349 A CN200510010349 A CN 200510010349A CN 1769365 A CN1769365 A CN 1769365A
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- nutrient solution
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- oil extraction
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Abstract
The invention relates to a micro-organism nutrient solution for petroleum production, which comprises the components of (by weight proportion) urea 1-3%, NH4Cl 0.05-0.1%, amino acid 0.5-1%, NH3NO3 0.05-0.25%, Na2HPO4 0.1-0.5%, MgSO4*7H2O 0.01-0.05%, FeSO4*5H2O 0.05-0.1%, CaCl2 0.05-0.1%, ZnCl2 0.05-0.1%, molasses 1-4%, isodulcitol 0.1-0.5%, C8-C10 alkyl glycoside 1-5%, and balancing water.
Description
Technical field:
The present invention relates to a kind of chemical agent of oil recovery usefulness in the oilfield exploitation field, belong to a kind of oil extraction microbial conenoses nutrient solution.
Background technology:
It is the technology that improves oil recovery factor rapidly of development both at home and abroad at present that microorganism is improved petroleum recovery technology, is 21 century high-new biotechnology.Compare with other tertiary oil recovery technologies, that the microbe oil production technology has is applied widely, technology is simple, characteristics such as good in economic efficiency, pollution-free, thereby more and more is subject to people's attention.Comparatively general biological oil recovery technique mainly is to introduce inoculating microbe in oil reservoir at present, in oil reservoir, inject simultaneously nutritive medium, microorganism is bred in oil reservoir, utilize its meta-bolites gas, acid, tensio-active agent, polymkeric substance etc., improve oil recovery factor.But this method has bacterial classification need develop and evaluation, the numerous and diverse shortcoming of bacterium liquid fermentation, and the microorganism of injection exists oil reservoir is adapted to the race problem that reaches with oil reservoir indigenous microorganism (the original microorganism of oil reservoir).
Summary of the invention:
The present invention is directed to above-mentioned the deficiencies in the prior art, propose a kind of indigenous microorganism nutrient solution and activate indigenous microorganism in the oil reservoir, thereby reach the purpose that improves the microbe oil production effect.Indigenous microorganism is meant that inhabiting for a long time in the oil reservoir with the hydrocarbon is the microorganism of sole carbon source growth.The indigenous microorganism oil recovery technique is a kind of biotechnology that increases oil recovery by the biological activity of adjusting intrinsic group in the oil reservoir.Indigenous microorganism is a metastable microflora on the inherent value volume and range of product of certain period in the stratum.This is to enter oil reservoir with the injection water that contains a large amount of bacteriums in oilfield development process.Because the difference of bacterial species etc., the incompatibility ground environment that has and dying, what have passs on into dormant state, also has a small amount of bacterium to adapt to abominable ground environment, and utilizes nutrition limited in the stratum to grow slowly and metabolism.Because the mesotrophic shortage in stratum has hindered a large amount of breedings of indigenous microorganism, therefore, as long as an amount of nutritive substance is provided and is injected into oil reservoir and just can selectively will help improving the bacterium activation of recovery ratio by appropriate means, and tachymetabolism is of value to the product of crude oil flow, raising reservoir development degree and recovery ratio.
The technical solution adopted in the present invention is: this oil extraction microbial conenoses nutrient solution comprises following each component, following each compositions in weight percentage proportioning: urea 1%～3%, NH
4CL 0.05～0.1%, amino acid 0.5～1%, NH
3NO
30.05 Na～0.25%,
2HPO
40.1%～0.5%, MgSO
47H
2O 0.01%～0.05%, FeSO
45H
2O 0.05%～0.1%, CaCL
20.05%～0.1%, ZnCL
20.05%～0.1%, molasses 1%～4%, rhamnosyl 0.1～0.5% and C
8～10Alkyl glycoside 1%～5%, surplus are water.
Above-mentioned urea 3%, NH
4CL 0.1%, amino acid 0.5%, NH
3NO
30.1%, Na
2HPO
40.3%, MgSO
47H
2O 0.01%, FeSO
45H
2O 0.05%, CaCL
20.05%, ZnCL
20.06%, molasses 4%, rhamnosyl 0.1% and C
8～10Alkyl glycoside 1%, water are 90.76%; Urea 2%, NH
4CL 0.07%, amino acid 0.8%, NH
3NO
30.15%, Na
2HPO
40.5%, MgSO
47H
2O0.02%, FeSO
45H
2O 0.08%, CaCL
20.1%, ZnCL
20.07%, molasses 2%, rhamnosyl 0.2% and C
8～10Alkyl glycoside 2%, water are 92.01%.
According to one or more the mixture that also can add in different these nutritive mediums of ground environment and temperature range in the following component: KNO
30～0.05%, (NH
4)
2SO
40～0.1%, KH
2PO
40～0.5%, Amino Trimethylene Phosphonic Acid 0～0.5%, butter cream 0～0.5%, sheep blood 0～1% and MgCL
24H
2O 0%～0.02%.
Above-mentioned nutritive medium using method is as follows: by injection pump biological nutrient liquid and pressurized air are injected the stratum by the waterflood-transmission line bypass, every mouthful of annual construction 4～6 of well is taken turns, and the interval is 50～70 days between the two-wheeled, construction is 2 years continuously, every individual well of taking turns is divided 3 injections, annotates closing well 1 day 1～2 day at every turn.
The invention has the beneficial effects as follows: indigenous microorganism is to rely on sole carbon source " hydro carbons " in the oil reservoir for nutrition as mentioned above, and it is exactly to provide enough nutritive substances to indigenous microorganism that the activation indigenous microorganism is feared by institute, makes its breeding, growth.
Microbial reaction thing and the effect table 1 in improving recovery ratio thereof
| Reactant | Do powerful |
| Acid | Increase rock porosity and rate of permeation and inorganic carbonate reactant salt and generate CO2 |
| Organism | Selectivity/nonselective shutoff sticks to the crude oil surface and plays the desulfidation that emulsifying effect changes mineral surface wettability reduction viscosity of crude and pour crude oil |
| Gas | Reservoir replenishes pressurization; The crude oil swelling agent; Reduce viscosity dissolved carbon hydrochlorate rock and increase rate of permeation |
| Solvent | The crude oil solvating agent |
| Tensio-active agent | Reduce oil water interfacial tension; Emulsifying effect |
| Polymkeric substance | Mobility control; Selectivity/non-selective shutoff |
By using this nutritive medium to have economic attractiveness to marginal production fields, cost is low, and effective period is long, and required equipment is simple.Do not need to inject microorganism to oil reservoir.Therefore producing microbial or required program and the expense of metabolite increase do not need to make a living.Adopt traditional water filling uphole equipment can reach construction requirement.Microbial nutrient solution is with low cost and not influenced by crude oil price; Can be used for various types of crude oil; Do not damage the stratum, can in same oil well, repeatedly use; Do not pollute stratum and ground environment; Improve recovery ratio 10% than original method.
This biological nutrient liquid and using method thereof are in the aboveground guide's experiment of having carried out reaching 3 years of the Shi Wukou of Dagang Oilfield.Accumulative total is injected 82.366 tons of concentrated nutrient solutions, air 91.2m
3, viscosity of crude descends, and methane content increases in the Sweet natural gas, and water ratio descends 2%; Improved fluid properties; Oil recovery factor and gas production have been improved.By China National Petroleum Corp.'s tertiary oil recovery evaluation method, accumulation increases oily 12211t in the period of 3.
Description of drawings:
Fig. 1 is a process flow sheet of the present invention.
Embodiment:
The invention will be further described below in conjunction with embodiment: this oil extraction microbial conenoses nutrient solution comprises following each component, following each compositions in weight percentage proportioning: urea 1%～3%, NH
4CL 0.05～0.1%, amino acid 0.5～1%, NH
3NO
30.05 Na～0.25%,
2HPO
40.1%～0.5%, MgSO
47H
2O 0.01%～0.05%, FeSO
45H
2O 0.05%～0.1%, CaCL
20.05%～0.1%, ZnCL
20.05%～0.1%, molasses 1%～4%, rhamnosyl 0.1～0.5% and C
8～10Alkyl glycoside 1%～5%, surplus are water.Above-mentioned each component preferred content is urea 3%, NH
4CL 0.1%, amino acid 0.5%, NH
3NO
30.1%, Na
2HPO
40.3%, MgSO
47H
2O0.01%, FeSO
45H
2O 0.05%, CaCL
20.05%, ZnCL
20.06%, molasses 4%, rhamnosyl 0.1% and C
8～10Alkyl glycoside 1%, water are 90.76%; Urea 2%, NH
4CL 0.07%, amino acid 0.8%, NH
3NO
30.15%, Na
2HPO
40.5%, MgSO
47H
2O 0.02%, FeSO
45H
2O 0.08%, CaCL
20.1%, ZnCL
20.07%, molasses 2%, rhamnosyl 0.2% and C
8～10Alkyl glycoside 2%, water are 92.01%.
According to one or more the mixture that also can add in different these nutritive mediums of ground environment and temperature range in the following component: KNO
30～0.05%, (NH
4)
2SO
40～0.1%, KH
2PO
40～0.5%, Amino Trimethylene Phosphonic Acid 0～0.5%, butter cream 0～0.5%, sheep blood 0～1% and MgCL
24H
2O 0%～0.02%.
Each component in the technique scheme is promptly obtained this nutritive medium to be mixed under normal temperature condition.
In the technique scheme: molasses, C
8～10Alkyl glycoside, butter cream, sheep blood, rhamnosyl and amino acid provide sugared source for microorganism; Urea, NH
4CL, KNO
3, NH
3NO
3, (NH
4)
2SO
4For microorganism provides nitrogenous source; Na
2HPO
4, KH
2PO
4, ATMP provides the phosphorus source for microorganism; MgSO
47H
2O, MgCL
24H
2O, FeSO
45H
2O, CaCL
2, ZnCL
2For microorganism provides other element nutrition.
Above-mentioned nutritive medium using method is as follows: as shown in Figure 1: by injection pump biological nutrient liquid and pressurized air are injected the stratum by the waterflood-transmission line bypass, every mouthful of annual construction 4～6 of well is taken turns, the interval is 50～70 days between the two-wheeled, construction is 2 years continuously, every individual well of taking turns is divided 3 injections, each notes 1～2 day, closing well 1 day.
Embodiment 1, be example with 35000 kilograms of daily water-injection rates, with 1157.28 kilograms in urea, NH
438.58 kilograms of CL, 92.88 kilograms of amino acid/11s, NH
3NO
338.58 kilogram, Na
2HPO
4115.73 kilogram, MgSO
47H
23.86 kilograms of O, FeSO
45H
219.29 kilograms of O, CaCL
219.29 kilogram, ZnCL
223.15 kilogram, 1543.04 kilograms in molasses, 38.58 kilograms of rhamnosyls and C
8～10Alkyl glycoside after the mixing, is carried out guide experiment with biological nutrient liquid and pressurized air by waterflood-transmission line bypass injection stratum by injection pump for 385.76 kilograms in material-compound tank, every mouthful of each construction 5 of well is taken turns, construction is 2 years continuously, every individual well of taking turns is divided 3 injections, annotates closing well 1 day 1 day at every turn.This method improves recovery ratio 10% than original method, and water ratio descends 2%.
Embodiment 2, be example with 35000 kilograms of daily water-injection rates, with 760.79 kilograms in urea, NH
4CL26.63 kilogram, 304.31 kilograms in amino acid, NH
3NO
357.06 kilogram, Na
2HPO
4190.20 kilogram, MgSO
47H
27.61 kilograms of O, FeSO
45H
230.43 kilograms of O, CaCL
238.04 kilogram, ZnCL
226.63 kilogram, 760.79 kilograms in molasses, 76.08 kilograms of rhamnosyls and C
8～10Alkyl glycoside after the mixing, is carried out guide experiment with biological nutrient liquid and pressurized air by waterflood-transmission line bypass injection stratum by injection pump for 760.79 kilograms in material-compound tank, every mouthful of each construction 5 of well is taken turns, construction is 2 years continuously, every individual well of taking turns is divided 3 injections, annotates closing well 1 day 1 day at every turn.This method improves recovery ratio 10% than original method, and water ratio descends 2%.
Embodiment 3, be example with 35000 kilograms of daily water-injection rates, with 384.74 kilograms in urea, NH
4CL19.24 kilogram, 384.74 kilograms in amino acid, NH
3NO
319.24 kilogram, Na
2HPO
438.47 kilogram, MgSO
47H
219.24 kilograms of O, FeSO
45H
238.47 kilograms of O, CaCL
230.78 kilogram, ZnCL
238.47 kilogram, 384.74 kilograms in molasses, 192.37 kilograms of rhamnosyls and C
8～10Alkyl glycoside after the mixing, is carried out guide experiment with biological nutrient liquid and pressurized air by waterflood-transmission line bypass injection stratum by injection pump for 1923.71 kilograms in material-compound tank, every mouthful of each construction 5 of well is taken turns, construction is 2 years continuously, every individual well of taking turns is divided 3 injections, annotates closing well 1 day 1 day at every turn.This method improves recovery ratio 10% than original method, and water ratio descends 2%.
Embodiment 4, be example with 35000 kilograms of daily water-injection rates, with 1170.83 kilograms in urea, NH
439.03 kilograms of CL, 95.14 kilograms of amino acid/11s, NH
3NO
339.03 kilogram, Na
2HPO
4117.08 kilogram, MgSO
47H
23.90 kilograms of O, FeSO
45H
219.51 kilograms of O, CaCL
219.51 kilogram, ZnCL
223.42 kilogram, 1561.11 kilograms in molasses, 39.03 kilograms of rhamnosyls, C
8～10390.28 kilograms of alkyl glycoside, KNO
3After 19.51 195.14 kilograms of kilograms, 195.14 kilograms of Amino Trimethylene Phosphonic Acid and butter cream mix in material-compound tank, by injection pump biological nutrient liquid and pressurized air are carried out guide's experiment by waterflood-transmission line bypass injection stratum, every mouthful of each construction 5 of well is taken turns, construction is 2 years continuously, every individual well of taking turns is divided 3 injections, each notes 1 day, closing well 1 day.This method improves recovery ratio 10% than original method, and water ratio descends 2%.This experiment is fit to contain shuttle shape bud bacillus, genus bacillus, false pseudomonas bacillus, Xanthomonas campestris, leukonid, desulfovibrio in the stratum.
Embodiment 5, be example with 35000 kilograms of daily water-injection rates, with 391.72 kilograms in urea, NH
4CL19.59 kilogram, 391.72 kilograms in amino acid, NH
3NO
319.59 kilogram, Na
2HPO
439.17 kilogram, MgSO
47H
219.59 kilograms of O, FeSO
45H
239.17 kilograms of O, CaCL
231.34 kilogram, ZnCL
239.17 kilogram, 391.72 kilograms in molasses, 195.86 kilograms of rhamnosyls, C
8～101958.59 kilograms of alkyl glycoside, (NH
4)
2SO
439.17 kilogram, KH
2PO
4195.86 kilogram, 391.72 kilograms of sheep blood and MgCL
24H
2O after the mixing, carries out guide experiment with biological nutrient liquid and pressurized air by waterflood-transmission line bypass injection stratum by injection pump for 7.83 kilograms in material-compound tank, every mouthful of each construction 5 of well is taken turns, construction is 2 years continuously, every individual well of taking turns is divided 3 injections, annotates closing well 1 day 1 day at every turn.This method improves recovery ratio 10% than original method, and water ratio descends 2%.This experiment is fit to contain mycobacterium, Nocardia bacteria, acinetobacter calcoaceticus, coryneform bacteria, enterobacteria in the stratum.
Claims (4)
1, a kind of oil extraction microbial conenoses nutrient solution is characterized in that: comprise following each component, following each compositions in weight percentage proportioning: urea 1%～3%, NH
4CL 0.05～0.1%, amino acid 0.5～1%, NH
3NO
30.05 Na～0.25%,
2HPO
40.1%～0.5%, MgSO
47H
2O 0.01%～0.05%, FeSO
45H
2O 0.05%～0.1%, CaCL
20.05%～0.1%, ZnCL
20.05%～0.1%, molasses 1%～4%, rhamnosyl 0.1～0.5% and C
8～10Alkyl glycoside 1%～5%, surplus are water.
2, oil extraction microbial conenoses nutrient solution according to claim 1 is characterized in that: urea 3%, NH
4CL 0.1%, amino acid 0.5%, NH
3NO
30.1%, Na
2HPO
40.3%, MgSO
47H
2O 0.01%, FeSO
45H
2O 0.05%, CaCL
20.05%, ZnCL
20.06%, molasses 4%, rhamnosyl 0.1% and C
8～10Alkyl glycoside 1%, water are 90.76%.
3, oil extraction microbial conenoses nutrient solution according to claim 1 is characterized in that: urea 2%, NH
4CL 0.07%, amino acid 0.8%, NH
3NO
30.15%, Na
2HPO
40.5%, MgSO
47H
2O 0.02%, FeSO
45H
2O 0.08%, CaCL
20.1%, ZnCL
20.07%, molasses 2%, rhamnosyl 0.2% and C
8～10Alkyl glycoside 2%, water are 92.01%.
4, oil extraction microbial conenoses nutrient solution according to claim 1 is characterized in that: also comprise one or more mixture in following each component: KNO for this nutritive medium of different geographical environments
30～0.05%, (NH
4)
2SO
40～0.1%, KH
2PO
40～0.5%, Amino Trimethylene Phosphonic Acid 0～0.5%, butter cream 0～0.5%, sheep blood 0～1% and MgCL
24H
2O0%～0.02%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100103494A CN1325599C (en) | 2005-09-16 | 2005-09-16 | Oil extraction microbial conenoses nutrient solution |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100103494A CN1325599C (en) | 2005-09-16 | 2005-09-16 | Oil extraction microbial conenoses nutrient solution |
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| Publication Number | Publication Date |
|---|---|
| CN1769365A true CN1769365A (en) | 2006-05-10 |
| CN1325599C CN1325599C (en) | 2007-07-11 |
Family
ID=36750915
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|---|---|---|---|
| CNB2005100103494A Expired - Fee Related CN1325599C (en) | 2005-09-16 | 2005-09-16 | Oil extraction microbial conenoses nutrient solution |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101210193B (en) * | 2007-12-25 | 2010-11-24 | 天津市工业微生物研究所 | Pipeline transportation method for easy-condensing high-viscous crude oil after degraded by microorganism |
| CN102116143A (en) * | 2010-12-30 | 2011-07-06 | 佘跃惠 | Method for extracting oil by utilizing indigenous microbe of oil pool subjected to polymer flooding |
| CN104212431A (en) * | 2014-06-29 | 2014-12-17 | 北京大学工学院包头研究院 | Petroleum endogenous microbe activating system, and screening method and application thereof |
| CN104431554A (en) * | 2014-12-15 | 2015-03-25 | 重庆市万源禽蛋食品有限公司 | Composition for preventing and treating bacterial pullorum |
| CN104522316A (en) * | 2014-12-15 | 2015-04-22 | 重庆市万源禽蛋食品有限公司 | Composition for preventing and treating chicken enteritis |
| CN105756637A (en) * | 2014-12-19 | 2016-07-13 | 中国石油天然气股份有限公司 | Method for increasing coal-bed gas recovery ratio by using coal-bed indigenous microbes |
| CN116285927A (en) * | 2023-03-28 | 2023-06-23 | 华东理工大学 | Method for improving metabolism activity of microorganisms in thickened oil and application |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4475590A (en) * | 1982-12-13 | 1984-10-09 | The Standard Oil Company | Method for increasing oil recovery |
| US4905761A (en) * | 1988-07-29 | 1990-03-06 | Iit Research Institute | Microbial enhanced oil recovery and compositions therefor |
| US5368099A (en) * | 1992-11-04 | 1994-11-29 | Phillips Petroleum Company | Injection of dextrins for subterranean microbial processes |
| CN1419035A (en) * | 2002-12-12 | 2003-05-21 | 华东理工大学 | Microbe oil extraction method |
| WO2005005773A2 (en) * | 2003-07-14 | 2005-01-20 | The Energy Research Institute | A process for enhanced recovery of crude oil from oil wells using novel microbial consortium |
-
2005
- 2005-09-16 CN CNB2005100103494A patent/CN1325599C/en not_active Expired - Fee Related
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101210193B (en) * | 2007-12-25 | 2010-11-24 | 天津市工业微生物研究所 | Pipeline transportation method for easy-condensing high-viscous crude oil after degraded by microorganism |
| CN102116143A (en) * | 2010-12-30 | 2011-07-06 | 佘跃惠 | Method for extracting oil by utilizing indigenous microbe of oil pool subjected to polymer flooding |
| CN102116143B (en) * | 2010-12-30 | 2014-04-02 | 长江大学 | Method for extracting oil by utilizing indigenous microbe of oil pool subjected to polymer flooding |
| CN104212431A (en) * | 2014-06-29 | 2014-12-17 | 北京大学工学院包头研究院 | Petroleum endogenous microbe activating system, and screening method and application thereof |
| CN104431554A (en) * | 2014-12-15 | 2015-03-25 | 重庆市万源禽蛋食品有限公司 | Composition for preventing and treating bacterial pullorum |
| CN104522316A (en) * | 2014-12-15 | 2015-04-22 | 重庆市万源禽蛋食品有限公司 | Composition for preventing and treating chicken enteritis |
| CN105756637A (en) * | 2014-12-19 | 2016-07-13 | 中国石油天然气股份有限公司 | Method for increasing coal-bed gas recovery ratio by using coal-bed indigenous microbes |
| CN105756637B (en) * | 2014-12-19 | 2018-11-16 | 中国石油天然气股份有限公司 | A method of coal bed gas recovery ratio is improved beneficial to endogenous microbes using coal seam |
| CN116285927A (en) * | 2023-03-28 | 2023-06-23 | 华东理工大学 | Method for improving metabolism activity of microorganisms in thickened oil and application |
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Effective date of registration: 20200616 Address after: Room 0912, building 2, Greenland Central Plaza, plot B07, Xiaotangshan Town, Changping District, Beijing 102200 Patentee after: BEIJING VICTEX ENVIRONMENTAL PROTECTION TECHNOLOGY DEVELOPMENT Co.,Ltd. Address before: 163114, No. 6, Hongwei Chemical Industrial Park, hi tech Industrial Development Zone, Heilongjiang, Daqing Patentee before: DAQING VERTEX CHEMICAL Co.,Ltd. |
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Granted publication date: 20070711 Termination date: 20200916 |